WO2016068219A1 - 潤滑剤及び軸受装置、並びに潤滑剤供給装置 - Google Patents
潤滑剤及び軸受装置、並びに潤滑剤供給装置 Download PDFInfo
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- WO2016068219A1 WO2016068219A1 PCT/JP2015/080467 JP2015080467W WO2016068219A1 WO 2016068219 A1 WO2016068219 A1 WO 2016068219A1 JP 2015080467 W JP2015080467 W JP 2015080467W WO 2016068219 A1 WO2016068219 A1 WO 2016068219A1
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- lubricant
- wax
- bearing
- lubricating oil
- temperature
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/02—Mixtures of base-materials and thickeners
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M171/00—Lubricating compositions characterised by purely physical criteria, e.g. containing as base-material, thickener or additive, ingredients which are characterised exclusively by their numerically specified physical properties, i.e. containing ingredients which are physically well-defined but for which the chemical nature is either unspecified or only very vaguely indicated
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M171/00—Lubricating compositions characterised by purely physical criteria, e.g. containing as base-material, thickener or additive, ingredients which are characterised exclusively by their numerically specified physical properties, i.e. containing ingredients which are physically well-defined but for which the chemical nature is either unspecified or only very vaguely indicated
- C10M171/02—Specified values of viscosity or viscosity index
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16N—LUBRICATING
- F16N11/00—Arrangements for supplying grease from a stationary reservoir or the equivalent in or on the machine or member to be lubricated; Grease cups
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16N—LUBRICATING
- F16N39/00—Arrangements for conditioning of lubricants in the lubricating system
- F16N39/04—Arrangements for conditioning of lubricants in the lubricating system by heating
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16N—LUBRICATING
- F16N7/00—Arrangements for supplying oil or unspecified lubricant from a stationary reservoir or the equivalent in or on the machine or member to be lubricated
- F16N7/30—Arrangements for supplying oil or unspecified lubricant from a stationary reservoir or the equivalent in or on the machine or member to be lubricated the oil being fed or carried along by another fluid
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16N—LUBRICATING
- F16N7/00—Arrangements for supplying oil or unspecified lubricant from a stationary reservoir or the equivalent in or on the machine or member to be lubricated
- F16N7/38—Arrangements for supplying oil or unspecified lubricant from a stationary reservoir or the equivalent in or on the machine or member to be lubricated with a separate pump; Central lubrication systems
- F16N7/385—Central lubrication systems
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/14—Synthetic waxes, e.g. polythene waxes
- C10M2205/146—Synthetic waxes, e.g. polythene waxes used as thickening agents
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
- C10M2205/166—Paraffin waxes; Petrolatum, e.g. slack wax used as thickening agent
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/18—Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras
- C10M2205/186—Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras used as thickening agents
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/2805—Esters used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/282—Esters of (cyclo)aliphatic oolycarboxylic acids
- C10M2207/2825—Esters of (cyclo)aliphatic oolycarboxylic acids used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
- C10N2020/01—Physico-chemical properties
- C10N2020/011—Cloud point
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/02—Bearings
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/10—Semi-solids; greasy
Definitions
- the present invention relates to a lubricant supplied to a bearing or the like.
- the present invention also relates to a bearing device including a bearing and a lubricant supply device that supplies the lubricant to the bearing, and a lubricant supply device for supplying the lubricant stored therein to the bearing.
- a predetermined amount of lubricant is periodically supplied to a bearing device 10 for supporting a spindle of a machine tool from a lubricant supply device 1 provided outside to a bearing 3 through a supply pipe 2.
- a lubricant supply device 1 provided outside to a bearing 3 through a supply pipe 2.
- an intermittent supply system for supplying lubricant is employed.
- a grease composition is generally used because lubrication can be maintained for a long time.
- the grease composition supplied to the bearing 3 is extremely small, the grease composition having a low consistency and a relatively hard grease composition has a long piping route, the piping route is bent in the middle, or perpendicularly.
- the present applicant has devised the structure of the lubricant supply device 1 in Patent Document 1 so as to stably supply the grease composition, but until the thickener of the grease composition is solidified. Is not solved.
- the object of the present invention is to provide a stable supply of the lubricant from the lubricant supply device to the bearing without the problem that the thickener separates from the base oil and hardens or solidifies unlike the grease composition.
- the present invention provides the following lubricant and bearing device, and a lubricant replenishing device for the bearing.
