AR034597A1 - Procedimiento para la obtencion de n-fosfonometilglicina. - Google Patents
Procedimiento para la obtencion de n-fosfonometilglicina.Info
- Publication number
- AR034597A1 AR034597A1 ARP020102292A ARP020102292A AR034597A1 AR 034597 A1 AR034597 A1 AR 034597A1 AR P020102292 A ARP020102292 A AR P020102292A AR P020102292 A ARP020102292 A AR P020102292A AR 034597 A1 AR034597 A1 AR 034597A1
- Authority
- AR
- Argentina
- Prior art keywords
- phosphonomethylglycine
- halides
- obtaining
- retentate
- poorer
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- XDDAORKBJWWYJS-UHFFFAOYSA-N glyphosate Chemical compound OC(=O)CNCP(O)(O)=O XDDAORKBJWWYJS-UHFFFAOYSA-N 0.000 abstract 8
- 239000000203 mixture Substances 0.000 abstract 3
- -1 ammonium halides Chemical class 0.000 abstract 2
- 150000004820 halides Chemical class 0.000 abstract 2
- 239000012465 retentate Substances 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- 239000005562 Glyphosate Substances 0.000 abstract 1
- 229910001508 alkali metal halide Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910001615 alkaline earth metal halide Inorganic materials 0.000 abstract 1
- 229940097068 glyphosate Drugs 0.000 abstract 1
- 230000002363 herbicidal effect Effects 0.000 abstract 1
- 239000004009 herbicide Substances 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000012528 membrane Substances 0.000 abstract 1
- 238000001728 nano-filtration Methods 0.000 abstract 1
- 239000012466 permeate Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
- C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Procedimiento para la obtención de N-fosfonometilglicina de la fórmula (1) a partir de una mezcla acuosa que contiene disueltos en la misma N-fosfonometilglicina, halogenuros de amonio, así como también halogenuros de metales alcalinos o alcalinotérreos y eventualmente impurezas orgánicas, en donde a) se ajusta el pH de la mezcla a un valor en el rango de 2 a 8; b) se realiza una separación de la mezcla en una membrana de nanofiltración selectiva, obteniéndose un retentato más rico en N-fosfonometilglicina y más pobre en halogenuros y un permeato más rico en halogenuros y más pobre en N-fosfonometilglicina; y c) se obtiene N-fosfonometilglicina a partir de retentato. El procedimiento descripto permite la obtención de la N-fosfonometilglicina con separación simultánea de las sales de halogenuros. La N-fosfonometilglicina, también conocida como glifosato, es un herbicida total ampliamente utilizado en el agro.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10130136A DE10130136A1 (de) | 2001-06-22 | 2001-06-22 | Verfahren zur Gewinnung von N-Phosphonomethylglycin |
Publications (1)
Publication Number | Publication Date |
---|---|
AR034597A1 true AR034597A1 (es) | 2004-03-03 |
Family
ID=7689074
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP020102292A AR034597A1 (es) | 2001-06-22 | 2002-06-19 | Procedimiento para la obtencion de n-fosfonometilglicina. |
Country Status (23)
Country | Link |
---|---|
US (1) | US7071354B2 (es) |
EP (1) | EP1401846B1 (es) |
JP (1) | JP3987488B2 (es) |
KR (1) | KR100859383B1 (es) |
CN (1) | CN1257909C (es) |
AR (1) | AR034597A1 (es) |
AT (1) | ATE284890T1 (es) |
AU (1) | AU2002321099B2 (es) |
BR (1) | BR0210569B1 (es) |
CA (1) | CA2451507C (es) |
DE (2) | DE10130136A1 (es) |
DK (1) | DK1401846T3 (es) |
ES (1) | ES2233846T3 (es) |
IL (2) | IL159072A0 (es) |
IN (1) | IN2003CH02042A (es) |
MX (1) | MX234329B (es) |
NZ (1) | NZ530049A (es) |
PT (1) | PT1401846E (es) |
RU (1) | RU2274641C2 (es) |
SI (1) | SI1401846T1 (es) |
TW (1) | TW575579B (es) |
WO (1) | WO2003000704A2 (es) |
ZA (1) | ZA200400433B (es) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AR039201A1 (es) * | 2003-03-28 | 2005-02-09 | Atanor S A | Procedimiento para purificar soluciones de glifosato mediante nanofiltracion |
TW200538459A (en) * | 2004-05-21 | 2005-12-01 | Dow Agrosciences Llc | Purification of n-(phosphonomethyl)glycine |
