WO2023179101A1 - 一种电磁反应釜及其应用 - Google Patents

一种电磁反应釜及其应用 Download PDF

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Publication number
WO2023179101A1
WO2023179101A1 PCT/CN2022/137780 CN2022137780W WO2023179101A1 WO 2023179101 A1 WO2023179101 A1 WO 2023179101A1 CN 2022137780 W CN2022137780 W CN 2022137780W WO 2023179101 A1 WO2023179101 A1 WO 2023179101A1
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WIPO (PCT)
Prior art keywords
electromagnetic
kettle
kettle body
reaction kettle
electromagnetic reaction
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PCT/CN2022/137780
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English (en)
French (fr)
Inventor
赵振
宋文星
张琼珶
喻学锋
周文华
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深圳先进技术研究院
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Publication of WO2023179101A1 publication Critical patent/WO2023179101A1/zh

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents

Definitions

  • This application belongs to the technical field of electromagnetic reaction equipment, and in particular relates to an electromagnetic reaction kettle and its application.
  • the broad understanding of a reactor is a container for physical or chemical reactions. Through the structural design and parameter configuration of the container, the heating, evaporation, cooling and low-speed mixing functions required by the process are realized.
  • the reactor is widely used in petroleum, chemical industry, In the fields of rubber, pesticides, dyes, medicine and food, it is a pressure vessel used to complete vulcanization, nitration, hydrogenation, hydrocarbonization, polymerization, condensation and other processes.
  • Magnetic polymer microspheres are a new type of magnetic material developed in recent years. They are composite microspheres with certain magnetism and special structure formed by combining magnetic inorganic particles and organic polymers through appropriate methods.
  • An electromagnetic reaction kettle is required.
  • the existing electromagnetic reaction kettles for the synthesis of magnetic microspheres currently on the market still have the disadvantage of being inconvenient for loading.
  • the traditional electromagnetic reaction kettle for synthesis of magnetic microspheres is generally loaded.
  • the magnetic microsphere raw materials are directly introduced into the reaction kettle for reaction, which is inconvenient to load according to the amount of raw materials, resulting in a reduction in the production and synthesis efficiency of magnetic microspheres, affecting the final yield of magnetic microspheres, and making it inconvenient to use.
  • the magnetic microsphere raw materials are generally directly introduced into the reaction kettle for reaction, which is inconvenient to load according to the amount of raw materials, resulting in a reduction in the production and synthesis efficiency of magnetic microspheres.
  • the problem affects the final yield of magnetic microspheres and is inconvenient to use.
  • This application provides an electromagnetic reaction kettle and its application.
  • an electromagnetic reaction kettle which includes a kettle body.
  • the kettle body is provided with a feeding mechanism and a discharging mechanism.
  • the feeding mechanism is connected with the kettle body, and the discharging mechanism is connected with the kettle body.
  • the feeding mechanism is connected with the kettle body, and the kettle body is provided with an electromagnetic reaction mechanism; the feeding mechanism includes a raw material storage component, and the raw material storage component is connected to the metering and feeding component.
  • the raw material storage assembly includes a material box, a horizontal bar is provided in the material box, a rotating motor is provided on the horizontal bar, the rotating motor is connected to the turntable, and the
  • the loading assembly includes a number of tracks, the tracks are arranged in the material box, a material sensor is provided in the track, the material sensor is connected to the meter, and the material box is connected to the kettle body through a discharge pipe.
  • the turntable is provided with a plurality of holes, the holes are slidingly connected to the blocking ball, and the blocking ball is connected to the hole through a spring.
  • the electromagnetic reaction mechanism includes a driving motor, the driving motor is arranged on the kettle body, the driving motor is connected to a rotating rod through a transmission assembly, and a rotating rod is provided on the rotating rod.
  • the driving motor is connected to a rotating rod through a transmission assembly, and a rotating rod is provided on the rotating rod.
  • the transmission assembly includes a driving bevel gear and a driven bevel gear that mesh with each other, the driving bevel gear is connected to the drive motor, and the driven bevel gear is connected to the rotating bevel gear. Rod connection.
  • stirring shaft is a U-shaped stirring shaft, and a protective cover is provided outside the driving motor.
