WO2014207947A1 - しごき加工用金型及び成形材製造方法 - Google Patents
しごき加工用金型及び成形材製造方法 Download PDFInfo
- Publication number
- WO2014207947A1 WO2014207947A1 PCT/JP2013/068880 JP2013068880W WO2014207947A1 WO 2014207947 A1 WO2014207947 A1 WO 2014207947A1 JP 2013068880 W JP2013068880 W JP 2013068880W WO 2014207947 A1 WO2014207947 A1 WO 2014207947A1
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- WO
- WIPO (PCT)
- Prior art keywords
- ironing
- punch
- stop
- molding
- shoulder
- Prior art date
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D22/00—Shaping without cutting, by stamping, spinning, or deep-drawing
- B21D22/20—Deep-drawing
- B21D22/28—Deep-drawing of cylindrical articles using consecutive dies
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D22/00—Shaping without cutting, by stamping, spinning, or deep-drawing
- B21D22/20—Deep-drawing
- B21D22/30—Deep-drawing to finish articles formed by deep-drawing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D—WORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21D51/00—Making hollow objects
- B21D51/16—Making hollow objects characterised by the use of the objects
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21J—FORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
- B21J13/00—Details of machines for forging, pressing, or hammering
- B21J13/02—Dies or mountings therefor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21K—MAKING FORGED OR PRESSED METAL PRODUCTS, e.g. HORSE-SHOES, RIVETS, BOLTS OR WHEELS
- B21K23/00—Making other articles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21K—MAKING FORGED OR PRESSED METAL PRODUCTS, e.g. HORSE-SHOES, RIVETS, BOLTS OR WHEELS
- B21K5/00—Making tools or tool parts, e.g. pliers
- B21K5/20—Making working faces of dies, either recessed or outstanding
Definitions
- the present invention relates to a die for ironing for performing ironing on a forming portion and a method for manufacturing a molding material.
- a convex shaped processed part is formed by press forming such as drawing using a surface-treated metal plate such as a plated steel plate as a raw material.
- a surface-treated metal plate such as a plated steel plate as a raw material.
- ironing is performed on the forming portion after the forming portion is formed.
- the clearance between the punch and the die is made narrower than the plate thickness of the forming part before ironing, and the plate surface of the forming part is ironed by the punch and die, This is a processing method in which the plate thickness of the forming portion is matched with the clearance.
- the conventional mold includes a punch and a die.
- the punch is a columnar member having an outer peripheral surface that extends linearly in parallel with the pressing direction into the pressing hole, and is inserted into the forming portion.
- the die has an indentation hole into which the forming portion is pushed together with the punch.
- the indentation hole is disposed at the outer edge of the indentation hole and is formed by a curved surface having a predetermined radius of curvature, and an inner peripheral surface linearly extending in parallel with the indentation direction from the R-stop of the shoulder portion And have.
- the plate surface of the forming portion is squeezed by the shoulder portion when being pushed into the push hole, and is gradually reduced in thickness to the clearance between the outer peripheral surface of the punch and the inner peripheral surface of the push hole.
- the plate thickness of the forming part before ironing is not uniform along the indentation direction. Specifically, the plate thickness on the rear end side of the forming portion along the pressing direction is often thicker than the plate thickness on the front end side of the forming portion. The reason why the rear end side becomes thick in this way is that the front end side is extended more greatly than the rear end side when the forming portion is formed.
- the outer peripheral surface of the punch and the inner peripheral surface of the pressing hole extend in parallel. For this reason, the clearance between the outer peripheral surface of the punch and the inner peripheral surface of the pressing hole is uniform along the pressing direction, and the portion where the plate thickness of the molded portion is thicker is squeezed more. For this reason, the surface treatment layer in the thick plate portion is scraped off, and powdery wrinkles may occur.
- the powdered wrinkles cause problems such as formation of minute dents (indentations) on the surface of the molded portion after ironing and deterioration of product performance using the molded material.
- the present invention has been made to solve the above-described problems, and its purpose is to avoid the occurrence of a large load on a part of the surface treatment layer, and to reduce the generation amount of powdery soot. It is to provide a mold for ironing and a method for producing a molding material.
- a die for ironing according to the present invention is a die for ironing for performing ironing on a convex forming portion formed by using a surface-treated metal plate as a raw material. And a die having a pressing hole into which the forming portion is pressed together with the punch, and the pressing hole is disposed on the outer edge of the inlet of the pressing hole and is configured by a curved surface having a predetermined radius of curvature.
- an inner peripheral surface that extends along the pushing direction of the forming portion from the R stop of the shoulder portion and on which the outer surface of the forming portion is slid by relative displacement of the punch and the die,
- the inner peripheral surface extends non-parallel to the outer peripheral surface of the punch, and the non-performing direction along the indentation direction of the forming portion before ironing is set so that the ironing amount of the forming portion is constant along the indentation direction.