EP1886976A1 (en) | 2006-08-09 | 2008-02-13 | Thermphos Trading GmbH | Method of scale inhibition |
US7771494B2 (en) * | 2007-01-31 | 2010-08-10 | Monsanto Technology Llc | Process for selective removal of water and impurities from N-(phosphonomethyl)glycine |
EP2090646A1 (en) | 2008-01-22 | 2009-08-19 | Thermphos Trading GmbH | Surface treatment composition containing phosphonic acid compounds |
EP2082991A1 (en) | 2008-01-22 | 2009-07-29 | Thermphos Trading GmbH | Method of Water Treatment |
CN102459091B (zh) * | 2009-05-18 | 2014-06-18 | 孟山都技术公司 | 含水废物流中磷有用成分和盐杂质的回收 |
KR200453576Y1 (ko) * | 2011-03-14 | 2011-05-17 | 이상호 | 라이트 박스 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3950402A (en) * | 1972-05-31 | 1976-04-13 | Monsanto Company | Process for producing N-phosphonomethyl glycine |
US3969398A (en) * | 1974-05-01 | 1976-07-13 | Monsanto Company | Process for producing N-phosphonomethyl glycine |
RO65811A (fr) | 1974-06-26 | 1979-07-15 | Budapesti Vegyimuevek | Procede pour obtenir du n-phosphonombethyl-glycine |
HU184601B (en) * | 1979-07-09 | 1984-09-28 | Alkaloida Vegyeszeti Gyar | Process for producing n-/phosphono-methyl/-glycine |
PL159424B1 (pl) * | 1989-04-18 | 1992-12-31 | Sposób wytwarzania N-fosfonometyloglicyny PL | |
EP0806428B1 (en) | 1994-11-09 | 2003-01-29 | Showa Denko Kabushiki Kaisha | Method for isolating N-phosphonomethylglycine |
US5587083A (en) | 1995-04-17 | 1996-12-24 | Chemetics International Company Ltd. | Nanofiltration of concentrated aqueous salt solutions |
IT1281094B1 (it) * | 1995-12-21 | 1998-02-11 | Graziello Donadello | Procedimento per la produzione di n-fosfonometilglicina e/o suoi sali |
AR027024A1 (es) | 1999-12-23 | 2003-03-12 | Basf Ag | Procedimiento para la preparacion de n-fosfonometilglicina |
AR029508A1 (es) | 2000-04-14 | 2003-07-02 | Dow Agrosciences Llc | Proceso para remover y recuperar cloruro de sodio de los efluentes de desecho provenientes de los procesos de fabricacion del acido n-fosfometiliminodiacetico (pmida) |
-
2001
- 2001-06-22 DE DE10130136A patent/DE10130136A1/de not_active Withdrawn
-
2002
- 2002-06-19 AR ARP020102292A patent/AR034597A1/es active IP Right Grant
- 2002-06-21 AT AT02754734T patent/ATE284890T1/de active
- 2002-06-21 US US10/481,565 patent/US7071354B2/en not_active Expired - Fee Related
- 2002-06-21 PT PT02754734T patent/PT1401846E/pt unknown
- 2002-06-21 CN CNB028122143A patent/CN1257909C/zh not_active Expired - Fee Related
- 2002-06-21 JP JP2003507107A patent/JP3987488B2/ja not_active Expired - Fee Related
- 2002-06-21 NZ NZ530049A patent/NZ530049A/en not_active IP Right Cessation
- 2002-06-21 DE DE50201799T patent/DE50201799D1/de not_active Expired - Lifetime
- 2002-06-21 AU AU2002321099A patent/AU2002321099B2/en not_active Ceased
- 2002-06-21 RU RU2004101770/04A patent/RU2274641C2/ru not_active IP Right Cessation
- 2002-06-21 CA CA2451507A patent/CA2451507C/en not_active Expired - Fee Related
- 2002-06-21 WO PCT/EP2002/006903 patent/WO2003000704A2/de active IP Right Grant
- 2002-06-21 KR KR1020037016619A patent/KR100859383B1/ko not_active IP Right Cessation
- 2002-06-21 ES ES02754734T patent/ES2233846T3/es not_active Expired - Lifetime
- 2002-06-21 SI SI200230059T patent/SI1401846T1/xx unknown
- 2002-06-21 MX MXPA03011229 patent/MX234329B/es active IP Right Grant
- 2002-06-21 DK DK02754734T patent/DK1401846T3/da active
- 2002-06-21 EP EP02754734A patent/EP1401846B1/de not_active Expired - Lifetime
- 2002-06-21 BR BRPI0210569-1B1A patent/BR0210569B1/pt not_active IP Right Cessation
- 2002-06-21 IL IL15907202A patent/IL159072A0/xx unknown
- 2002-10-18 TW TW91113652A patent/TW575579B/zh not_active IP Right Cessation
-
2003
- 2003-11-26 IL IL159072A patent/IL159072A/en not_active IP Right Cessation
- 2003-12-03 IN IN2042CH2003 patent/IN2003CH02042A/en unknown
-
2004
- 2004-01-21 ZA ZA200400433A patent/ZA200400433B/en unknown
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Legal Events
Date | Code | Title | Description |
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FG | Grant, registration |