  • a heating component is provided in the kettle body.
  • the heating component includes a chamber, the chamber is disposed on the inner wall of the kettle, a heating liquid is disposed in the chamber, and an electric heating tube is disposed in the chamber.
  • Another implementation provided by this application is: it also includes a plurality of legs, the legs are arranged at the bottom of the kettle body, and the kettle body is provided with a side material pipe.
  • This application also provides an application of the electromagnetic reactor, which is used in the synthesis of magnetic microspheres.
  • the electromagnetic reaction kettle provided by this application has the advantage of being easy to load materials, and solves the problem that the existing electromagnetic reaction kettles used for the synthesis of magnetic microspheres are not easy to load materials.
  • the electromagnetic reaction kettle provided by this application is equipped with a feeding mechanism above the kettle body.
  • the feeding mechanism can automatically load materials and at the same time has a metering function, which can measure the amount of magnetic microspheres entering the kettle body, thereby making the magnetic microspheres.
  • the reaction synthesis effect is better, the yield of the final magnetic microspheres is improved, and a mechanical structure is used for loading, with a high degree of automation, simple operation, and convenient use.
  • the application of the electromagnetic reaction kettle provided in this application can not only be applied to the synthesis of magnetic microspheres, but also can be used to purify magnetic microspheres by installing an electromagnetic reaction mechanism in the kettle body and integrating the design to combine reaction with electromagnetism. , greatly compressing the steps and time of purification, reducing the cost of purification, and meeting the requirements for preparation and purification of magnetic microspheres.
  • Figure 1 is a schematic structural diagram of the electromagnetic reactor of the present application.
  • FIG. 2 is a schematic structural diagram of the loading mechanism of the present application.
  • FIG. 3 is a partial structural diagram of the present application.
  • Figure 4 is a schematic structural diagram of the electromagnetic reaction mechanism of the present application.
  • Figure 5 is a schematic structural diagram of the electromagnetic coil of the present application.
  • this application provides an electromagnetic reaction kettle, which includes a kettle body 1.
  • the kettle body 1 is provided with a feeding mechanism 3 and a discharging mechanism.
  • the feeding mechanism is connected with the kettle body 1.
  • the discharging mechanism is connected to the kettle body 1, and an electromagnetic reaction mechanism 2 is provided in the kettle body 1;
  • the feeding mechanism 3 includes a raw material storage component, and the raw material storage component is connected to the metering and feeding component.
  • the loading mechanism 3 is used to automatically meter and load magnetic microsphere raw materials, thereby improving the preparation and purification effect of magnetic microspheres.
  • the kettle body 1 is provided with an electromagnetic reaction mechanism 2, a feeding mechanism 3 is provided on the upper surface of the kettle body 1, and a discharge pipe 7 is fixedly connected to the center of the bottom of the kettle body 1.
  • the bottom of the inner cavity of the kettle body 1 is tapered to facilitate unloading.
  • the amount of material is adjusted by measuring the feeding component, so that an appropriate amount of material enters the kettle body 1 from the feeding mechanism 3 for reaction, and then the remaining material is discharged through the discharging mechanism.
  • the raw material storage assembly includes a material box 302, a cross bar 303 is provided in the material box 302, a rotating motor 304 is provided on the cross bar 303, the rotating motor 304 is connected to the turntable 305, and the upper
  • the material assembly includes a number of tracks 306.
  • the tracks 306 are arranged in the material box 302.
  • a material sensor 308 is provided in the track 306.
  • the material sensor 308 is connected to a meter.
  • the material box 302 passes through a feeding pipe. 301 is connected with the cauldron body 1.
  • the loading mechanism 3 includes a feeding tube 301 fixedly connected to the left end of the upper surface of the kettle body 1.
  • the top of the feeding tube 301 is fixedly connected to a material box 302.
  • the left and right sides of the inner cavity of the material box 302 are A crossbar 303 is fixedly connected between the walls, a rotating motor 304 is fixedly connected to the top of the crossbar 303, and a turntable 305 is fixedly connected to the output shaft of the rotating motor 304.
  • the upper and lower ends of the turntable 305 are tapered, and the bottom of the inner cavity of the material box 302 is tapered.
