MX220474B - Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions - Google Patents

Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions

Info

Publication number
MX220474B
MX220474B MXPA01009012A MX220474B MX 220474 B MX220474 B MX 220474B MX PA01009012 A MXPA01009012 A MX PA01009012A MX 220474 B MX220474 B MX 220474B
Authority
MX
Mexico
Prior art keywords
sub
diameter
reactor
catalytic gas
phase reactions
Prior art date
Application number
Other languages
English (en)
Inventor
Gerhard Olbert
Franz Corr
Peter Reuter
Ludwig Wambach
Ulrich Hammon
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of MXPA01009012A publication Critical patent/MXPA01009012A/es
Publication of MX220474B publication Critical patent/MX220474B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/2425—Tubular reactors in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/37—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups
    • C07C45/38—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups being a primary hydroxyl group
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Catalysts (AREA)
MXPA01009012 1999-03-16 2001-09-06 Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions MX220474B (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19912735 1999-03-16
DE19956329 1999-11-23

Publications (2)

Publication Number Publication Date
MXPA01009012A MXPA01009012A (es) 2002-01-01
MX220474B true MX220474B (en) 2004-05-20

Family

ID=26052502

Family Applications (1)

Application Number Title Priority Date Filing Date
MXPA01009012 MX220474B (en) 1999-03-16 2001-09-06 Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions

Country Status (14)

Country Link
US (1) US7226567B1 (es)
EP (1) EP1169119B1 (es)
JP (1) JP5204356B2 (es)
KR (1) KR100648579B1 (es)
CN (1) CN1231291C (es)
AT (1) ATE251944T1 (es)
AU (1) AU4538700A (es)
BR (1) BR0009000B1 (es)
DE (1) DE50004079D1 (es)
ES (1) ES2209870T3 (es)
MX (1) MX220474B (es)
MY (1) MY125244A (es)
TW (1) TW527218B (es)
WO (1) WO2000054877A2 (es)