- Clearer according to uniform thickness distribution It It is provided so as to have between the outer peripheral surface of the scan.
- the forming material manufacturing method includes a step of forming a convex forming portion by performing at least one forming process on a surface-treated metal plate, and a mold for ironing after forming the forming portion.
- a molding material manufacturing method including a step of performing ironing on a molding processing portion, wherein a die for ironing processing includes a punch inserted into the molding processing portion, and a pressing hole into which the molding processing portion is pushed together with the punch. And a pressing hole is arranged at the inlet outer edge of the pressing hole and is formed of a curved surface having a predetermined radius of curvature, and from the R-stop of the shoulder part in the pressing direction of the forming portion.
- the molding process Amount can is provided so as to have between the outer peripheral surface of the clearance corresponding to the non-uniform thickness distribution along the pushing direction of the molding portion before ironing to be constant along the pushing direction.
- the inner peripheral surface of the pressing hole extends non-parallel to the outer peripheral surface of the punch, and the ironing amount of the forming portion is in the pressing direction. Because it is provided to have a clearance according to the non-uniform plate thickness distribution along the indentation direction of the forming part before ironing so as to be constant along the outer peripheral surface, some surface treatment It is possible to avoid a large load on the layer and to reduce the amount of powdery soot generated.
- FIG. 1 It is a flowchart which shows the molding material manufacturing method by embodiment of this invention. It is a perspective view which shows the molding material containing the shaping
- FIG. 1 is a flowchart showing a molding material manufacturing method according to an embodiment of the present invention
- FIG. 2 is a perspective view showing a molding material including a molding part 1 molded in the molding step S1 of FIG.
- FIG. 1 is a flowchart showing a molding material manufacturing method according to an embodiment of the present invention
- FIG. 2 is a perspective view showing a molding material including a molding part 1 molded in the molding step S1 of FIG.
- the molding material manufacturing method of the present embodiment includes a molding step S1 and an ironing step S2.
- the forming step S1 is a step of forming the convex forming portion 1 (see FIG. 2) by performing at least one forming process on the surface-treated metal plate.
- the forming process includes a pressing process such as a drawing process or an overhang process.
- the surface-treated metal plate is a metal plate having a surface-treated layer provided on the surface.
- the surface treatment layer includes a coating film and a plating layer.
- the surface-treated metal plate will be described as a Zn-based plated steel plate in which Zn (zinc) -based plating is applied to the surface of the steel plate.
- the forming portion 1 of the present embodiment is a convex portion that is formed so as to protrude further from the top of the cap body after the Zn-based plated steel sheet is formed on the cap body.
- the direction from the base 1b of the forming portion 1 toward the top 1a is referred to as a pressing direction 1c.
- This indentation direction 1c means the direction in which the shaping
- the ironing step S2 is a step in which ironing is performed on the forming portion 1 using a die for ironing described later. With ironing, the clearance between the punch and die of the ironing die is narrower than the thickness of the molding part before ironing, and the plate surface of the molding part is punched with the punch and die.
- This is a processing method in which the thickness of the forming portion is matched with the clearance between the die and the die. That is, the thickness of the forming portion 1 after ironing is made thinner than the thickness of the forming portion 1 before ironing.
- molding process part 1 is made small by performing ironing.
- the molding material manufactured through the molding step S1 and the ironing step S2, that is, the molding material manufactured by the molding material manufacturing method of the present embodiment can be used for various applications. This is particularly used in applications where the dimensional accuracy of the molded part 1 is required.
- FIG. 4 is a cross-sectional view of the forming portion 1 of FIG.
- the thickness of the forming portion 1 before ironing is not uniform along the pressing direction 1c.
- the plate thickness on the base portion 1 b side of the molding portion 1 along the pressing direction 1 c is thicker than the plate thickness on the top portion 1 a side of the molding portion 1.
- the plate thickness of the forming portion 1 is gradually reduced from the rear end side (base portion 1b side) along the pushing direction 1c toward the front end side (top portion 1a side).
- the reason for this non-uniform thickness distribution is that the top portion 1a side is extended more than the base portion 1b side when the forming portion is formed in the forming step S1.
- the reduction rate of the plate thickness is constant or non-constant along the pressing direction 1c.
- FIG. 5 is a cross-sectional view of the ironing die 2 used in the ironing step S2 of FIG. 1, and FIG. 6 shows an ironing process for the forming portion using the ironing die 2 of FIG. It is explanatory drawing which expands and shows the shoulder part 211 periphery of the state which is performing.