  • the turntable 305 is provided with a plurality of holes 309 , the holes 309 are slidingly connected to the blocking ball 311 , and the blocking ball 311 is connected to the hole 309 through a spring 310 .
  • a plurality of rails 306 are fixedly connected to the bottom of the inner wall of the material box 302.
  • a moving groove 307 is provided inside the rails 306.
  • a material sensor 308 is fixedly connected to the inside of the moving groove 307.
  • the turntable 305 A plurality of holes 309 are opened on the outer surface of the hole 309 , and a retaining ball 311 is slidably connected inside the hole 309 .
  • a spring 310 is in contact between the retaining ball 311 and the inner wall of the hole 309 .
  • the cross section of the moving groove 307 is semicircular, and the two ends of the rail 306 are in the shape of arc-shaped crests, which facilitates the material to enter the inside of the moving groove 307.
  • the rail 306 can be squeezed.
  • the pressing ball 311 moves, and then the pressing spring 310 contracts.
  • the material sensor 308 is in the same plane as the inner wall of the moving groove 307, which facilitates smooth movement of the material in the moving groove 307 and facilitates inductive measurement of the material.
  • the loading mechanism 3 is rotated by the turntable 305 and cooperates with the retaining ball 311 to realize automatic loading of magnetic microsphere materials and facilitate the measurement of materials.
  • the electromagnetic reaction mechanism 2 includes a driving motor 201.
  • the driving motor 201 is arranged on the kettle body 1.
  • the driving motor 201 is connected to the rotating rod 203 through the transmission assembly 202.
  • the rotating rod 203 is provided with There are several stirring shafts 205, and electromagnetic coils 206 are provided on the stirring shafts 205, and the electromagnetic coils 206 are connected to wires 204.
  • the electromagnetic reaction mechanism 2 includes a drive motor 201 fixedly connected to the upper surface of the kettle body 1.
  • the electromagnetic reaction mechanism 2 also includes a rotating rod 203 that is rotationally connected to the top of the kettle body 1.
  • the rotating rod 203 is connected to the drive motor 201.
  • a transmission assembly 202 is provided between the motors 201, and a wire 204 is provided inside the rotating rod 203.
  • a plurality of stirring shafts 205 are fixedly connected to the outer surface of the rotating rod 203, and an electromagnetic coil is sleeved on the stirring shaft 205. 206.
  • the electromagnetic coil 205 When the electromagnetic coil 205 is powered on, it can adsorb the magnetic microspheres, and when the power is turned off, the magnetic microspheres will fall off.
  • the electromagnetic coil 206 includes a coil outer cover 2061 and a coil inner core 2062.
  • the coil outer cover 2061 is sleeved on the outer surface of the coil inner core 2062.
  • the transmission assembly 202 includes driving bevel teeth and driven bevel teeth that mesh with each other.
  • the driving bevel teeth are connected to the driving motor 201
  • the driven bevel teeth are connected to the rotating rod 203 .
  • the transmission assembly 202 includes a driving bevel gear fixedly connected to the output shaft of the drive motor 201.
  • the transmission assembly 202 also includes a driven bevel gear fixedly connected to the top of the outer surface of the rotating rod 203.
  • the driven bevel gear Engage with the driving bevel teeth.
  • the output shaft of the driving motor 201 drives the driving bevel gear to rotate, and cooperates with the driven bevel gear to drive the rotating rod 203 to rotate.
  • the stirring shaft 205 is a U-shaped stirring shaft, and a protective cover is provided outside the driving motor 201.
  • a protective cover is fixedly connected to the top of the kettle body 1, the driving motor 201 is located inside the protective cover, and the top of the rotating rod 203 penetrates to the outside of the protective cover and is rotationally connected with it.
  • the electromagnetic reaction mechanism 2 drives the output shaft of the motor 201 to rotate, and cooperates with the transmission assembly 202 to drive the rotating rod 203 to rotate, thereby driving the stirring shaft 205 and the electromagnetic coil 206 to rotate, and realizes the preparation and purification of magnetic microspheres.
  • a heating component is provided in the kettle body 1 .
  • the heating component includes a chamber 4, which is arranged on the inner wall of the kettle body 1.
