BRPI0518767A2 - processo para a produÇço de alfa-alcàxi-âmega-hidràxi-polialquilenoglicàis puros - Google Patents
processo para a produÇço de alfa-alcàxi-âmega-hidràxi-polialquilenoglicàis purosInfo
- Publication number
- BRPI0518767A2 BRPI0518767A2 BRPI0518767-2A BRPI0518767A BRPI0518767A2 BR PI0518767 A2 BRPI0518767 A2 BR PI0518767A2 BR PI0518767 A BRPI0518767 A BR PI0518767A BR PI0518767 A2 BRPI0518767 A2 BR PI0518767A2
- Authority
- BR
- Brazil
- Prior art keywords
- sub
- hydroxy
- polyalkylene glycols
- alkoxy
- omega
- Prior art date
Links
- 229920001515 polyalkylene glycol Polymers 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 239000003999 initiator Substances 0.000 abstract 3
- 150000001298 alcohols Chemical class 0.000 abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- -1 preferably R-H Chemical group 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
- C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2648—Alkali metals or compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2651—Alkaline earth metals or compounds thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCESSO PARA A PRODUÇçO DE ALFA- ALCàXI-âMEGA-HIDRàXI-POLIALQUILENOGLICàIS PUROS. A presente invenção refere-se a um processo para a produção de <244>-alcóxi-<87>-hidróxi-polialquilenoglicóis, que leva a pequenas impurezas do produto <244>-<87>-dihidróxi-polialquilenoglicóis de peso molecular elevado. O processo baseia-se no emprego de álcoois iniciadores com ponto de ebulição elevado da seguinte estrutura geral R~ 2~-(OCH~ 2~CHR)~ k~ OH, na qual R~ 2~ representa um radical alquila com (1) até (4) átomos de carbono, preferentemente R~ 2~ = CH~ 3~, k representa um número de (1) até (10), preferentemente (1) até (4) e R H, CH~ 3~ ou um radical alquila com (2) até (4) átomos de carbono, preferentemente R = H, CH~ 3~. Através da utilização dos álcoois iniciadores mencionados, é possível secar a mistura de catalisador básico e álcool iniciador para teores de água muito baixos e com isso, produzir concentrações muito baixas de impurezas de <244>-<87>-dihidróxi-polialquilenoglicol incômodas.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102004059489A DE102004059489C5 (de) | 2004-12-10 | 2004-12-10 | Verfahren zur Herstellung von reinen alpha-Alkoxy-omega-hydroxy-Polyalkylenglykolen |
PCT/EP2005/012622 WO2006061110A1 (de) | 2004-12-10 | 2005-11-25 | Verfahren zur herstellung von reinen alpha-alkoxy-omega-hydroxy-polyalkylenglykolen |
Publications (2)
Publication Number | Publication Date |
---|---|
BRPI0518767A2 true BRPI0518767A2 (pt) | 2008-12-09 |
BRPI0518767B1 BRPI0518767B1 (pt) | 2016-09-13 |
Family
ID=36086038
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0518767A BRPI0518767B1 (pt) | 2004-12-10 | 2005-11-25 | processo para a produção de alfa-alcóxi-ômega-hidróxi-polialquilenoglicóis puros |
Country Status (10)
Country | Link |
---|---|
US (1) | US7435857B2 (pt) |
EP (1) | EP1824901B2 (pt) |
JP (1) | JP5081625B2 (pt) |
AT (1) | ATE413425T1 (pt) |
BR (1) | BRPI0518767B1 (pt) |
DE (2) | DE102004059489C5 (pt) |
ES (1) | ES2314735T5 (pt) |
MX (1) | MX2007006875A (pt) |
PT (1) | PT1824901E (pt) |
WO (1) | WO2006061110A1 (pt) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102006037079A1 (de) * | 2006-08-07 | 2008-02-14 | Evonik Degussa Gmbh | Ruß, Verfahren zur Herstellung von Ruß und Vorrichtung zur Durchführung des Verfahrens |
DE102007026551A1 (de) * | 2007-06-08 | 2008-12-11 | Evonik Degussa Gmbh | Pigmentpräparation, Verfahren zu deren Herstellung und Verwendung |
DE102007060307A1 (de) | 2007-12-12 | 2009-06-18 | Evonik Degussa Gmbh | Verfahren zur Nachbehandlung von Ruß |
CN101925630A (zh) * | 2008-02-01 | 2010-12-22 | 陶氏环球技术公司 | 低二醇含量的单官能烷氧基聚亚烷基二醇及其制备方法 |
DE102008026894A1 (de) * | 2008-06-05 | 2009-12-10 | Evonik Degussa Gmbh | Ink Jet Tinte |
DE102008044116A1 (de) | 2008-11-27 | 2010-06-02 | Evonik Degussa Gmbh | Pigmentgranulat, Verfahren zu dessen Herstellung und Verwendung |