- the lubricating oil and the wax are contained in a ratio of 90 to 60% by mass of the lubricating oil and 10 to 40% by mass of the wax with respect to the total amount of both, and in the range of 10 to 70 ° C.
- a lubricant characterized by becoming liquid at a predetermined temperature.
- the lubricant according to (1) above which becomes semi-solid when the temperature becomes lower than the temperature at which it becomes liquid.
- the lubricant according to (1) or (2) above wherein the change in state between liquid and semi-solid is reversible.
- a bearing device comprising a bearing, a lubricant supply device for supplying a lubricant to the bearing, and a pipe connecting the bearing and the lubricant supply device,
- the lubricant supply device stores the lubricant according to any one of the above (1) to (6), distributes the lubricant in a semi-solid state through the pipe, and supplies the lubricant to the bearing.
- a bearing device characterized in that the agent is supplied in a liquid state.
- a lubricant supply device provided outside the bearing for storing the lubricant and supplying the lubricant to the bearing through a pipe, A lubricant supply device that stores the lubricant according to any one of (1) to (6) and discharges the lubricant in a semi-solid state to the pipe.
- the bearing device of the present invention also has a longer life than the grease supply method because the wax-based lubricant is stably supplied from the lubricant supply device for a long period of time.
- FIG. 1 It is a schematic diagram showing a bearing device for supporting a spindle of a machine tool as an example of a lubricant supply system. It is a figure for demonstrating a liquefaction point. It is a graph which shows the result of having measured the temperature change of the viscosity about the wax-type lubricant prepared in Example 1. FIG. It is a graph which shows the result of having measured the temperature change of the moving amount
- the bearing device is not limited as long as the bearing and the lubricant supply device are connected by piping.
- a bearing device 10 for supporting a spindle of a machine tool as illustrated in FIG. 1 is illustrated. be able to.
- Lubricant supply device 1 is not limited as long as the lubricant supply device 1 is configured to periodically discharge a stored lubricant to the supply pipe 2 in a constant amount. That is, the lubricant supply device 1 of the present invention includes a tank for storing the wax-based lubricant, a pressure feeding means for periodically discharging the wax-based lubricant from the tank to the supply pipe 2 at regular intervals.
- the specific structure can be based on a conventional lubricant supply device.
- the wax-based lubricant is ejected from the lubricant supply device 1 in a semi-solid state and moves in a semi-solid state within the supply pipe 2, but the wax-based lubricant is basically composed of lubricating oil and wax. Since it is a component, it has lubricity, is semi-solid, and wax functions as a thickener for grease, so that it can be adequately handled by a conventional lubricant supply device for a grease composition.
- ⁇ Wax lubricants contain lubricating oil and wax as basic components.
- the wax is solidified or semi-solidified at a temperature lower than its melting point, becomes a liquid at a temperature higher than the melting point, and has fluidity.
- the wax-based lubricant of the present invention is a mixture of lubricating oil (liquid) and wax (semi-solid) (corresponding to a dilute solution obtained by adding lubricating oil (dilute liquid) to wax (solute)).
- the wax-based lubricant changes from a semisolid state to a liquid state at a temperature lower than the melting point of the wax.
- the temperature at which a semi-solid state changes to a liquid state (hereinafter referred to as “liquefaction point”) is closely related to the melting point of the wax contained and the mixing ratio with the lubricating oil. That is, since “the melting point of the wax> the liquefaction point”, the liquefaction point can be controlled to a predetermined temperature below the melting point of the wax by the mixing ratio of the contained wax and the lubricating oil. Specifically, the temperature difference between the liquefaction point and the melting point of the wax can be set to about 10 to 30 ° C.
- the lubricating oil and the wax depending on the types of the lubricating oil and the wax and the mixing ratio of the two. Further, by adjusting the type of wax contained, the mixing ratio with the lubricating oil, and the like, it can be reversibly changed between a liquid state and a semi-solid state according to the temperature.
- the liquid and liquefaction points are confirmed as shown in FIG. 2 and below.
- This method is in accordance with the regulations on dangerous goods regulations in Japan, Chapter 12 Miscellaneous Article 69-2 (Liquid Definition).
- (1) Put a test article (wax-based lubricant) up to two test tubes (diameter 30 mm, height 120 mm) A line (height 55 mm).
- (2) Seal one test tube (liquid determination test tube) with a rubber plug without a hole.
- the other test tube (temperature measurement test tube) is sealed with a rubber stopper equipped with a thermometer. The thermometer is inserted so that its tip is 30 mm deep from the surface of the test article, and is upright with respect to the test tube.
- test tubes are immersed in a thermostatic bath maintained at a liquid confirmation temperature of ⁇ 0.1 ° C. so that the B line (30 mm above the surface of the test article) is submerged under the water surface of the thermostatic bath. Let stand upright. (5) The state of the test article in the temperature measurement test tube is maintained as it is for 10 minutes after the liquid confirmation temperature becomes ⁇ 0.1 ° C. (6) Remove the liquid judgment test tube from the constant temperature water tank while standing upright on a horizontal table, immediately lay down horizontally on the table, and measure the time until the tip of the test article reaches line B. (7) When the time until the test article reaches line B is within 90 seconds, it is determined that the test article is “liquid”.
- the liquefaction point is not a fixed point temperature such as the freezing point of water (0 ° / pure water, under atmospheric pressure), but is defined and quantified in a range of about ⁇ 2 ° C. with respect to a specific temperature. .
- a liquid wax-based lubricant is caused to flow through a supply port provided in the outer ring of the bearing 3.
- a cooling pipe is arranged around the outer ring in the housing so that the bearing is not seized and cooled so that the bearing temperature is about 40 to 50 ° C. during operation. Yes.
- the wax-based lubricant from the lubricant supply device 1 needs to change into a liquid state immediately before the supply port provided in the outer ring of the bearing 3 at least inside the supply pipe 2 through the supply pipe 2 in a semi-solid state.
- the liquefaction point is defined as 10 to 70 ° C.
- the supplied wax-based lubricant is liquid. Since the wax-like lubricant does not contain a thickening agent and both the lubricating oil and the wax are lubricating components, it becomes the same state as the proportion of the base oil in the grease composition is increased, and the lubricating performance is higher than that of the grease composition. Rise. Therefore, since the replenishment amount per time can be reduced and the replenishment interval can be lengthened, the consumption amount of the wax-based lubricant can be reduced, and the entire lubricant replenishment system has a long life.
- the wax-based lubricant does not contain a thickening agent like the grease composition, it does not solidify even when pressure is applied, and stable supply can be made even if the supply pipe 2 is long or has a bent part. become.
- the wax-based lubricant is sent from the bearing 3 through the discharge pipe 4 to the outside of the housing.
- the discharge pipe 4 is exposed to the outside air (room temperature)
- the wax-based lubricant is It changes from liquid to semi-solid again.
- a residue derived from the thickener is generated by long-term use, and the air flow is blocked, which can contribute to an increase in the temperature of the bearing.
- the wax-based lubricant is discharged in a liquid state up to a certain distance after being discharged from the bearing 3, such a problem does not occur.
- the wax-based lubricant is composed mainly of a lubricating oil and a wax, but both the lubricating oil and the wax have sufficient lubricity and are liquid at 10 to 70 ° C. at a lower temperature. As long as it changes to a semi-solid state, both types are not limited. Moreover, preferably, it adjusts so that it may change into a liquid and a semi-solid reversibly with temperature.
- lubricating oil various lubricating oils conventionally used for bearing lubrication can be used.
- paraffinic or naphthenic mineral oil, or synthetic oil such as ester oil, hydrocarbon oil, ether oil, or the like can be used, and a plurality of types can be mixed and used.
- the viscosity may be in a general range, but considering the lubricity of the bearing 3, the kinematic viscosity at 40 ° C. is preferably 5 to 200 mm 2 / s.
- the kinematic viscosity of the lubricating oil is set according to the application of the bearing. For example, when it is desired to achieve both a low temperature rise characteristic and seizure resistance, such as a spindle bearing of a machine tool, 10 to 130 mm 2 / s (40 ° C).
- the wax is an organic substance having an alkyl group that is solid or semi-solid at room temperature.
- natural wax or synthetic wax may be used. However, since it becomes a mixture with lubricating oil inside a bearing, a thing with high compatibility with lubricating oil is preferable.
- Natural waxes include animal / plant waxes, mineral waxes, and petroleum waxes.
- Synthetic waxes include Fischer-Tropsch wax, polyethylene wax, oil-based synthetic waxes (esters, ketones, amides), hydrogenated waxes, and the like. It is also possible to use a mixture of a plurality of types.
- the liquefaction point of the wax-based lubricant is substantially determined by the mixing ratio of the melting point of the wax and the lubricating oil
- the wax exemplified above is selected so that the liquefaction point is 10 to 70 ° C.
- lubricating oil and wax are prepared at an appropriate mixing ratio.
- the liquefaction point which is the liquefaction temperature, is preferably set according to the application of the bearing. For example, in a machine tool bearing, it is preferably set to a predetermined temperature in the range of 30 to 70 ° C.
- microcrystalline wax can be used as the wax.
- the mixing ratio of the lubricating oil and the wax is preferably 10 to 40% by mass of the wax and 90 to 60% by mass of the lubricating oil with respect to the total amount of both.
- the wax ratio increases, the fluidity when the wax-based lubricant is in a semi-solid state deteriorates, and when it exceeds 40% by mass, the dischargeability from the lubricant supply device 1 and the transportability in the supply pipe 2 deteriorate.
- the mixing ratio of the wax is 10% by mass or more and less than 20% by mass and the mixing ratio of the lubricating oil is 90% by mass or more and more than 80% by mass.
- the wax may be added as an oiliness improver for lubricating oil or grease.
- the amount of wax added is larger than the general additive amount as described above. Therefore, the semi-solid property (function as a thickener) equivalent to that of grease is retained.
- the microcrystalline wax has a melting point of 67 to 98 ° C.
- the wax-based lubricant mixed with the lubricating oil in the above mixing ratio has a liquefaction point of 35 to 50 ° C. within a predetermined temperature range.
- Can be set to Paraffin wax has a melting point of 47 to 69 ° C., but the wax-based lubricant mixed with the lubricating oil at the above mixing ratio should set the liquefaction point to a predetermined temperature in the range of 20 to 35 ° C. Can do.
- additives can be added to the wax-based lubricant depending on the purpose.
- an appropriate amount of a known antioxidant, rust inhibitor, extreme pressure agent or the like can be added.
- the wax In order to prepare a wax-based lubricant, the wax is heated to a temperature equal to or higher than the melting point to form a liquid, to which a lubricating oil or a lubricating oil to which an additive has been added is added and thoroughly mixed, and then a temperature below the melting point of the wax. What is necessary is just to cool to (usually below a liquefaction point).
- the lubricating oil or lubricating oil to which additives are added and solid wax are put in a suitable container, the whole is heated and mixed to a temperature above the melting point of the wax, and then cooled to a temperature below the liquefaction point. May be.
- the wax-based lubricant of the present invention is particularly preferably used for ball bearing lubrication.
- the ball rotates with the contact angle line as the equator.
- the ball exhibits a pumping effect, and an air current is generated in a space in which the lubricant is enclosed. Therefore, by using a wax-based lubricant having good fluidity, it is possible to prevent the lubricant from staying in the bearing and to prevent the temperature of the bearing from rising.
- Example 1 Preparation of wax-based lubricant
- Diester oil dioctyl sebacate
- microcrystalline wax melting point 82 ° C.
- the mixture was mixed at a temperature equal to or higher than the melting point of the wax and naturally cooled to room temperature to obtain a wax-based lubricant.
- Example 2> Preparation of wax-based lubricant 83% by mass of diester oil (dioctyl sebacate), 10.5% by mass of microcrystalline wax (melting point 72 ° C.), and a mixture containing an antioxidant and an extreme pressure agent as additives at a ratio of 6.5% by mass , Mixed at a temperature above the melting point of the wax, and naturally cooled to room temperature to obtain a wax-based lubricant
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Abstract
Description
(1)潤滑油とワックスとを、両者の合計量に対し、前記潤滑油を90~60質量%、前記ワックスを10~40質量%の割合で含有し、かつ、10~70℃の範囲の所定の温度で液状になることを特徴とする潤滑剤。
(2)液状になる温度よりも低い温度になった際には、半固体状になることを特徴とする上記(1)記載の潤滑剤。
(3)液状と半固体状の状態変化が可逆的であることを特徴とする上記(1)または(2)記載の潤滑剤。
(4)潤滑油を90~80質量%、ワックスを10質量%以上20質量%未満の割合で含有することを特徴とする上記(1)~(3)の何れか1項に記載の潤滑剤。
(5)潤滑油の粘度が5~200mm2/s(40℃)であることを特徴とする上記(1)~(4)の何れか1項に記載の潤滑剤。
(6)潤滑油がエステル油で、ワックスがマイクロクリスタリンワックスであることを特徴とする上記(1)~(5)の何れか1項に記載の潤滑剤。
(7)軸受と、前記軸受に潤滑剤を供給するための潤滑剤供給装置と、前記軸受と前記潤滑剤供給装置とを連結する配管とを備える軸受装置であって、
前記潤滑剤供給装置は上記(1)~(6)の何れか1項に記載の潤滑剤を貯蔵しており、前記潤滑剤を半固体状で前記配管を流通させ、前記軸受には前記潤滑剤を液状に変化させて供給することを特徴とする軸受装置。
(8)潤滑剤を貯蔵し、配管を通じて前記潤滑剤を軸受に供給するために、軸受外部に設けられる潤滑剤供給装置であって、
上記(1)~(6)の何れか1項に記載の潤滑剤を貯蔵し、半固体状で前記配管に吐出することを特徴とする潤滑剤供給装置。
(1)試験物品(ワックス系潤滑剤)を2本の試験管(直径30mm、高さ120mm)のA線(高さ55mm)まで入れる。
(2)一方の試験管(液状判断用試験管)を孔穴の無いゴム栓で密栓する。
(3)他方の試験管(温度測定用試験管)を、温度計を付けたゴム栓で密栓する。尚、温度計は、その先端が試験物品の表面より30mmの深さになるように挿入し、試験管に対して直立させる。
(4)2本の試験管を、液状確認温度±0.1℃に保持された恒温槽中に、B線(試験物品の表面よりも30mm上方)が恒温槽の水面下に没するように直立させて静置する。
(5)温度測定用試験管中の試験物品の温度が液状確認温度±0.1℃になってから、10分間そのままの状態を保持する。
(6)液状判断試験管を恒温水槽から水平な台上に直立したまま取り出し、直ちに台の上に水平に倒し、試験物品の先端がB線に到達するまでの時間を計測する。
(7)試験物品がB線に達するまでの時間が90秒以内であるとき、試験物品が「液状」であると判断する。
(8)そして、恒温水槽の温度を種々変更して(1)~(7)を行い、液状になった温度を「液状化点」とする。
尚、液状化点とは、水の凝固点(0°/純水、大気圧下)のような定点温度ではなく、ある特定温度に対して略±2℃程度の範囲で定義、数値化される。
(ワックス系潤滑剤の調製)
ジエステル油(ジオクチルセバケート)を78.5質量%、マイクロクリスタリンワックス(融点82℃)を15質量%、添加剤として酸化防止剤及び極圧剤を含む混合物を6.5質量%の割合にて、ワックスの融点以上の温度で混合し、室温まで自然冷却してワックス系潤滑剤を得た。
コーンプレート型粘度計(E型粘度計)を用い、温度を変えて上記ワックス系潤滑剤の粘度を測定した。結果を表1及び図3に示すが、温度の上昇とともに粘度が低下し、流動性が高まることがわかる。具体的には、図4に示すように、42℃までは試料表面の移動はなく、44℃で5mm、46℃で17mmの移動が確認され、48℃で50mmを超えて容器の先端まで達した。そのため、実施例1の組成のワックス系潤滑剤は、47℃の液状化点を有している。即ち、47℃付近で半固体状から液状に変化し始め、一般的な工作機械の主軸支持用の軸受装置の潤滑剤補給システムに利用できることがわかる。
(ワックス系潤滑剤の調製)
ジエステル油(ジオクチルセバケート)を83質量%、マイクロクリスタリンワックス(融点72℃)を10.5質量%、添加剤として酸化防止剤及び極圧剤を含む混合物を6.5質量%の割合にて、ワックスの融点以上の温度で混合し、室温まで自然冷却してワックス系潤滑剤を得た
コーンプレート型粘度計(E型粘度計)を用いて、実施例1と同様にして温度を変えて上記ワックス系潤滑剤の粘度を測定した。結果を図5に示すが、実施例2の組成のワックス系潤滑剤は、温度上昇による粘度変化の割合が38℃を境に減少しており、液状化点は38℃付近である。そのため、20~40℃程度で使用される軸受装置の潤滑剤補給システムに利用できることがわかる。
本出願は、2014年10月29日出願の日本特許出願(特願2014-220705)に基づくものであり、その内容はここに参照として取り込まれる。
2 供給管
3 軸受
4 排出管
10 軸受装置
Claims (8)
- 潤滑油とワックスとを、両者の合計量に対し、前記潤滑油を90~60質量%、前記ワックスを10~40質量%の割合で含有し、かつ、10~70℃の範囲の所定の温度で液状になることを特徴とする潤滑剤。
- 液状になる温度よりも低い温度になった際には、半固体状になることを特徴とする請求項1記載の潤滑剤。
- 液状と半固体状の状態変化が可逆的であることを特徴とする請求項1または2記載の潤滑剤。
- 潤滑油を90~80質量%、ワックスを10質量%以上20質量%未満の割合で含有することを特徴とする請求項1~3の何れか1項に記載の潤滑剤。
- 潤滑油の粘度が5~200mm2/s(40℃)であることを特徴とする請求項1~4の何れか1項に記載の潤滑剤。
- 潤滑油がエステル油で、ワックスがマイクロクリスタリンワックスであることを特徴とする請求項1~5の何れか1項に記載の潤滑剤。
- 軸受と、前記軸受に潤滑剤を供給するための潤滑剤供給装置と、前記軸受と前記潤滑剤供給装置とを連結する配管とを備える軸受装置であって、
前記潤滑剤供給装置は請求項1~6の何れか1項に記載の潤滑剤を貯蔵しており、前記潤滑剤を半固体状で前記配管を流通させ、前記軸受には前記潤滑剤を液状に変化させて供給することを特徴とする軸受装置。 - 潤滑剤を貯蔵し、配管を通じて前記潤滑剤を軸受に供給するために、軸受外部に設けられる潤滑剤供給装置であって、
請求項1~6の何れか1項に記載の潤滑剤を貯蔵し、半固体状で前記配管に吐出することを特徴とする潤滑剤供給装置。
Priority Applications (5)
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EP19154829.6A EP3495464A1 (en) | 2014-10-29 | 2015-10-28 | Bearing device |
JP2016556614A JP6668251B2 (ja) | 2014-10-29 | 2015-10-28 | 軸受装置 |
EP15855093.9A EP3214160B1 (en) | 2014-10-29 | 2015-10-28 | Bearing device |
CN201580059551.8A CN107207990A (zh) | 2014-10-29 | 2015-10-28 | 润滑剂和轴承装置、以及润滑剂供给装置 |
KR1020177011754A KR20170094130A (ko) | 2014-10-29 | 2015-10-28 | 윤활제 및 베어링 장치, 그리고 윤활제 공급 장치 |
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JP (1) | JP6668251B2 (ja) |
KR (1) | KR20170094130A (ja) |
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CN106566648A (zh) * | 2016-09-19 | 2017-04-19 | 新疆福克油品股份有限公司 | 废润滑油再生生产线断电自救的补偿装置 |
WO2022071491A1 (ja) * | 2020-09-30 | 2022-04-07 | 協同油脂株式会社 | カーボンナノチューブを含む潤滑剤組成物 |
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CN109899668A (zh) * | 2019-04-01 | 2019-06-18 | 国电联合动力技术有限公司 | 风电机组主轴轴承的润滑补偿方法及系统 |
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- 2015-10-28 KR KR1020177011754A patent/KR20170094130A/ko not_active Application Discontinuation
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- 2015-10-28 EP EP15855093.9A patent/EP3214160B1/en active Active
- 2015-10-28 CN CN201580059551.8A patent/CN107207990A/zh active Pending
- 2015-10-28 WO PCT/JP2015/080467 patent/WO2016068219A1/ja active Application Filing
- 2015-10-28 EP EP19154829.6A patent/EP3495464A1/en not_active Withdrawn
- 2015-10-29 TW TW104135689A patent/TW201627491A/zh unknown
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TW201627491A (zh) | 2016-08-01 |
EP3214160B1 (en) | 2019-03-06 |
CN107207990A (zh) | 2017-09-26 |
EP3495464A1 (en) | 2019-06-12 |
EP3214160A1 (en) | 2017-09-06 |
JP6668251B2 (ja) | 2020-03-18 |
JPWO2016068219A1 (ja) | 2018-01-18 |
KR20170094130A (ko) | 2017-08-17 |
EP3214160A4 (en) | 2017-09-06 |
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