  • a heating liquid 5 is arranged in the chamber 4, and an electric heating tube 6 is arranged in the chamber 4. .
  • a chamber 4 is provided on the inner wall of the kettle body 1, and the interior of the chamber 4 is filled with heating liquid 5.
  • Electric heating tubes 6 are fixedly connected to both left and right ends of the bottom of the kettle body 1.
  • the top of the electric heating tube 6 is located inside the chamber 4.
  • the electric heating tube 6 works to heat the heating liquid 5.
  • the top of the right end of the kettle body 1 is fixedly connected with an L-shaped liquid replenishing tube connected to the chamber 4. .
  • the left and right ends of the bottom of the kettle body 1 are fixedly connected with drain pipes connected to the chamber 4, and the drain pipes are provided with drain valves to facilitate the discharge of the heating liquid 5.
  • the bottom of the inner cavity of the kettle body 1 is tapered, and the left and right ends of the bottom of the kettle body 1 are fixedly connected with drain pipes connected to the chamber 4, and the drain pipes are provided with drain valves, so
  • the discharge pipe 7 is provided with a discharge valve.
  • the kettle body 1 also includes a plurality of legs 8, which are arranged at the bottom of the kettle body 1, and a side material pipe 9 is provided on the kettle body 1.
  • Legs 8 are fixedly connected around the bottom of the kettle body 1, and a side material pipe 9 is fixedly connected to the right end of the top of the kettle body 1.
  • This application also provides an application of the electromagnetic reactor, which is used in the synthesis of magnetic microspheres.
  • the magnetic microsphere raw materials are in the material box 302, and the output shaft of the rotating motor 304 drives the turntable 305 to rotate. Since the upper and lower ends of the turntable 305 are tapered, the magnetic microsphere raw materials can enter the edge of the turntable 305 and move along the The moving groove 307 enters. When the turntable 305 rotates, the turntable 305 drives the blocking ball 311 to move into the moving groove 307, which can block the magnetic microsphere raw material from continuing to fall. When the turntable 305 drives the blocking ball 311 to move to the point where it no longer contacts the moving groove 307. , the magnetic microsphere raw materials continue to fall and enter the kettle body 1 through the discharge pipe 301.
  • the material sensor 308 senses the falling materials and is connected through an external counter to count. When the magnetic microsphere raw materials meet the reaction quantity, The blocking ball 311 moves into the moving groove 307 to block the magnetic microsphere raw material from being discharged. At the same time, the speed during discharging can also be adjusted.
  • the output shaft of the driving motor 201 drives the driving gear to rotate.
  • the driving gear meshes with the driven gear, thereby causing the rotating rod 203 to rotate.
  • the electromagnetic coil 206 is connected to the external power supply and control through wires. When the electromagnetic coil 206 is energized, the magnetic microspheres can be magnetically attracted, enter the chamber 4 through the heating liquid 5, and then be heated by the electric heating tube 6, so as to facilitate the heating reaction inside the kettle body 1.

