BR0009000A - Reator multitubular e aplicação do mesmo - Google Patents
Reator multitubular e aplicação do mesmoInfo
- Publication number
- BR0009000A BR0009000A BR0009000-0A BR0009000A BR0009000A BR 0009000 A BR0009000 A BR 0009000A BR 0009000 A BR0009000 A BR 0009000A BR 0009000 A BR0009000 A BR 0009000A
- Authority
- BR
- Brazil
- Prior art keywords
- tube
- diameter
- reactor
- application
- gas phase
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
- C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
- C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
- C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/2425—Tubular reactors in parallel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
- B01J8/067—Heating or cooling the reactor
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
- C07C45/37—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups
- C07C45/38—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups being a primary hydroxyl group
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00212—Plates; Jackets; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00212—Plates; Jackets; Cylinders
- B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Catalysts (AREA)
Abstract
"REATOR MULTITUBULAR E APLICAçãO DO MESMO". A invenção trata de um reator multitubular a leito fixo e da aplicação de um reator deste tipo para a condução de reações catalíticas em fase gasosa, especialmente para a realização de reações de fase gasosa catalítica exotérmicas ou endotérmicas tal como produzindo anidrido ftálico (PSA),ácido acrílico (AA), ácido metacrílico (MAA), acroleina, anidrido maleico (MAS), glioxal, fosgênio, ácido cianídrico ou formamida de vinila (VFA). De acordo com a invenção, no caso de reatores de maior porte onde um considerável calor de reação é produzido ou requerido e tem de ser dissipado como um resultado dos numerosos tubos de reação (17), a relação de distribuição de tubos t para o diâmetro externo do tubo d~ a~, é tornada dependente do diâmetro do reator ou do diâmetro do feixe de tubos d~ Rba~. Se o diâmetro externo do feixe de tubos de reação (18) é de mais de 4 metros, uma relação de distribuição de tubos t para o diâmetro externo do tubo d~ a~, de pelo menos 1.3 tem preferência.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19912735 | 1999-03-16 | ||
DE19956329 | 1999-11-23 | ||
PCT/EP2000/002304 WO2000054877A2 (de) | 1999-03-16 | 2000-03-15 | Rohrbündelreaktor, insbesondere für katalytische gasphasenreaktionen |
Publications (2)
Publication Number | Publication Date |
---|---|
BR0009000A true BR0009000A (pt) | 2002-01-02 |
BR0009000B1 BR0009000B1 (pt) | 2011-01-25 |
Family
ID=26052502
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0009000-0A BR0009000B1 (pt) | 1999-03-16 | 2000-03-15 | reator multitubular e aplicação do mesmo. |
Country Status (14)
Country | Link |
---|---|
US (1) | US7226567B1 (pt) |
EP (1) | EP1169119B1 (pt) |
JP (1) | JP5204356B2 (pt) |
KR (1) | KR100648579B1 (pt) |
CN (1) | CN1231291C (pt) |
