AR071694A1 - Procedimiento para la obtencion de arilcarboxamidas - Google Patents

Procedimiento para la obtencion de arilcarboxamidas

Info

Publication number
AR071694A1
AR071694A1 ARP090101657A ARP090101657A AR071694A1 AR 071694 A1 AR071694 A1 AR 071694A1 AR P090101657 A ARP090101657 A AR P090101657A AR P090101657 A ARP090101657 A AR P090101657A AR 071694 A1 AR071694 A1 AR 071694A1
Authority
AR
Argentina
Prior art keywords
halogen
obtaining
arylamine
substituents
mono
Prior art date
Application number
ARP090101657A
Other languages
English (en)
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of AR071694A1 publication Critical patent/AR071694A1/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/81—Amides; Imides
    • C07D213/82—Amides; Imides in position 3
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/16—Halogen atoms or nitro radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Pyridine Compounds (AREA)
  • Heterocyclic Compounds Containing Sulfur Atoms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Procedimiento para la obtencion de arilcarboxamidas de la formula (1) en la que Ar es un anillo fenilo, piridilo o pirazolilo mono a trisustituido, seleccionando los sustituyentes de halogeno, alquilo C1-4 y halogenoalquilo C1-4; M es tienilo o fenilo, que puede llevar un sustituyente halogeno; Q es un enlace directo, ciclopropileno, un anillo biciclo[2.2.1]heptano o biciclo[2.2.1]hepteno anelado; R1 es hidrogeno, halogeno, alquilo C1-6, alcoxi C1-4, halogenoalcoxi C1-4, fenilo mono a trisustituido, seleccionando los sustituyentes de halogeno y trifluorometiltio, o ciclopropilo; transformando un cloruro de  cido de la formula (2) con una arilamina (3) en un solvente no soluble en agua apropiado, en cuyo procedimiento a) se presenta el cloruro de  cido (2) como carga inicial en presencia de una base auxiliar, b) se regula una presion de 0 hasta 700 mbar, c) se dosifica la arilamina (3) en cantidad aproximadamente estequiometrica y d) se a¡sla el producto de valor.
ARP090101657A 2008-05-08 2009-05-07 Procedimiento para la obtencion de arilcarboxamidas AR071694A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP08155888 2008-05-08

Publications (1)

Publication Number Publication Date
AR071694A1 true AR071694A1 (es) 2010-07-07

Family

ID=39719199

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP090101657A AR071694A1 (es) 2008-05-08 2009-05-07 Procedimiento para la obtencion de arilcarboxamidas

Country Status (19)

Country Link
US (1) US8350046B2 (es)
EP (1) EP2285779B1 (es)
JP (1) JP5731374B2 (es)
KR (1) KR20110004903A (es)
CN (1) CN102015649B (es)
AR (1) AR071694A1 (es)
AU (1) AU2009245791B2 (es)
BR (1) BRPI0912383A2 (es)
CA (1) CA2721695C (es)
DK (1) DK2285779T3 (es)
EA (1) EA018518B1 (es)
ES (1) ES2409605T3 (es)
IL (1) IL208657A (es)
MX (1) MX317270B (es)
PL (1) PL2285779T3 (es)
PT (1) PT2285779E (es)
UA (1) UA103323C2 (es)
WO (1) WO2009135860A1 (es)
ZA (1) ZA201008742B (es)

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GB0908435D0 (en) 2009-05-15 2009-06-24 Syngenta Ltd Processes
JP5763634B2 (ja) 2009-07-28 2015-08-12 シンジェンタ パーティシペーションズ アクチェンゲゼルシャフト ピラゾールのアルキル化に関する方法
MX2012001067A (es) 2009-07-31 2012-03-16 Syngenta Participations Ag Procesos para la alquilacion de pirazoles.
GB201004299D0 (en) 2010-03-15 2010-04-28 Syngenta Participations Ag Process
GB201004301D0 (en) 2010-03-15 2010-04-28 Syngenta Participations Ag Process
CA3004565C (en) 2010-08-10 2020-03-24 Syngenta Participations Ag Process for the preparation of 3-haloalkylpyrazoles
WO2012065947A1 (en) * 2010-11-15 2012-05-24 Bayer Cropscience Ag 5-halogenopyrazolecarboxamides
EP2723720A1 (de) 2011-06-21 2014-04-30 Bayer Intellectual Property GmbH Verfahren zur herstellung von pyrazolylcarboxaniliden
CN104995171B (zh) 2012-12-19 2018-02-06 拜耳作物科学股份公司 作为杀真菌剂的二氟甲基‑烟碱‑茚满基甲酰胺
EP2935218A1 (en) 2012-12-19 2015-10-28 Bayer CropScience AG Difluoromethyl-nicotinic- tetrahydronaphtyl carboxamides
CN103980192B (zh) * 2014-01-20 2016-02-17 泰州百力化学股份有限公司 一种选择性合成不同晶型啶酰菌胺的方法
CN104016915B (zh) * 2014-06-27 2016-03-30 重庆工商大学 一种啶酰菌胺的制备方法
GB2539022B (en) * 2015-06-04 2018-02-07 Rotam Agrochem Int Co Ltd Process for preparing boscalid
GB2536979B (en) * 2015-06-04 2019-03-13 Rotam Agrochem Int Co Ltd Process for preparing boscalid
CN108699004A (zh) * 2016-02-18 2018-10-23 索尔维公司 用于制造羧酰胺的方法
WO2018060836A1 (en) * 2016-09-28 2018-04-05 Upl Limited Process for preparation of boscalid anhydrate form i and boscalid anhydrate form ii
CN110028450A (zh) * 2018-01-12 2019-07-19 沈阳中化农药化工研发有限公司 一种吡唑酰胺类化合物的制备方法
MX2020010512A (es) * 2018-04-06 2020-10-22 Bayer Ag Metodo para la produccion de 3,4-dicloro-n-(2-cianofenil)-5-isotia zolecarboxamida.
WO2019224175A1 (en) * 2018-05-23 2019-11-28 Bayer Aktiengesellschaft Process for producing difluoromethyl-nicotinic-indanyl carboxamides
EP4069681A1 (en) 2019-12-05 2022-10-12 Basf Se Preparation of substituted aromatic carboxamides

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Also Published As

Publication number Publication date
PL2285779T3 (pl) 2013-08-30
IL208657A (en) 2014-05-28
EA018518B1 (ru) 2013-08-30
WO2009135860A1 (de) 2009-11-12
BRPI0912383A2 (pt) 2015-07-28
CA2721695A1 (en) 2009-11-12
ZA201008742B (en) 2012-02-29
JP5731374B2 (ja) 2015-06-10
UA103323C2 (ru) 2013-10-10
US8350046B2 (en) 2013-01-08
CA2721695C (en) 2016-04-12
CN102015649A (zh) 2011-04-13
EP2285779A1 (de) 2011-02-23
AU2009245791A1 (en) 2009-11-12
MX2010011276A (es) 2010-11-09
AU2009245791B2 (en) 2013-05-16
DK2285779T3 (da) 2013-06-24
IL208657A0 (en) 2010-12-30
US20110054183A1 (en) 2011-03-03
EP2285779B1 (de) 2013-03-27
ES2409605T3 (es) 2013-06-27
MX317270B (es) 2014-01-20
CN102015649B (zh) 2013-06-19
PT2285779E (pt) 2013-05-22
JP2011519895A (ja) 2011-07-14
EA201001730A1 (ru) 2011-06-30
KR20110004903A (ko) 2011-01-14

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