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Abstract

本申请属于电磁反应设备技术领域，特别是涉及一种电磁反应釜及其应用。传统的磁性微球合成用电磁反应釜上料，一般是直接将磁性微球原料导入至反应釜中进行反应，不便于根据原料的多少，进行上料，导致磁性微球生产合成效率降低，影响最终磁性微球的成品率，不便于使用。本申请提供了一种电磁反应釜，包括釜体，所述釜体上设置有上料机构和出料机构，所述上料机构与所述釜体连通，所述出料机构与所述釜体连通，所述釜体内设置有电磁反应机构；所述上料机构包括原料存储组件，所述原料存储组件与计量上料组件连接。使得磁性微球反应合成效果更好，提高最终磁性微球的成品率，且采用机械结构进行上料，自动化程度高，操作简便，使用方便。

Description

一种电磁反应釜及其应用 技术领域
本申请属于电磁反应设备技术领域，特别是涉及一种电磁反应釜及其应用。
 背景技术
反应釜的广义理解即有物理或化学反应的容器，通过对容器的结构设计与参数配置，实现工艺要求的加热、蒸发、冷却及低高速的混配功能，反应釜广泛应用于石油、化工、橡胶、农药、染料、医药和食品等领域，是用来完成硫化、硝化、氢化、烃化、聚合、缩合等工艺过程的压力容器。
磁性高分子微球是近年发展起来的一种新型磁性材料，是通过适当方法将磁性无机粒子与有机高分子结合形成的具有一定磁性及特殊结构的复合微球，在磁性微球生产过程中，需要用到电磁反应釜，目前市面上现有的磁性微球合成用电磁反应釜还存在着不便于上料的缺点，在使用过程中，传统的磁性微球合成用电磁反应釜上料，一般是直接将磁性微球原料导入至反应釜中进行反应，不便于根据原料的多少，进行上料，导致磁性微球生产合成效率降低，影响最终磁性微球的成品率，不便于使用。
 技术问题
基于传统的磁性微球合成用电磁反应釜上料，一般是直接将磁性微球原料导入至反应釜中进行反应，不便于根据原料的多少，进行上料，导致磁性微球生产合成效率降低，影响最终磁性微球的成品率，不便于使用的问题，本申请提供了一种电磁反应釜及其应用。
 技术解决方案
为了达到上述的目的，本申请提供了一种电磁反应釜，包括釜体，所述釜体上设置有上料机构和出料机构，所述上料机构与所述釜体连通，所述出料机构与所述釜体连通，所述釜体内设置有电磁反应机构；所述上料机构包括原料存储组件，所述原料存储组件与计量上料组件连接。
本申请提供的另一种实施方式为：所述原料存储组件包括料箱，所述料箱内设置有横杆，所述横杆上设置有旋转电机，所述旋转电机与转盘连接，所述上料组件包括若干轨道，所述轨道设置于所述料箱内，所述轨道内设置有物料传感器，所述物料传感器与计量器连接，所述料箱通过下料管与釜体贯通。
本申请提供的另一种实施方式为：所述转盘上设置有若干孔道，所述孔道与挡球滑动连接，所述挡球通过弹簧与所述孔道连接。
本申请提供的另一种实施方式为：所述电磁反应机构包括驱动电机，所述驱动电机设置于所述釜体上，所述驱动电机通过传动组件与转杆连接，所述转杆上设置有若干搅拌轴，所述搅拌轴上设置有电磁线圈，所述电磁线圈与导线连接。
本申请提供的另一种实施方式为：所述传动组件包括相互啮合的主动锥齿和从动锥齿，所述主动锥齿与所述驱动电机连接，所述从动锥齿与所述转杆连接。
本申请提供的另一种实施方式为：所述搅拌轴为U形搅拌轴，所述驱动电机外侧设置有防护罩。
本申请提供的另一种实施方式为：所述釜体内设置有加热组件。
本申请提供的另一种实施方式为：所述加热组件包括腔室，所述腔室设置于所述釜体内壁上，所述腔室内设置有加热液，所述腔室内设置有电热管。
本申请提供的另一种实施方式为：还包括若干支脚，所述支脚设置于所述釜体底部，所述釜体上设置有侧料管。
本申请还提供一种对所述的电磁反应釜的应用，将所述电磁反应釜应用于磁性微球合成。
 有益效果
与现有技术相比，本申请提供的电磁反应釜及其应用的有益效果在于：
本申请提供的电磁反应釜，具备便于上料等优点，解决了现有的磁性微球合成用电磁反应釜不便于上料的问题。
本申请提供的电磁反应釜，通过在釜体上方设有上料机构，上料机构可自动上料的同时，具有计量功能，可计量进入到釜体内磁性微球的多少，从而使得磁性微球反应合成效果更好，提高最终磁性微球的成品率，且采用机械结构进行上料，自动化程度高，操作简便，使用方便。