- the ironing die 2 includes a punch 20 and a die 21.
- the punch 20 is a convex body that is inserted into the molding portion 1 described above.
- the outer peripheral surface 20 a of the punch 20 extends linearly in parallel with the pressing direction 1 c into the pressing hole 210.
- the die 21 is a member having a pressing hole 210 into which the molding unit 1 is pressed together with the punch 20.
- the push hole 210 has a shoulder portion 211 and an inner peripheral surface 212.
- the shoulder portion 211 is disposed on the outer edge of the entrance of the push hole 210, and is configured by a curved surface having a predetermined radius of curvature.
- the inner peripheral surface 212 is a wall surface extending from the R stop 211a of the shoulder portion 211 along the pushing direction 1c.
- the R stop 211 a of the shoulder portion 211 means a terminal end on the back side of the curved push-in hole 210 constituting the shoulder portion 211.
- That the inner peripheral surface 212 extends along the pushing direction 1c means that the component of the pushing direction 1c is included in the extending direction of the inner peripheral surface 212.
- the inner peripheral surface 212 of the push-in hole 210 extends non-parallel to the outer peripheral surface 20a of the punch 20 (but does not extend in parallel).
- the plate surface of the forming unit 1 is squeezed by the shoulder 211 as shown in FIG. Further, the outer surface of the forming portion 1 is slid on the inner peripheral surface 212 by the relative displacement of the punch 20 and the die 21.
- the inner peripheral surface 212 extends non-parallel to the outer peripheral surface 20a of the punch 20 as described above. Squeeze the face (thinning).
- the inner circumferential surface 212 has a clearance 212a corresponding to a non-uniform plate thickness distribution along the pushing direction 1c of the forming part 1 before ironing so that the ironing amount of the forming part 1 is constant along the pushing direction 1c.
- the clearance 212a here is a clearance between the inner peripheral surface 212 and the outer peripheral surface 20a when the punch 20 is pushed into the push hole 210 to the position where the ironing process is finished as shown in FIG. .
- Amount and is ironing, which is the difference between the ironing unprocessed plate thickness t b and ironing after plate thickness t a ( t b -t a ).
- the clearance 212a between the inner peripheral surface 212 and the outer peripheral surface 20a at each position along the pressing direction 1c is a constant value (required amount of ironing) from the plate thickness of the forming portion 1 before ironing at the same position. ) To reduce the value.
- the clearance 212a at each position along the pushing direction 1c is C (d)
- the plate thickness of the forming part 1 before ironing at the same position is T b (d)
- the required ironing amount is A
- d means the distance from the base 1b of the shaping
- the clearance 212a between the inner peripheral surface 212 and the outer peripheral surface 20a is equal to the pressing direction 1c in the inner peripheral surface 212 at the same rate as the reduction rate of the thickness of the forming portion 1 along the pressing direction 1c before ironing. It is provided so that it may decrease along. If the reduction rate of the thickness of the forming part 1 before the ironing process along the pushing direction 1c is constant, the inner peripheral surface 212 extends at an angle corresponding to the reduction rate of the thickness of the forming part 1. It is comprised by the linear taper surface made.
- the inner peripheral surface 212 is formed of a tapered surface so as to extend at an angle according to the above.
- the inner peripheral surface 212 By configuring the inner peripheral surface 212 in this way, even if the plate thickness distribution of the forming portion 1 along the pressing direction 1c is non-uniform, the load on the surface of the forming portion 1 by ironing is pushed in the pressing direction. It can be uniform along 1c. Thereby, it can avoid that a big load arises in a part of plating, can prevent that a part of surface treatment layer is shaved largely, and can reduce the generation amount of a powdery flaw (plating flaw).
- FIG. 7 is an explanatory diagram conceptually showing the relationship between the shoulder portion 211 of FIG. 6 and the plating layer 10 of the Zn-based plated steel sheet.
- fine unevenness 10a exists on the surface of the plated layer 10 of the Zn-based plated steel sheet.
- the unevenness 10 a may be scraped by the shoulder portion 211 when the plate surface of the forming portion 1 is squeezed by the shoulder portion 211, and may become a plating flaw.
- the amount of plating wrinkles is correlated with the curvature radius r of the shoulder 211 and the ratio r / t of the plate thickness t of the Zn-based plated steel sheet.
- the radius of curvature r of the shoulder portion 211 is smaller, the local strain increases and the sliding resistance between the surface of the plating layer 10 and the shoulder portion 211 increases, so that the amount of plating flaws increases.
- the plate thickness t of the Zn-based plated steel sheet increases, the amount of thickness reduction by the shoulder portion 211 increases and the load applied to the surface of the Zn-based plated steel sheet increases, so the amount of plating flaws increases. That is, the smaller the ratio r / t, the greater the amount of plating flaws generated, and the larger the ratio r / t, the smaller the amount of plating flaws generated.