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AU2002360970A1 (en) * 2002-12-12 2004-06-30 Man Dwe Gmbh Shell-and-tube type reactor for catalytic gas phase reactions
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CN100377773C (zh) * 2003-07-14 2008-04-02 三菱丽阳株式会社 固定床多管式反应器
EP1748839B1 (de) * 2004-05-07 2020-04-01 Basf Se Verfahren zur strukturierten befüllung von kontaktrohren eines kontaktrohrbündels
SG160371A1 (en) * 2005-03-08 2010-04-29 Basf Ag Method for filling a reactor
DE102005010645A1 (de) * 2005-03-08 2005-08-04 Basf Ag Verfahren zum Befüllen eines Reaktors
CN100393404C (zh) * 2005-04-28 2008-06-11 浙江工业大学 一种适用于强放热反应的固定床反应器
WO2007132011A1 (de) * 2006-05-17 2007-11-22 Basf Aktiengesellschaft Verfahren zur herstellung vicinaler dioxoverbindungen durch oxidation vicinaler dihydroxyverbindungen an einer strukturierten katalysatorschüttung
DE102006034811A1 (de) 2006-07-27 2008-01-31 Man Dwe Gmbh Verfahren zur Temperaturänderung eines Rohrbündelreaktors
JP6022770B2 (ja) * 2008-10-13 2016-11-09 ブルー キューブ アイピー エルエルシー 塩素化及び／又はフッ素化プロペンの製造方法
CN102272084A (zh) 2008-12-29 2011-12-07 巴斯夫欧洲公司 提纯乙二醛水溶液的方法
DE102009001021A1 (de) * 2009-02-19 2010-08-26 Wacker Chemie Ag Verfahren und Vorrichtung zur Herstellung von Vinylacetat
KR20120093857A (ko) * 2009-10-09 2012-08-23 다우 글로벌 테크놀로지스 엘엘씨 염화 및/또는 불화 프로펜의 제조 방법
CN105664811B (zh) * 2009-10-09 2018-10-09 蓝立方知识产权公司 生产氯化和/或氟化丙烯和高级烯烃的绝热活塞流反应器及方法
WO2011044536A1 (en) * 2009-10-09 2011-04-14 Dow Global Technologies, Inc Process for the production of chlorinated and/or fluorinated propenes and higher alkenes
CN102596387B (zh) 2009-10-09 2015-11-25 陶氏环球技术有限责任公司 生产氯化和/或氟化丙烯和高级烯烃的等温多管反应器和方法
US8461396B2 (en) 2010-10-01 2013-06-11 Basf Se Process for purifying aqueous glyoxal solutions
EP2621878B1 (de) 2010-10-01 2016-06-01 Basf Se Verfahren zur reinigung wässriger glyoxal-lösungen
WO2012166393A1 (en) 2011-05-31 2012-12-06 Dow Global Technologies, Llc Process for the production of chlorinated propenes
WO2012166394A1 (en) 2011-05-31 2012-12-06 Dow Global Technologies, Llc Process for the production of chlorinated propenes
ES2721451T3 (es) 2011-06-08 2019-07-31 Dow Agrosciences Llc Procedimiento para la producción de propenos clorados y/o fluorados
CN103717559A (zh) 2011-08-07 2014-04-09 陶氏环球技术有限责任公司 生产氯化的丙烯的方法
JP6166261B2 (ja) 2011-08-07 2017-07-19 ブルー キューブ アイピー エルエルシー 塩素化プロペンの製造方法
EP2782889B1 (en) 2011-11-21 2016-12-21 Blue Cube IP LLC Process for the production of chlorinated alkanes
JP6050375B2 (ja) 2011-12-02 2016-12-21 ブルー キューブ アイピー エルエルシー クロロアルカンの製造方法
US9199899B2 (en) 2011-12-02 2015-12-01 Blue Cube Ip Llc Process for the production of chlorinated alkanes
JP6170068B2 (ja) 2011-12-13 2017-07-26 ブルー キューブ アイピー エルエルシー 塩素化プロパン及びプロペンの製造方法
IN2014CN04418A (es) 2011-12-22 2015-09-04 Dow Global Technologies Llc
BR112014015123A2 (pt) 2011-12-23 2017-06-13 Dow Global Technologies Llc processo para a produção de um ou mais alcenos ou compostos aromáticos
CN102744018B (zh) * 2012-06-25 2014-08-27 华东理工大学 一种可调节进口物料温度的固定床催化反应装置
CN104755448A (zh) 2012-09-20 2015-07-01 陶氏环球技术有限公司 用于制造氯化丙烯的方法
EP2897930A1 (en) 2012-09-20 2015-07-29 Dow Global Technologies LLC Process for the production of chlorinated propenes
US9440903B2 (en) 2012-09-24 2016-09-13 Arkema Inc. Shell and tube oxidation reactor with improved resistance to fouling
EP2900364B1 (en) 2012-09-30 2018-06-13 Blue Cube IP LLC Weir quench and processes incorporating the same
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Also Published As

Publication number Publication date
WO2000054877A2 (de) 2000-09-21
CN1343137A (zh) 2002-04-03
EP1169119B1 (de) 2003-10-15
JP2002538951A (ja) 2002-11-19
KR20020004965A (ko) 2002-01-16
KR100648579B1 (ko) 2006-11-24
WO2000054877A3 (de) 2001-04-05
DE50004079D1 (de) 2003-11-20
JP5204356B2 (ja) 2013-06-05
ES2209870T3 (es) 2004-07-01
TW527218B (en) 2003-04-11
MXPA01009012A (es) 2002-01-01
ATE251944T1 (de) 2003-11-15
BR0009000B1 (pt) 2011-01-25
CN1231291C (zh) 2005-12-14
EP1169119A2 (de) 2002-01-09
US7226567B1 (en) 2007-06-05
BR0009000A (pt) 2002-01-02
MY125244A (en) 2006-07-31
AU4538700A (en) 2000-10-04

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