本申请提供的电磁反应釜的应用，通过在釜体内设有电磁反应机构，集成化设计，将反应与电磁进行结合，不仅可以应用于磁性微球的合成，而且可以对磁性微球进行纯化处理，大大压缩了纯化的步骤和时间，且降低了纯化成本，满足磁性微球制备与纯化要求。
 附图说明
图1是本申请的电磁反应釜结构示意图；
图2是本申请的上料机构结构示意图；
图3是本申请的局部结构示意图；
图4是本申请的电磁反应机构结构示意图；
图5是本申请的电磁线圈结构示意图。
 本发明的实施方式
在下文中，将参考附图对本申请的具体实施例进行详细地描述，依照这些详细的描述，所属领域技术人员能够清楚地理解本申请，并能够实施本申请。在不违背本申请原理的情况下，各个不同的实施例中的特征可以进行组合以获得新的实施方式，或者替代某些实施例中的某些特征，获得其它优选的实施方式。
参见图1～5，本申请提供一种电磁反应釜，包括釜体1，所述釜体1上设置有上料机构3和出料机构，所述上料机构与所述釜体1连通，所述出料机构与所述釜体1连通，所述釜体1内设置有电磁反应机构2；所述上料机构3包括原料存储组件，所述原料存储组件与计量上料组件连接。
所述上料机构3用于对磁性微球原料进行自动计量上料，以此提高磁性微球的制备与纯化效果。
具体的，所述釜体1内设有电磁反应机构2，所述釜体1的上表面设有上料机构3，所述釜体1底部的中心处固定连接有出料管7。釜体1内腔的底部呈锥形，方便进行卸料。
通过计量上料组件调整物料的量，使得适量的物料从上料机构3进入釜体1进行反应后，通过出料机构将残料排出。
进一步地，所述原料存储组件包括料箱302，所述料箱302内设置有横杆303，所述横杆303上设置有旋转电机304，所述旋转电机304与转盘305连接，所述上料组件包括若干轨道306，所述轨道306设置于所述料箱302内，所述轨道306内设置有物料传感器308，所述物料传感器308与计量器连接，所述料箱302通过下料管301与釜体1贯通。
具体的，所述上料机构3包括与釜体1上表面左端固定连接的下料管301，所述下料管301的顶部固定连接有料箱302，所述料箱302内腔的左右两侧壁之间固定连接有横杆303，所述横杆303的顶部固定连接有旋转电机304，所述旋转电机304的输出轴固定连接有转盘305。所述转盘305的上下两端均呈锥形，所述料箱302内腔的底部呈锥形。
进一步地，所述转盘305上设置有若干孔道309，所述孔道309与挡球311滑动连接，所述挡球311通过弹簧310与所述孔道309连接。
具体的，所述料箱302内侧壁的底部固定连接有多个轨道306，所述轨道306的内部开设有移动槽307，所述移动槽307的内部固定连接有物料传感器308，所述转盘305的外表面开设有多个孔道309，所述孔道309的内部滑动连接有挡球311，所述挡球311与孔道309的内壁之间抵接有弹簧310。
所述移动槽307的截面呈半圆形，所述轨道306的两端呈弧形的波峰状，方便物料进入到移动槽307内部的同时，挡球311接触到轨道306后，轨道306可挤压球体311移动，进而挤压弹簧310收缩。所述物料传感器308与移动槽307的内壁处于同一平面内，便于物料在移动槽307中平顺移动，同时方便对物料进行感应计量。
上料机构3，由转盘305旋转，并配合挡球311，可实现对磁性微球物料的自动上料，同时便于对物料进行计量。
进一步地，所述电磁反应机构2包括驱动电机201，所述驱动电机201设置于所述釜体1上，所述驱动电机201通过传动组件202与转杆203连接，所述转杆203上设置有若干搅拌轴205，所述搅拌轴205上设置有电磁线圈206，所述电磁线圈206与导线204连接。
具体的，所述电磁反应机构2包括与釜体1上表面固定连接的驱动电机201，所述电磁反应机构2还包括与釜体1顶部转动连接的转杆203，所述转杆203与驱动电机201之间设有传动组件202，所述转杆203的内部设有导线204，所述转杆203的外表面固定连接有多个搅拌轴205，所述搅拌轴205上套接有电磁线圈206。当电磁线圈205通电后，可对磁性微球吸附，断电则磁性微球掉落。
所述电磁线圈206包括线圈外套2061与线圈内芯2062，所述线圈外套2061套接于线圈内芯2062的外表面。
进一步地，所述传动组件202包括相互啮合的主动锥齿和从动锥齿，所述主动锥齿与所述驱动电机201连接，所述从动锥齿与所述转杆203连接。
具体的，所述传动组件202包括与驱动电机201输出轴固定连接的主动锥齿，所述传动组件202还包括与转杆203外表面顶部固定连接的从动锥齿，所述从动锥齿与主动锥齿相啮合。由驱动电机201的输出轴带动主动锥齿旋转，并配合从动锥齿，即可带动转杆203转动。
进一步地，所述搅拌轴205为U形搅拌轴，所述驱动电机201外侧设置有防护罩。
具体的，所述釜体1的顶部固定连接有防护罩，所述驱动电机201位于防护罩的内部，所述转杆203的顶部贯穿至防护罩的外部且与其转动连接。电磁反应机构2，通过驱动电机201的输出轴旋转，并配合传动组件202带动转杆203旋转，从而带动搅拌轴205与电磁线圈206旋转，并实现对磁性微球的制备与纯化。
进一步地，所述釜体1内设置有加热组件。
进一步地，所述加热组件包括腔室4，所述腔室4设置于所述釜体1内壁上，所述腔室4内设置有加热液5，所述腔室4内设置有电热管6。
具体的，所述釜体1的内壁上开设有腔室4，所述腔室4的内部填充有加热液5，所述釜体1底部的左右两端均固定连接有电热管6。所述电热管6的顶部位于腔室4的内部，由电热管6工作，可对加热液5进行加热，所述釜体1右端的顶部固定连接有与腔室4相连通的L形补液管。釜体1底部的左右两端均固定连接有与腔室4相连通的排液管，且排液管上设有排液阀，便于将加热液5排出，
所述釜体1内腔的底部呈锥形，所述釜体1底部的左右两端均固定连接有与腔室4相连通的排液管，且排液管上设有排液阀，所述出料管7上设有出料阀。
进一步地，还包括若干支脚8，所述支脚8设置于所述釜体1底部，所述釜体1上设置有侧料管9。
所述釜体1底部的四周均固定连接有支脚8，所述釜体1顶部的右端固定连接有侧料管9。
本申请还提供一种对所述的电磁反应釜的应用，将所述电磁反应釜应用于磁性微球合成。
本申请中的电磁反应釜工作原理为：
磁性微球原料处于料箱302中，由旋转电机304的输出轴带动转盘305旋转，由于转盘305的上下两端均呈锥形，使得磁性微球原料可以进入到转盘305的边缘处，同时沿移动槽307进入，当转盘305进行旋转时，转盘305带动挡球311移动到移动槽307内，可挡住磁性微球原料继续下落，而当转盘305带动挡球311移动到不在接触移动槽307时，磁性微球原料持续下落，并通过下料管301进入到釜体1内，物料传感器308对下落物料进行感应，并通过外部计数器连接，从而进行计数，当磁性微球原料满足反应数量时，挡球311移动到移动槽307内，挡住磁性微球原料不再下料，同时下料时的速度也可进行调节。
当磁性微球原料进入到釜体1后，由驱动电机201的输出轴带动主动齿轮旋转，主动齿轮与从动齿轮相啮合，从而使得转杆203转动，电磁线圈206通过导线与外部电源及控制器电连接，当电磁线圈206通电后，可对磁性微球进行磁吸，通过加热液5进入到腔室4内，然后由电热管6进行加热，方便对釜体1内部进行加热反应。
尽管在上文中参考特定的实施例对本申请进行了描述，但是所属领域技术人员应当理解，在本申请公开的原理和范围内，可以针对本申请公开的配置和细节做出许多修改。本申请的保护范围由所附的权利要求来确定，并且权利要求意在涵盖权利要求中技术特征的等同物文字意义或范围所包含的全部修改。

Claims (10)

  1. 一种电磁反应釜，其特征在于：包括釜体，所述釜体上设置有上料机构和出料机构，所述上料机构与所述釜体连通，所述出料机构与所述釜体连通，所述釜体内设置有电磁反应机构；
    所述上料机构包括原料存储组件，所述原料存储组件与计量上料组件连接。
  2. 如权利要求1所述的电磁反应釜，其特征在于：所述原料存储组件包括料箱，所述料箱内设置有横杆，所述横杆上设置有旋转电机，所述旋转电机与转盘连接，所述上料组件包括若干轨道，所述轨道设置于所述料箱内，所述轨道内设置有物料传感器，所述物料传感器与计量器连接，所述料箱通过下料管与釜体贯通。
  3. 如权利要求2所述的电磁反应釜，其特征在于：所述转盘上设置有若干孔道，所述孔道与挡球滑动连接，所述挡球通过弹簧与所述孔道连接。
  4. 如权利要求1所述的电磁反应釜，其特征在于：所述电磁反应机构包括驱动电机，所述驱动电机设置于所述釜体上，所述驱动电机通过传动组件与转杆连接，所述转杆上设置有若干搅拌轴，所述搅拌轴上设置有电磁线圈，所述电磁线圈与导线连接。
