CA1038597A - Process for reacting nitric oxide with hydrogen - Google Patents
Process for reacting nitric oxide with hydrogenInfo
- Publication number
- CA1038597A CA1038597A CA204,866A CA204866A CA1038597A CA 1038597 A CA1038597 A CA 1038597A CA 204866 A CA204866 A CA 204866A CA 1038597 A CA1038597 A CA 1038597A
- Authority
- CA
- Canada
- Prior art keywords
- gas
- liquid
- column
- process according
- bubbles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims abstract description 16
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 title abstract description 12
- 239000001257 hydrogen Substances 0.000 title description 4
- 229910052739 hydrogen Inorganic materials 0.000 title description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title description 3
- 239000007789 gas Substances 0.000 claims abstract description 82
- 239000007788 liquid Substances 0.000 claims abstract description 49
- 239000002912 waste gas Substances 0.000 claims abstract description 14
- 239000003054 catalyst Substances 0.000 claims abstract description 10
- 229910000510 noble metal Inorganic materials 0.000 claims abstract description 4
- 238000006243 chemical reaction Methods 0.000 claims description 17
- 239000011261 inert gas Substances 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 6
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims description 4
- 239000006227 byproduct Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000002699 waste material Substances 0.000 claims description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 2
- 229910001338 liquidmetal Inorganic materials 0.000 claims 1
- 238000004064 recycling Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 description 9
- 239000000725 suspension Substances 0.000 description 5
- 239000000470 constituent Substances 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000003377 acid catalyst Substances 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- 238000009903 catalytic hydrogenation reaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- -1 hydroxylamine salt Chemical class 0.000 description 1
- 150000002443 hydroxylamines Chemical class 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001272 nitrous oxide Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000010517 secondary reaction Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Catalysts (AREA)
- Gas Separation By Absorption (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1036273A CH584163A5 (OSRAM) | 1973-07-17 | 1973-07-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1038597A true CA1038597A (en) | 1978-09-19 |
Family
ID=4362397
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA204,866A Expired CA1038597A (en) | 1973-07-17 | 1974-07-16 | Process for reacting nitric oxide with hydrogen |
Country Status (16)
| Country | Link |
|---|---|
| JP (1) | JPS5529925B2 (OSRAM) |
| AR (1) | AR199539A1 (OSRAM) |
| BE (1) | BE817700A (OSRAM) |
| CA (1) | CA1038597A (OSRAM) |
| CH (1) | CH584163A5 (OSRAM) |
| DE (1) | DE2433967B2 (OSRAM) |
| EG (1) | EG11522A (OSRAM) |
| ES (1) | ES428311A1 (OSRAM) |
| FR (1) | FR2237835B1 (OSRAM) |
| GB (1) | GB1463857A (OSRAM) |
| IN (1) | IN141812B (OSRAM) |
| IT (1) | IT1029605B (OSRAM) |
| MY (1) | MY7800016A (OSRAM) |
| NL (1) | NL7409661A (OSRAM) |
| PH (1) | PH10936A (OSRAM) |
| TR (1) | TR18418A (OSRAM) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2736872B2 (de) * | 1977-08-16 | 1979-07-19 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Hydroxylammoniumsalzen |
| DE3130305A1 (de) * | 1981-07-31 | 1983-02-17 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von hydroxylammoniumsalzen |
| JPH03124752U (OSRAM) * | 1990-03-28 | 1991-12-17 |
-
1973
- 1973-07-17 CH CH1036273A patent/CH584163A5/xx not_active IP Right Cessation
-
1974
- 1974-07-06 IN IN1518/CAL/1974A patent/IN141812B/en unknown
- 1974-07-12 TR TR18418A patent/TR18418A/xx unknown
- 1974-07-12 PH PH16036A patent/PH10936A/en unknown
- 1974-07-15 DE DE19742433967 patent/DE2433967B2/de active Granted
- 1974-07-15 IT IT52111/74A patent/IT1029605B/it active
- 1974-07-15 FR FR7424505A patent/FR2237835B1/fr not_active Expired
- 1974-07-15 AR AR254691A patent/AR199539A1/es active
- 1974-07-16 ES ES74428311A patent/ES428311A1/es not_active Expired
- 1974-07-16 CA CA204,866A patent/CA1038597A/en not_active Expired
- 1974-07-16 BE BE146597A patent/BE817700A/xx unknown
- 1974-07-16 EG EG278/74A patent/EG11522A/xx active
- 1974-07-17 NL NL7409661A patent/NL7409661A/xx not_active Application Discontinuation
- 1974-07-17 JP JP8209474A patent/JPS5529925B2/ja not_active Expired
- 1974-08-07 GB GB3473574A patent/GB1463857A/en not_active Expired
-
1978
- 1978-12-31 MY MY197816A patent/MY7800016A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR2237835A1 (OSRAM) | 1975-02-14 |
| IN141812B (OSRAM) | 1977-04-23 |
| PH10936A (en) | 1977-10-05 |
| FR2237835B1 (OSRAM) | 1978-12-29 |
| TR18418A (tr) | 1977-01-28 |
| DE2433967A1 (de) | 1975-02-13 |
| JPS5529925B2 (OSRAM) | 1980-08-07 |
| MY7800016A (en) | 1978-12-31 |
| AR199539A1 (es) | 1974-09-09 |
| EG11522A (en) | 1978-03-29 |
| DE2433967B2 (de) | 1977-02-17 |
| GB1463857A (en) | 1977-02-09 |
| CH584163A5 (OSRAM) | 1977-01-31 |
| NL7409661A (nl) | 1975-01-21 |
| IT1029605B (it) | 1979-03-20 |
| JPS5043099A (OSRAM) | 1975-04-18 |
| ES428311A1 (es) | 1976-07-16 |
| BE817700A (fr) | 1974-11-18 |
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