AT (1) | ATE251944T1 (pt) |
AU (1) | AU4538700A (pt) |
BR (1) | BR0009000B1 (pt) |
DE (1) | DE50004079D1 (pt) |
ES (1) | ES2209870T3 (pt) |
MX (1) | MX220474B (pt) |
MY (1) | MY125244A (pt) |
TW (1) | TW527218B (pt) |
WO (1) | WO2000054877A2 (pt) |
Families Citing this family (44)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4648515B2 (ja) * | 2000-05-02 | 2011-03-09 | 株式会社日本触媒 | 反応器のスタートアップ方法 |
AU2002360970A1 (en) * | 2002-12-12 | 2004-06-30 | Man Dwe Gmbh | Shell-and-tube type reactor for catalytic gas phase reactions |
DE10258153A1 (de) * | 2002-12-12 | 2004-06-24 | Basf Ag | Verfahren zur Herstellung von Chlor durch Gasphasenoxidation von Chlorwasserstoff |
WO2005005037A1 (ja) * | 2003-07-14 | 2005-01-20 | Mitsubishi Rayon Co., Ltd. | 固定床多管式反応器 |
WO2005113123A1 (de) * | 2004-05-07 | 2005-12-01 | Basf Aktiengesellschaft | Verfahren zur strukturierten befüllung von kontaktrohren eines kontaktrohrbündels |
WO2006094766A1 (de) * | 2005-03-08 | 2006-09-14 | Basf Aktiengesellschaft | Verfahren zum befüllen eines reaktors |
DE102005010645A1 (de) * | 2005-03-08 | 2005-08-04 | Basf Ag | Verfahren zum Befüllen eines Reaktors |
CN100393404C (zh) * | 2005-04-28 | 2008-06-11 | 浙江工业大学 | 一种适用于强放热反应的固定床反应器 |
WO2007132011A1 (de) * | 2006-05-17 | 2007-11-22 | Basf Aktiengesellschaft | Verfahren zur herstellung vicinaler dioxoverbindungen durch oxidation vicinaler dihydroxyverbindungen an einer strukturierten katalysatorschüttung |
DE102006034811A1 (de) * | 2006-07-27 | 2008-01-31 | Man Dwe Gmbh | Verfahren zur Temperaturänderung eines Rohrbündelreaktors |
EP2349961B1 (en) * | 2008-10-13 | 2016-11-23 | Blue Cube IP LLC | Process for the production of chlorinated and/or fluorinated propenes |
EP2382175B1 (de) | 2008-12-29 | 2015-02-25 | Basf Se | Verfahren zur reinigung wässriger glyoxal-lösungen |
DE102009001021A1 (de) * | 2009-02-19 | 2010-08-26 | Wacker Chemie Ag | Verfahren und Vorrichtung zur Herstellung von Vinylacetat |
CN102596387B (zh) | 2009-10-09 | 2015-11-25 | 陶氏环球技术有限责任公司 | 生产氯化和/或氟化丙烯和高级烯烃的等温多管反应器和方法 |
US8581012B2 (en) * | 2009-10-09 | 2013-11-12 | Dow Global Technologies, Llc | Processes for the production of chlorinated and/or fluorinated propenes and higher alkenes |
BR112012007913A2 (pt) * | 2009-10-09 | 2019-09-24 | Dow Global Technologies Llc | reator adiabático de fluxo pistonado, processo para produzir um prpeno clorado ou fluorado, processo para preparar um produto a jusante e processo para preparar 2,3,3,3-tetrafluoroprop-1-eno (hfo-123yf) ou 1,3,3,3-tetrafluoroprop-1-eno (hfo-123ze) |
EP2485996B1 (en) * | 2009-10-09 | 2016-06-15 | Blue Cube IP LLC | Process for the production of chlorinated and/or fluorinated propenes |
EP2621878B1 (de) | 2010-10-01 | 2016-06-01 | Basf Se | Verfahren zur reinigung wässriger glyoxal-lösungen |
US8461396B2 (en) | 2010-10-01 | 2013-06-11 | Basf Se | Process for purifying aqueous glyoxal solutions |
CA2836493A1 (en) | 2011-05-31 | 2012-12-06 | Max Markus Tirtowidjojo | Process for the production of chlorinated propenes |
EP2714631B1 (en) | 2011-05-31 | 2020-05-13 | Blue Cube IP LLC | Process for the production of chlorinated propenes |
WO2012170239A1 (en) | 2011-06-08 | 2012-12-13 | Dow Agrosciences, Llc | Process for the production of chlorinated and/or fluorinated propenes |
JP6420145B2 (ja) | 2011-08-07 | 2018-11-07 | ブルー キューブ アイピー エルエルシー | 塩素化プロペンの製造方法 |
CN103717557A (zh) | 2011-08-07 | 2014-04-09 | 陶氏环球技术有限责任公司 | 生产氯化的丙烯的方法 |
CN104039744B (zh) | 2011-11-21 | 2016-04-20 | 陶氏环球技术有限责任公司 | 制备氯化烷烃的方法 |
EP2785670B1 (en) | 2011-12-02 | 2017-10-25 | Blue Cube IP LLC | Process for the production of chlorinated alkanes |
JP6050375B2 (ja) | 2011-12-02 | 2016-12-21 | ブルー キューブ アイピー エルエルシー | クロロアルカンの製造方法 |
JP6170068B2 (ja) | 2011-12-13 | 2017-07-26 | ブルー キューブ アイピー エルエルシー | 塩素化プロパン及びプロペンの製造方法 |
JP2015503523A (ja) | 2011-12-22 | 2015-02-02 | ダウ グローバル テクノロジーズ エルエルシー | テトラクロロメタンの製造方法 |
US9512049B2 (en) | 2011-12-23 | 2016-12-06 | Dow Global Technologies Llc | Process for the production of alkenes and/or aromatic compounds |
CN102744018B (zh) * | 2012-06-25 | 2014-08-27 | 华东理工大学 | 一种可调节进口物料温度的固定床催化反应装置 |
CA2884435A1 (en) | 2012-09-20 | 2014-03-27 | Dow Global Technologies Llc | Process for the production of chlorinated propenes |
US9321707B2 (en) | 2012-09-20 | 2016-04-26 | Blue Cube Ip Llc | Process for the production of chlorinated propenes |
US9440903B2 (en) | 2012-09-24 | 2016-09-13 | Arkema Inc. | Shell and tube oxidation reactor with improved resistance to fouling |
CA2885329A1 (en) | 2012-09-30 | 2014-03-04 | Dow Global Technologies Llc | Weir quench and processes incorporating the same |
EP2911773B1 (en) | 2012-10-26 | 2017-10-04 | Blue Cube IP LLC | Mixer and reactor and process incorporating the same |
EP2935165A1 (en) | 2012-12-18 | 2015-10-28 | Blue Cube IP LLC | Process for the production of chlorinated propenes |
CA2894168C (en) | 2012-12-19 | 2018-04-24 | Dow Global Technologies Llc | Process for the production of chlorinated propenes |
CN104981449B (zh) | 2013-02-27 | 2016-12-28 | 蓝立方知识产权有限责任公司 | 用于生产氯化丙烯的方法 |
CN105026348A (zh) | 2013-03-09 | 2015-11-04 | 蓝立方知识产权有限责任公司 | 用于生产氯化烷烃的方法 |
DE102014226928A1 (de) * | 2014-12-23 | 2016-06-23 | Siemens Aktiengesellschaft | Dampfkraftwerksystem mit Katalysatoranordnung |
JP6630721B2 (ja) * | 2015-03-23 | 2020-01-15 | 千代田化工建設株式会社 | 合成ガスの製造方法および製造装置 |
CN105381778A (zh) * | 2015-12-18 | 2016-03-09 | 张家港市江南锅炉压力容器有限公司 | 反应釜 |
DK201700031A1 (en) * | 2016-09-27 | 2017-11-13 | Haldor Topsoe As | Short Gasket Reactor |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CH493811A (de) * | 1967-09-06 | 1970-07-15 | Basf Ag | Wärmetauschvorrichtung |
DE2330765A1 (de) | 1973-06-16 | 1975-01-09 | Grundig Emv | Beleuchtungseinrichtung fuer skalenzeiger |
US3910768A (en) * | 1973-11-06 | 1975-10-07 | Stone & Webster Eng Corp | High pressure cracking furnace and system |
AU529228B2 (en) * | 1977-07-13 | 1983-06-02 | Nippon Shokubai Kagaku Kogyo Co. Ltd. | Catalytic vapour phase oxidation |
FR2452315B1 (fr) * | 1979-03-28 | 1985-07-05 | Azote & Prod Chim | Reacteur de nitration d'hydrocarbures en phase gazeuse sous pression |