  5. 如权利要求4所述的电磁反应釜，其特征在于：所述传动组件包括相互啮合的主动锥齿和从动锥齿，所述主动锥齿与所述驱动电机连接，所述从动锥齿与所述转杆连接。
  6. 如权利要求4所述的电磁反应釜，其特征在于：所述搅拌轴为U形搅拌轴，所述驱动电机外侧设置有防护罩。
  7. 如权利要求1所述的电磁反应釜，其特征在于：所述釜体内设置有加热组件。
  8. 如权利要求7所述的电磁反应釜，其特征在于：所述加热组件包括腔室，所述腔室设置于所述釜体内壁上，所述腔室内设置有加热液，所述腔室内设置有电热管。
  9. 如权利要求1～8中任一项所述的电磁反应釜，其特征在于：还包括若干支脚，所述支脚设置于所述釜体底部，所述釜体上设置有侧料管。
  10. 一种对权利要求1～9中任一项所述的电磁反应釜的应用，其特征在于：将所述电磁反应釜应用于磁性微球合成。
PCT/CN2022/137780 2022-03-21 2022-12-09 一种电磁反应釜及其应用 WO2023179101A1 (zh)

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005022707A1 (de) * 2005-05-18 2006-11-23 Degussa Ag Verfahren und Vorrichtung zur Phasenumwandlung von Stoffen
JP2007064688A (ja) * 2005-08-29 2007-03-15 Toyo Seiki Kk 液体定量供給装置
CN212524106U (zh) * 2020-06-17 2021-02-12 怀化学院 一种光催化剂制备用反应釜
CN213102161U (zh) * 2020-07-16 2021-05-04 开化诚信树脂有限公司 一种松香树脂加工设备
CN214514604U (zh) * 2020-09-07 2021-10-29 福建省建阳金石氟业有限公司 一种投料可控的化学反应釜
CN214810884U (zh) * 2021-06-25 2021-11-23 杭州映山花颜料化工有限公司 一种用于颜料生产的偶合反应釜
CN215234172U (zh) * 2021-05-25 2021-12-21 邵武永太高新材料有限公司 一种二氯六氟磷酸与氟化锂合成反应的密封装置
CN215693904U (zh) * 2021-09-03 2022-02-01 济凡生物科技（北京）有限公司 一种磁性微球制备与纯化的电磁反应釜

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005022707A1 (de) * 2005-05-18 2006-11-23 Degussa Ag Verfahren und Vorrichtung zur Phasenumwandlung von Stoffen
JP2007064688A (ja) * 2005-08-29 2007-03-15 Toyo Seiki Kk 液体定量供給装置
CN212524106U (zh) * 2020-06-17 2021-02-12 怀化学院 一种光催化剂制备用反应釜
CN213102161U (zh) * 2020-07-16 2021-05-04 开化诚信树脂有限公司 一种松香树脂加工设备
CN214514604U (zh) * 2020-09-07 2021-10-29 福建省建阳金石氟业有限公司 一种投料可控的化学反应釜
CN215234172U (zh) * 2021-05-25 2021-12-21 邵武永太高新材料有限公司 一种二氯六氟磷酸与氟化锂合成反应的密封装置
CN214810884U (zh) * 2021-06-25 2021-11-23 杭州映山花颜料化工有限公司 一种用于颜料生产的偶合反应釜
CN215693904U (zh) * 2021-09-03 2022-02-01 济凡生物科技（北京）有限公司 一种磁性微球制备与纯化的电磁反应釜

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