BR0207803A - processo para recuperação e purificação de caprolactama a partir de um solvente orgánico - Google Patents
processo para recuperação e purificação de caprolactama a partir de um solvente orgánicoInfo
- Publication number
- BR0207803A BR0207803A BRPI0207803-1A BR0207803A BR0207803A BR 0207803 A BR0207803 A BR 0207803A BR 0207803 A BR0207803 A BR 0207803A BR 0207803 A BR0207803 A BR 0207803A
- Authority
- BR
- Brazil
- Prior art keywords
- caprolactam
- organic solvent
- solution
- product
- purification
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Processing Of Solid Wastes (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
- Pyrrole Compounds (AREA)
Abstract
"PROCESSO PARA RECUPERAçãO E PURIFICAçãO DE CAPROLACTAMA A PARTIR DE UM SOLVENTE ORGáNICO". A invenção refere-se a um processo para recuperação de caprolactama a partir de uma solução que compreende caprolactama dissolvida em um solvente orgânico, processo este que compreende: a) lavar a solução com água ou uma solução aquosa alcalina, resultando em uma solução lavada que compreende caprolactama e solvente orgânico e em um resíduo de lavagem, b) evaporar solvente orgânico da solução lavada, resultando em produto de caprolactama, c) opcionalmente, hidrogenar o produto de caprolactama, d) opcionalmente, evaporar a água do produto de caprolactama, e) destilar o produto de caprolactama para recuperar caprolactama e um resíduo de destilação, f) extrair o resíduo de destilação com um solvente orgânico na presença de água para obter (i) um extrato que compreende caprolactama dissolvido em solvente orgânico e (ii) um efluente aquoso, e g) reciclar o extrato para a etapa a) ou b).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL1017471 | 2001-03-01 | ||
PCT/NL2002/000125 WO2002070475A1 (en) | 2001-03-01 | 2002-02-27 | Process for recovering and purifying caprolactam from an organic solvent |
Publications (1)
Publication Number | Publication Date |
---|---|
BR0207803A true BR0207803A (pt) | 2006-05-23 |
Family
ID=19772980
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0207803-1A BR0207803A (pt) | 2001-03-01 | 2002-02-27 | processo para recuperação e purificação de caprolactama a partir de um solvente orgánico |
Country Status (17)
Country | Link |
---|---|
US (1) | US6849731B2 (pt) |
EP (1) | EP1373201B1 (pt) |
JP (1) | JP4465151B2 (pt) |
KR (1) | KR100841157B1 (pt) |
CN (1) | CN1262539C (pt) |
AT (1) | ATE498610T1 (pt) |
BR (1) | BR0207803A (pt) |
CZ (1) | CZ20032357A3 (pt) |
DE (1) | DE60239191D1 (pt) |
EA (1) | EA006504B1 (pt) |
ES (1) | ES2359791T3 (pt) |
MX (1) | MXPA03007835A (pt) |
MY (1) | MY124831A (pt) |
PL (1) | PL206266B1 (pt) |
RO (1) | RO121266B1 (pt) |
TW (1) | TW574213B (pt) |
WO (1) | WO2002070475A1 (pt) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4351908B2 (ja) † | 2001-08-27 | 2009-10-28 | ディーエスエム アイピー アセッツ ビー.ブイ. | 減圧においてアルカリ性のカプロラクタム生成物を蒸留する方法 |
CN100384818C (zh) * | 2005-12-27 | 2008-04-30 | 湘潭大学 | 高纯度己内酰胺的精制方法 |
CN101613311B (zh) * | 2008-06-25 | 2013-01-02 | 中国石油化学工业开发股份有限公司 | 从重排混合物中回收己内酰胺的系统和方法 |
EP2326620A1 (en) * | 2008-09-04 | 2011-06-01 | DSM IP Assets B.V. | Washing of an organic phase comprising caprolactam |
IN2012DN05159A (pt) | 2009-12-18 | 2015-10-23 | Dsm Ip Assets Bv | |
RU2522540C1 (ru) * | 2012-11-08 | 2014-07-20 | Закрытое акционерное общество "МЕТАКЛЭЙ" (ЗАО "МЕТАКЛЭЙ") | Способ получения катализатора полимеризации эпсилон-капролактама |
PL2935210T3 (pl) * | 2012-12-19 | 2017-05-31 | Basf Se | Sposób wytwarzania oczyszczonego kaprolaktamu z przegrupowania beckmanna oksymu cykloheksanonu |
US8841445B2 (en) * | 2012-12-19 | 2014-09-23 | Basf Se | Process for preparing purified caprolactam from the Beckmann rearrangement of cyclohexane oxime |
CN103896841B (zh) * | 2012-12-28 | 2018-11-09 | Cap Iii 有限公司 | 从有机溶剂中回收和提纯ε-己内酰胺的方法 |
CN104072419B (zh) * | 2013-10-28 | 2016-11-02 | 中国石油化工股份有限公司 | 一种己内酰胺的纯化方法和纯化装置 |
TWI520944B (zh) * | 2015-02-13 | 2016-02-11 | 中國石油化學工業開發股份有限公司 | 己內醯胺之製造方法及其系統 |
CN106554309A (zh) * | 2015-09-24 | 2017-04-05 | 中国石油化工股份有限公司 | 一种深度脱除苯-己溶液中残余盐类杂质的方法 |
CN107556240B (zh) * | 2016-08-24 | 2020-10-30 | 沧州旭阳化工有限公司 | 一种己内酰胺精制方法及精制己内酰胺的系统 |
CN107118156B (zh) * | 2017-06-26 | 2020-08-28 | 山东清创化工有限公司 | 一种己内酰胺分离精制工艺 |
EP3568389B1 (en) * | 2017-12-15 | 2021-01-20 | Aquafilslo D.O.O. | Process for the purification of caprolactam from a solution of crude caprolactam without organic solvent extraction |
CN109942492A (zh) * | 2019-04-11 | 2019-06-28 | 江苏凌瑞化工科技有限公司 | 一种己内酰胺精制工艺 |
EP3862321A1 (en) | 2020-02-07 | 2021-08-11 | Cap Iii B.V. | Ammonium sulphate production on industrial scale |
CN111686477B (zh) * | 2020-06-30 | 2022-07-29 | 聊城鲁西聚酰胺新材料科技有限公司 | 一种己内酰胺萃取液洗涤塔、系统及工艺 |
CN114452924B (zh) * | 2022-01-19 | 2024-06-04 | 福建省力恒锦纶实业有限公司 | 一种提高回收己内酰胺品质、改进回收工艺的系统及方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2758991A (en) * | 1956-08-14 | Hvvevvtofry | ||
US3761467A (en) * | 1971-02-11 | 1973-09-25 | Allied Chem | Recovery of epsilon-caprolactam |
DE3700247A1 (de) * | 1987-01-07 | 1988-07-21 | Basf Ag | Verfahren zur entfernung von nicht mit wasser mischbaren loesungsmitteln aus solche enthaltenden abgasen |
BE1011047A3 (nl) * | 1997-03-17 | 1999-04-06 | Dsm Nv | Werkwijze voor het zuiveren van caprolactam. |
NL1005927C2 (nl) * | 1997-04-29 | 1998-11-02 | Dsm Nv | Werkwijze voor het winnen van caprolactam uit een geneutraliseerd omlegmengsel. |
-
2002
- 2002-02-27 WO PCT/NL2002/000125 patent/WO2002070475A1/en active Application Filing
- 2002-02-27 JP JP2002569795A patent/JP4465151B2/ja not_active Expired - Fee Related
- 2002-02-27 EP EP02712538A patent/EP1373201B1/en not_active Expired - Lifetime
- 2002-02-27 CN CNB028057848A patent/CN1262539C/zh not_active Expired - Fee Related
- 2002-02-27 EA EA200300957A patent/EA006504B1/ru not_active IP Right Cessation
- 2002-02-27 PL PL364226A patent/PL206266B1/pl unknown
- 2002-02-27 DE DE60239191T patent/DE60239191D1/de not_active Expired - Lifetime
- 2002-02-27 US US10/468,263 patent/US6849731B2/en not_active Expired - Fee Related
- 2002-02-27 RO ROA200300700A patent/RO121266B1/ro unknown
- 2002-02-27 MX MXPA03007835A patent/MXPA03007835A/es active IP Right Grant
- 2002-02-27 BR BRPI0207803-1A patent/BR0207803A/pt not_active Application Discontinuation
- 2002-02-27 CZ CZ20032357A patent/CZ20032357A3/cs unknown
- 2002-02-27 KR KR1020037011191A patent/KR100841157B1/ko not_active IP Right Cessation
- 2002-02-27 AT AT02712538T patent/ATE498610T1/de not_active IP Right Cessation
- 2002-02-27 ES ES02712538T patent/ES2359791T3/es not_active Expired - Lifetime
- 2002-02-28 MY MYPI20020714A patent/MY124831A/en unknown
- 2002-03-01 TW TW91103848A patent/TW574213B/zh not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
PL364226A1 (en) | 2004-12-13 |
CZ20032357A3 (cs) | 2004-02-18 |
DE60239191D1 (de) | 2011-03-31 |
MY124831A (en) | 2006-07-31 |
KR20030089699A (ko) | 2003-11-22 |
EP1373201B1 (en) | 2011-02-16 |
KR100841157B1 (ko) | 2008-06-24 |
TW574213B (en) | 2004-02-01 |
MXPA03007835A (es) | 2004-11-12 |
CN1262539C (zh) | 2006-07-05 |
EA200300957A1 (ru) | 2004-02-26 |
EA006504B1 (ru) | 2005-12-29 |
ATE498610T1 (de) | 2011-03-15 |
JP2004521923A (ja) | 2004-07-22 |
CN1535263A (zh) | 2004-10-06 |
US20040110943A1 (en) | 2004-06-10 |
RO121266B1 (ro) | 2007-02-28 |
US6849731B2 (en) | 2005-02-01 |
EP1373201A1 (en) | 2004-01-02 |
ES2359791T3 (es) | 2011-05-26 |
WO2002070475A1 (en) | 2002-09-12 |
PL206266B1 (pl) | 2010-07-30 |
JP4465151B2 (ja) | 2010-05-19 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL. |