ATE516330T1 (de) * | 2008-12-12 | 2011-07-15 | Evonik Carbon Black Gmbh | Ink jet tinte |
ES2379571T3 (es) | 2009-06-18 | 2012-04-27 | Basf Se | Procedimiento para la obtención de óxidos de monohidroxipolialquileno |
DE102010002244A1 (de) | 2010-02-23 | 2011-08-25 | Evonik Carbon Black GmbH, 63457 | Ruß, Verfahren zu seiner Herstellung und seine Verwendung |
JP6106104B2 (ja) * | 2014-01-16 | 2017-03-29 | 信越化学工業株式会社 | 末端にアミノ基を有する狭分散ポリアルキレングリコール誘導体の製造方法 |
WO2019035090A1 (en) * | 2017-08-17 | 2019-02-21 | Sabic Global Technologies B.V. | PROCESS FOR THE PREPARATION OF A POLYOXYETHYLENE FATTY ACID MONOESTER, ESTER THEREOF, AND CORRESPONDING USES THEREOF |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3121929C1 (de) | 1981-06-03 | 1983-02-24 | Th. Goldschmidt Ag, 4300 Essen | Verfahren zur Herstellung von Polyoxyalkylenmonoallyl- oder -methallylethern |
JPS60199031A (ja) * | 1984-03-23 | 1985-10-08 | Asahi Glass Co Ltd | ポリエ−テル類の製法 |
CA2101361A1 (en) | 1992-08-27 | 1994-02-28 | Robert A. Snow | Low diol polyalkylene oxide biologically active proteinaceous substances |
JPH06248070A (ja) * | 1993-03-01 | 1994-09-06 | Kao Corp | 加熱着色しにくいポリオキシアルキレン付加物の製造法 |
JPH08109254A (ja) * | 1994-10-11 | 1996-04-30 | Dai Ichi Kogyo Seiyaku Co Ltd | ポリエーテルの製造方法 |
US6166112A (en) | 1997-03-10 | 2000-12-26 | Nippon Shokubai Co., Ltd. | Cement admixture and cement composition |
JP3285820B2 (ja) * | 1997-06-10 | 2002-05-27 | 株式会社日本触媒 | ポリカルボン酸の製造方法 |
JP4385440B2 (ja) * | 1999-06-08 | 2009-12-16 | 日油株式会社 | 重合性ポリオキシアルキレンモノアルキルエーテル誘導体、該誘導体の重合体及び該重合体を含有する分散剤 |
JP3296332B2 (ja) * | 1998-06-17 | 2002-06-24 | 日本油脂株式会社 | ポリオキシアルキレンモノアルキルエーテル、その製造方法、重合性ポリオキシアルキレンモノアルキルエーテル誘導体、該誘導体の共重合体及び該共重合体を含有する分散剤 |
WO2000012576A1 (fr) | 1998-08-27 | 2000-03-09 | Kao Corporation | Procede de production de polymere d'acide (meth)acrylique |
JP2001220440A (ja) * | 2000-02-10 | 2001-08-14 | Kao Corp | ポリアルキレングリコールエーテルの製造方法 |
EP1295902A1 (en) | 2001-09-20 | 2003-03-26 | Shell Internationale Researchmaatschappij B.V. | Process for preparing polyoxyalkylene polyether products. |
US7199193B2 (en) † | 2004-09-28 | 2007-04-03 | Dow Global Technologies, Inc. | Polyethylene glycol compounds and process of making |
-
2004
- 2004-12-10 DE DE102004059489A patent/DE102004059489C5/de not_active Expired - Fee Related
-
2005
- 2005-11-25 ES ES05811995T patent/ES2314735T5/es active Active
- 2005-11-25 DE DE502005005918T patent/DE502005005918D1/de active Active
- 2005-11-25 WO PCT/EP2005/012622 patent/WO2006061110A1/de active Application Filing
- 2005-11-25 EP EP05811995.9A patent/EP1824901B2/de active Active
- 2005-11-25 PT PT05811995T patent/PT1824901E/pt unknown
- 2005-11-25 MX MX2007006875A patent/MX2007006875A/es active IP Right Grant
- 2005-11-25 BR BRPI0518767A patent/BRPI0518767B1/pt not_active IP Right Cessation
- 2005-11-25 US US11/792,768 patent/US7435857B2/en active Active
- 2005-11-25 AT AT05811995T patent/ATE413425T1/de not_active IP Right Cessation
- 2005-11-25 JP JP2007544768A patent/JP5081625B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
DE102004059489C5 (de) | 2011-12-08 |
PT1824901E (pt) | 2008-12-31 |
DE102004059489A1 (de) | 2006-06-22 |
US7435857B2 (en) | 2008-10-14 |
ES2314735T5 (es) | 2013-10-09 |
DE102004059489B4 (de) | 2008-08-14 |
JP5081625B2 (ja) | 2012-11-28 |
JP2008523178A (ja) | 2008-07-03 |
MX2007006875A (es) | 2007-06-22 |
US20080076947A1 (en) | 2008-03-27 |
BRPI0518767B1 (pt) | 2016-09-13 |
EP1824901A1 (de) | 2007-08-29 |
ES2314735T3 (es) | 2009-03-16 |
DE502005005918D1 (de) | 2008-12-18 |
ATE413425T1 (de) | 2008-11-15 |
EP1824901B2 (de) | 2013-08-07 |
EP1824901B1 (de) | 2008-11-05 |
WO2006061110A1 (de) | 2006-06-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 13/09/2016, OBSERVADAS AS CONDICOES LEGAIS. |
|
B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 18A ANUIDADE. |
|
B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2750 DE 19-09-2023 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |