WO2016101933A2 - 金花捷报精品油 - Google Patents

金花捷报精品油 Download PDF

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WO2016101933A2
WO2016101933A2 PCT/CN2016/072616 CN2016072616W WO2016101933A2 WO 2016101933 A2 WO2016101933 A2 WO 2016101933A2 CN 2016072616 W CN2016072616 W CN 2016072616W WO 2016101933 A2 WO2016101933 A2 WO 2016101933A2
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oil
temperature
product
jiebao
jinhua
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PCT/CN2016/072616
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English (en)
French (fr)
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WO2016101933A3 (zh
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董文佳
李建波
李文一
杨苏睿
王建树
王亚伦
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王亚伦
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Priority to PCT/CN2016/072616 priority Critical patent/WO2016101933A2/zh
Publication of WO2016101933A2 publication Critical patent/WO2016101933A2/zh
Publication of WO2016101933A3 publication Critical patent/WO2016101933A3/zh

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  • the invention belongs to the field of food development and relates to a multi-type natural vitamin E oil product.
  • Jinhua Jiebao is a non-toxic plant.
  • Jinhua Jiebao is the name of the Chinese herbal medicine. It is published in the Dictionary of Chinese Medicine, published by the Shanghai Science and Technology Press in 1995. It is published in the 2075 page 4252 and 4254. The scientific name is Abelmoschus. Manihot (Linn.) Medicus], the code in the code of the national standard "Chinese Plant Classification and Code" GB/T14467-93 is 6000010003.
  • Hass is a Chinese herbal medicine, the Hazel oil isolated from the Hazel, there are proteins, carbohydrates, etc., the latter generally accounted for more than 30%.
  • the price in Tong Ren Tang is about 20,000 yuan / kg.
  • Ganoderma lucidum cytoplasmic oil In recent years, Chinese herbal medicine products circulating in the city include Ganoderma lucidum cytoplasmic oil and sea buckthorn oil.
  • Ganoderma lucidum spore oil is priced at 360,000 yuan/kg in the market, but its impurity content and de-doping process are not known.
  • Seabuckthorn oil is divided into seabuckthorn seed oil and seabuckthorn fruit oil. There are many articles on seabuckthorn oil production, but no report on how to make essential oil.
  • the essential oils named after many famous Chinese medicines except the volatile oils such as rose essential oil and spearmint oil, are not essential oils in the volatile oil, and their oils are not in the corresponding Chinese herbal medicine cells.
  • the obtained oil is obtained by using another conventional edible medium vegetable oil as a carrier and immersing in the corresponding Chinese medicinal material.
  • the premium oil of the present invention is a fatty oil which has a fundamental classification of the molecular structure and oil components of the volatile oil. None of the oils isolated from the plant cells of Jinhua Jiebao are free of impurities.
  • the categories of impurities include proteins, cellulose, carbohydrate clusters, heavy metal clusters, etc. Separation of impurities, and the maximum process to maintain the content of useful components in the oil, but also to maintain its stability, such as oil temperature control, no acid-base contact requirements, etc. have not seen the open literature.
  • the object of the present invention is to provide a Jinhua Jiebao boutique oil, which is characterized in that the hair oil directly obtained from the Jinhua Jiebao seed or the Jinhuajie newspaper flower or the golden flower, the flower, and the hair oil which are only disposed and disposed, Control oil temperature, remove impurities by filtration or centrifugal separation process; oil temperature control is based on different boiling temperature of different hair oil, multiply this base by 57%, the obtained temperature is the highest temperature control value of oil temperature, after removal The temperature of the oil in the impurity process is below this maximum temperature control value.
  • the pressure for pressurizing it is controlled to 4.7 kg/cm 2 or less.
  • mesh membranes or filter tubes Used to filter oil fluids are mesh membranes or filter tubes made of metal or organic materials or ceramic materials. These membranes or filter tubes do not contain activated carbon or ion adsorbents in conventional techniques.
  • Oils are not exposed to acidic or alkaline materials during heating and filtration operations.
  • the filtered essential oil is input into the storage container within 12 hours, and stored in the dark.
  • the filter membrane and filter tube in the operation process are replaced and cleaned, and no acidic or alkaline cleaning solution is used.
  • the product is used as a raw material for pharmaceuticals, foods, cosmetics and other products.
  • the target hair oil for carrying out the present invention is an impurity-containing oil separated from the seeds of Jinhuajiebao or flower cells, and is an impurity-containing fatty oil, that is, an animal fat oil containing impurities.
  • the process of separating the hair oil from the cells can be obtained by any of the methods provided by known techniques, for example, the first section of the fifth chapter of the book "Introduction to Seabuckthorn Oils" published by Northwestern University Press in 1997. The methods of the second quarter, the fourth quarter, and the fifth quarter.
  • the apparatus for carrying out the invention, the process requirements in operation are all conventional equipment and conventionally available on the market provided by known techniques.
  • Technology but pay special attention to the application of equipment and processes that are continuously operated in conjunction with degumming, deacidification, decolorization, deodorization, dewaxing, winterization, ammoniation, etc., as published by the Agricultural Press in 1988.
  • the second section of Chapter 7 of the book "Oil Extraction and Processing" edited by Wuxi Institute of Light Industry can be used as reference.
  • the second to fifth sections are not applicable.
  • oil is directed to the production of essential oils, which contain impurities such as fatty oil, also known as hair oil.
  • oil fluid and “hair oil in fluid” are terms for describing the dynamics and morphology of the oil during operation. It means the oil in the flow processing and the state in which the oil is in the flow processing.
  • the invention relates to the oil and fat separated from the cells of the Chinese herbal medicine of Jinhua Jiebao, and calculates the oil temperature control in the method for removing impurities by using the boiling point of the oil as the base; thereby maximally ensuring the content and quality of the active ingredients in the oil and fat.
  • the molecular formula of natural active vitamin E in oils and fats is more than four types, and the left-handed molecular type is about 70%.
  • the total content, especially in terms of stability, is far superior to the seabuckthorn oil promoted by NASA for medicine. Food The choice of raw materials for the products and cosmetics industry.
  • the 100kg of the hair oil obtained from the Jinhua Jiebao Flower Lv was processed by centrifugation method to prepare Jinhua Jiebao Fine Oil. Because the moisture content of the oil is as high as 20%, the oil is first heated to 120 ° C, and the water in the oil is evaporated to remove the water. Note that in this process, the oil in the oil is more, in order to avoid the active substances in the oil. Impurity reaction suffers loss, the temperature of evaporating water process should not be higher, the oil temperature is controlled below 110 °C, after the water is evaporated, 92kg of hair oil is obtained, and the 92kg hair oil is immediately cooled down to 60 °C.
  • the amount of processed oil is not large, and no pressure is applied during the filtration. Only the fluid mechanics common sense is used, and the filtered fat oil is taken under the filter device, and the grease flows smoothly due to the difference in the position.
  • the oil obtained from the Jinhua Jiebao seed by pressing method was used.
  • the oil has a boiling point of 160 ° C, indicating that it contains a considerable amount of impurities, and thus the degree of damage to the active ingredients in the hair oil is much greater.
  • the temperature is 70 ° C, in the shortest period of time, reduce the retention time of impurities in the oil, immediately put into the filter tank to carry out filtration, and at the same time start the pressure pump pressure, pressure control Above and below 3kg/cm 2 .
  • 260 kg of fine oil was obtained, and 40 kg of oily impurities were separated.
  • the oil-containing impurities are relatively sealed, and when the production accumulation reaches more than 100kg, they are combined and heated to 38°C-60°C, and then placed in a filter tank and treated under pressure of 4kg/cm 2 . According to past experience, 100kg of such impurities are included. Still can get about 18kg of fat.

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  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Edible Oils And Fats (AREA)

Abstract

本发明涉及一种多型天然维生素E油制品。金花捷报做为植物中药材名,是一种无毒植物，本发明是把从金花捷报中药材细胞中分离的油脂，以油品沸点为基数，计算确定去除杂质法中的油温控制；从而最大限度地保障了油脂中活性成分的含量和质量。油脂中天然活性维生素E的分子式为四种以上类型，左旋式分子类型达70%左右，总含量，特别是以稳定性比较总含量远远优于美国宇航局推崇的沙棘油，用于医药、食品、香妆品产业做原料的选择。

Description

金花捷报精品油 技术领域
本发明属于食品开发领域，涉及一种多型天然维生素E油制品。
背景技术
金花捷报是一种无毒植物，金花捷报做为植物中药材名，见诸1995年上海科学技术出版社出版的《中药大辞典》2075页4252、4254号辞目，学名是黄蜀葵[Abelmoschus manihot(Linn.)Medicus]，在国家标准《中国植物分类与代码》GB/T14467-93的编码中的编码是6000010003。
从中药材中分离出油脂食用，古已有之，但以去杂质的精油定位者，特别是列明工艺参数做精油者，罕见。如：哈士蟆是味中药材，从哈士蟆分离出的哈士蟆油，有蛋白质、碳水化物等，后者占比例一般在30％以上。但它做为成品，在同仁堂的售价是2万元/公斤左右。
近些年流通于市的中药材制品油有灵芝胞子油、沙棘油。灵芝胞子油在市场售价折合36万元/公斤，但它的杂质含量及去杂工艺，却不为人知。沙棘油分沙棘籽油和沙棘果油两种，沙棘油的制取文献不少，但在怎样制做精油上，没见报导。
市场上，特别是化妆品市场上，以诸多中药名子命名的精油，除玫瑰精油、留兰香精油之类的挥发性油外，不在挥发油之列的精油，其油脂不是相应中药材细胞中所制得的油品，而是用另外的常规食用介质植物油做载体，浸入相应中药材后制得。
中药经典中，直接以中药名加油字记载的条目中，都是只记什么科植物的什么收获物的脂肪油等，没有有关精品油加工的内容。如：中药大辞典3321号词目的山茶油，以及麻油等。至于利用现代工艺从中药制得的，广泛应用的一类油，如薄荷油等，属于挥发油一类。
本发明的精品油是属于脂肪油，它和挥发油在分子结构和油的组分上有根本的类别区分。从金花捷报这种植物细胞中分离出的油脂，没有一种是不含杂质的，杂质的类别有蛋白质、纤维素、碳水化合物分子团、重金属分子团等，就从最大限度上，把这些杂质分离出来，及最大限度的既保持油品中有用成分含量，又保持其稳定的工艺，如油温控制、无酸碱接触要求等没见公开文献。
发明内容
本发明目的是提供一种金花捷报精品油，其特征是对从金花捷报种子或金花捷报花中直接制得的毛油或对只做沉降处置的金花捷报花、种毛油，控制油温，用过滤或离心分离工艺去除杂质；油温的控制是以不同毛油的不同沸点温度为基数，用这个基数乘以57％，所得温度是油温的最高温度控制数值，在去除杂质工艺中的油品温度要在这个最高温度控制数值以下。
毛油加压过滤时，对其加压的压力控制在4.7kg/cm2以下。
用于滤过油品流体的是金属或有机材料或陶瓷材料制做的网膜或滤管，这些网膜或滤管中，不含常规技术中的活性炭或离子吸附物。
油品在加温和滤过作业时，不接触酸性或碱性物品。
滤清后的成品精油在12小时内输入贮运容器，避光贮运。
对作业流程中的滤网膜、滤管更换清理，不使用显酸性或碱性清洗液。
产品的用途是做为药品、食品、香妆品等制品的原材料。
实施本发明应明白的要素是：
实施本发明的标的物毛油，是从金花捷报种子或花细胞中分离出的含杂质油脂，是含杂质脂肪油，即含杂质植物脂肪油。从细胞中分离毛油的工艺，可以是任何一种已知技术所提供的方法制得，如，1997年西北大学出版社出版的《沙棘油脂概论》一书第五章中第一节、第二节、第四节、第五节的方法。
除发明中所专门提及的油温控制，压力控制、及相关特别要求外，实施本发明的设备，操作中工艺要求，均采用已知技术所提供的、市场上有供应的常规设备和常规技术，但要特别注意，千万不要应用与脱胶、脱酸、脱色、脱臭、脱腊、冬化、氨化等工艺相联而连续作业的设备和工艺，如1988年农业出版社出版的，无锡轻工业学院编的《油脂提取与加工》一书中第七章第二节可参考使用，第二节至第五节就不可参考应用等。
上文中“油品”的指向是制成成品精油前，在制成工艺流程中含杂质脂肪油，也称毛油。
上文中“油品流体”，“毛油呈流体”是对操作中油品动态、形态的描述用语，其意思也是流动加工中的毛油，毛油在流动加工的状态等。
本发明是把从金花捷报中药材细胞中分离的油脂，以油品沸点为基数，计算确定去除杂质法中的油温控制；从而最大限度地保障了油脂中活性成分的含量和质量。油脂中天然活性维生素E的分子式为四种以上类型，左旋式分子类型达70％左右，总含量，特别是以稳定性比较总含量远远优于美国宇航局推崇的沙棘油，用于医药、食 品、香妆品产业做原料的选择。
具体实施方式
实施例1
受委托，对100kg用离心方法，从金花捷报鲜花吕制得的毛油做加工，制备金花捷报精品油。因该毛油含水分高达20％，先行把毛油加热到120℃，蒸发去掉毛油中水分，注意这一过程时向段中，油品中水分较多，为避免毛油中活性物质与杂质反应遭受损失，蒸发水分过程温度不宜再高，油温控制在110℃以下，待蒸发完水分后，得到毛油92kg，马上对这92kg毛油降温，直至降温到60℃。从此92kg毛油中取0.5kg，置试验室用烧瓶中，用工业温度计或红外线测温仪，检测该毛油沸点。这样的检测是考虑到毛油的原料性状差异，毛油制得方法不同，其所含杂质的差异会造成其沸点有差异，所以对每一批次毛油都要测沸点。这个沸点做为加工过程油温控制计算基数的重要性在于，沸点的高低表明毛油杂质含量的多少和毛油特性，依此基数做计算确定毛油加工中温度的控制，是为了减少毛油中活性物质的损失。
经检测，上述92kg毛油的沸点是180℃。确定加工艺中的油温应在180℃×57％＝103.6℃以下。
此时，把检测使用的0.5kg毛油放入正在降温的91.5kg毛油中，测该毛油温度已降至48℃，即行对其进行过滤作业。
作业中，因加工毛油量不大，在过滤中，没有施行加压，只是利用流体力学常识，在过滤设备下方接取滤过的脂肪油，由于位差，油脂流出顺利。
操作结束，分离杂质0.3kg，得精品油91.3kg，差数是油耗。因批量小，做油耗比例显高。
实施例2
对300kg用压榨法从金花捷报种子制得的毛油进行作业。该毛油检测沸点是160℃，表明其含杂质相当多，从而对毛油中活性成分的危害程度也大的多。
操作中，计算，160℃×57＝91.2℃确定油温。时油温因刚制得运来，温度在70℃，为在最短时间段，减少杂质在毛油中的留存时间，立即置入过滤槽中实施过滤，同时开动加压泵加压，压力控制在3kg/cm2上下。作业结束制得精品油260kg，分离出含油杂质40kg。对含油杂质相对密封，留待生产积累达100kg以上数量时，再合并加温至38℃—60℃，然后放置过滤槽中，以4kg/cm2加压处置，按以往经验，100kg此类杂质中，仍可得18kg左右油脂。

Claims (7)

  1. 本发明提供一种金花捷报精品油，其特征是：对从金花捷报种子或金花捷报花中直接制得的毛油或对只做沉降处置的金花捷报花、种毛油，控制油温，用过滤或离心分离工艺去除杂质；油温的控制是以不同毛油的不同沸点温度为基数，用这个基数乘以57％，所得温度是油温的最高温度控制数值，在对毛油去除杂质工艺中的油品温度，要在这个最高温度控制数值以下。
  2. 权利要求1所述产品，毛油加压过滤时，对其加压的压力控制在4.7kg/cm2以下。
  3. 权利要求1所述产品用于滤过油品流体的是：金属或有机材料或陶瓷材料制作的网膜或滤管，这些网膜或滤管中，不含常规技术中的活性炭或离子吸附物。
  4. 权利要求1所述产品，油品在加温和滤过作业时，不接触酸性或碱性物品。
  5. 权利要求1所述产品滤清后的成品精油在12小时内输入贮运容器，避光贮运。
  6. 权利要求1所述产品对作业流程中的滤网膜、滤管更换清理，不使用显酸性或碱性清洗液。
  7. 权利要求1所述产品的用途是做为药品、食品、香妆品等制品的原材料。
PCT/CN2016/072616 2016-01-28 2016-01-28 金花捷报精品油 WO2016101933A2 (zh)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115178012A (zh) * 2022-07-12 2022-10-14 吉水县金海天然香料油科技有限公司 一种化妆品用茶油加工设备及其精制工艺

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Publication number Priority date Publication date Assignee Title
CN1057115C (zh) * 1990-12-10 2000-10-04 王绍璋 黄蜀葵油脂的制取与加工方法
CN100497568C (zh) * 2003-02-26 2009-06-10 张英梅 葵油
CN103881803A (zh) * 2012-12-20 2014-06-25 宽甸辰阳山珍食品开发有限公司 一种苏籽油的制备方法
CN103875824B (zh) * 2012-12-20 2016-09-14 宽甸辰阳山珍食品开发有限公司 一种核桃油的制备方法
CN104342282B (zh) * 2013-07-23 2017-05-10 台建祥 一种利用黄蜀葵制备功能油脂及活性蛋白粉的方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115178012A (zh) * 2022-07-12 2022-10-14 吉水县金海天然香料油科技有限公司 一种化妆品用茶油加工设备及其精制工艺
CN115178012B (zh) * 2022-07-12 2024-05-03 吉水县金海天然香料油科技有限公司 一种化妆品用茶油加工设备及其精制工艺

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