US4398595A (en) | 1979-11-29 | 1983-08-16 | Phillips Petroleum Company | Vortex generators |
GB8721964D0 (en) * | 1987-09-18 | 1987-10-28 | Shell Int Research | Multitube reactor |
US5227556A (en) * | 1990-04-17 | 1993-07-13 | The Dow Chemical Company | Turbulent flow process, monoalkyl aromatic production process and reactor for such process |
EP0512911B1 (fr) * | 1991-05-06 | 1995-08-09 | Institut Français du Pétrole | Procédé et dispositif de déshydrogénation d'hydrocarbures aliphatiques en hydrocarbures oléfiniques |
DE4431957A1 (de) * | 1994-09-08 | 1995-03-16 | Basf Ag | Verfahren zur katalytischen Gasphasenoxidation von Propen zu Acrolein |
US5730843A (en) * | 1995-12-29 | 1998-03-24 | Chemical Research & Licensing Company | Catalytic distillation structure |
EP0959120B1 (en) * | 1996-10-03 | 2006-08-02 | Hajime Kato | Method for hydrocarbon steam reforming |
US5723094A (en) * | 1996-10-29 | 1998-03-03 | Arco Chemical Technology, L.P. | Reactor for chemical reactions |
US6296814B1 (en) * | 1998-11-10 | 2001-10-02 | International Fuel Cells, L.L.C. | Hydrocarbon fuel gas reformer assembly for a fuel cell power plant |
-
2000
- 2000-03-09 TW TW089104252A patent/TW527218B/zh not_active IP Right Cessation
- 2000-03-14 MY MYPI20001007A patent/MY125244A/en unknown
- 2000-03-15 ES ES00926738T patent/ES2209870T3/es not_active Expired - Lifetime
- 2000-03-15 JP JP2000604943A patent/JP5204356B2/ja not_active Expired - Lifetime
- 2000-03-15 CN CNB008050376A patent/CN1231291C/zh not_active Expired - Lifetime
- 2000-03-15 KR KR1020017011640A patent/KR100648579B1/ko active IP Right Grant
- 2000-03-15 DE DE50004079T patent/DE50004079D1/de not_active Expired - Lifetime
- 2000-03-15 AU AU45387/00A patent/AU4538700A/en not_active Abandoned
- 2000-03-15 BR BRPI0009000-0A patent/BR0009000B1/pt not_active IP Right Cessation
- 2000-03-15 AT AT00926738T patent/ATE251944T1/de not_active IP Right Cessation
- 2000-03-15 US US09/936,354 patent/US7226567B1/en not_active Expired - Lifetime
- 2000-03-15 WO PCT/EP2000/002304 patent/WO2000054877A2/de active IP Right Grant
- 2000-03-15 EP EP00926738A patent/EP1169119B1/de not_active Expired - Lifetime
-
2001
- 2001-09-06 MX MXPA01009012 patent/MX220474B/es unknown
Also Published As
Publication number | Publication date |
---|---|
AU4538700A (en) | 2000-10-04 |
MXPA01009012A (es) | 2002-01-01 |
JP2002538951A (ja) | 2002-11-19 |
WO2000054877A2 (de) | 2000-09-21 |
US7226567B1 (en) | 2007-06-05 |
CN1231291C (zh) | 2005-12-14 |
JP5204356B2 (ja) | 2013-06-05 |
KR20020004965A (ko) | 2002-01-16 |
EP1169119B1 (de) | 2003-10-15 |
CN1343137A (zh) | 2002-04-03 |
DE50004079D1 (de) | 2003-11-20 |
EP1169119A2 (de) | 2002-01-09 |
KR100648579B1 (ko) | 2006-11-24 |
TW527218B (en) | 2003-04-11 |
MY125244A (en) | 2006-07-31 |
MX220474B (en) | 2004-05-20 |
BR0009000B1 (pt) | 2011-01-25 |
WO2000054877A3 (de) | 2001-04-05 |
ATE251944T1 (de) | 2003-11-15 |
ES2209870T3 (es) | 2004-07-01 |
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