- the plate surface of the forming part 1 before the ironing process at the position sandwiched between the R-stop 211a and the punch 20 is most reduced by the shoulder part 211.
- the generation amount of the plating flaw is sandwiched between the radius of curvature r of the shoulder portion 211 and the R stop 211a and the punch 20 when the ironing process is finished. It has a ratio r / t re a strong correlation between the thickness t re a molding unit 1 before ironing at the position.
- the amount of plating flaws is correlated with the ironing rate by the shoulder portion 211.
- the ironing rate the clearance between the R stop 211a and the punch 20 is c re, and when the ironing process is finished, the forming part 1 before the ironing process at the position sandwiched between the R stop 211a and the punch 20 is used.
- the plate thickness is t re , it is represented by ⁇ (t re ⁇ c re ) / t re ⁇ ⁇ 100.
- the clearance c re corresponds to the plate thickness of the forming part 1 after the ironing process at a position sandwiched between the R stop 211a and the punch 20.
- FIG. 8 is a graph showing the skewness Rsk of the plating layer 10 of FIG. 6 in various plating layers.
- the amount of plating soot is also correlated with the skewness Rsk of the plating layer 10.
- the skewness Rsk is defined by Japanese Industrial Standard B0601, and is represented by the following equation.
- Skewness Rsk represents the existence probability of the convex part in the unevenness 10a (see FIG. 7) of the plating layer 10. As the skewness Rsk is smaller, the number of convex portions is smaller and the amount of plating defects is suppressed. Note that the skewness Rsk is also described in Japanese Patent Laid-Open No. 2006-193776 by the present applicant.
- examples of the Zn-based plated steel sheet include Zn—Al—Mg alloy-plated steel sheet, alloyed hot-dip galvanized steel sheet, hot-dip galvanized steel sheet, and electrogalvanized steel sheet.
- a Zn—Al—Mg alloy-plated steel sheet is typically a steel sheet with a plating layer made of an alloy containing Zn, 6 mass% Al (aluminum) and 3 mass% Mg (magnesium). is there.
- the skewness Rsk of the Zn—Al—Mg alloy-plated steel sheet is included in the range of less than ⁇ 0.6 and ⁇ 1.3 or more. It was found that the other plated steel sheets were included in the range of ⁇ 0.6 or more and 0 or less.
- the inventors of the present invention performed ironing of a Zn—Al—Mg alloy-plated steel sheet under the following conditions so as to change the ironing rate and r / tre , respectively.
- board thickness of a test material is 1.8 mm
- the vertical axis of FIG. 9 is the ironing rate represented by ⁇ (t re ⁇ c re ) / t re ⁇ ⁇ 100, and the horizontal axis is the radius of curvature r of the shoulder portion 211 represented by r / t re , and the ironing process is completed.
- the ratio of the thickness t re a molding unit 1 before ironing at a position sandwiched between the R blind 211a and the punch 20 during the.
- ⁇ shows the evaluation that the generation of plating flaws could be suppressed
- ⁇ shows the evaluation that the generation of plating flaws could not be suppressed.
- ⁇ indicates that the dimensional accuracy is out of the predetermined range.
- the present inventors performed the same experiment on the alloyed hot-dip galvanized steel sheet, hot-dip galvanized steel sheet, and electrogalvanized steel sheet under the following conditions. Note that the experimental conditions (see Table 3) of the press machine and the like are the same as the ironing of the Zn—Al—Mg alloy-plated steel sheet described above.
- the alloyed hot-dip galvanized steel sheet and hot-dip galvanized steel sheet had a plate thickness of 1.8 mm and a plating adhesion amount of 90 g / m 2 .
- the plate thickness was 1.8 mm, and the amount of plating was 20 g / m 2 .
- the inner peripheral surface 212 is formed so that the ironing amount of the molding part 1 is constant along the pressing direction 1c and the molding part 1 before the ironing process 1 Since the clearance 212a corresponding to the non-uniform plate thickness distribution along the pressing direction 1c is provided between the punch 20 and the outer peripheral surface 20a, a large load is applied to a part of the surface treatment layer (plating layer 10). Can be avoided, and the generation amount of powdery soot (plating soot) can be reduced.
- the surface-treated metal plate is described as a Zn-based plated steel plate, but the present invention can also be applied to other surface-treated metal plates such as an aluminum plate provided with a coating film on the surface.
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Shaping Metal By Deep-Drawing, Or The Like (AREA)
- Blow-Moulding Or Thermoforming Of Plastics Or The Like (AREA)
- Laminated Bodies (AREA)
Priority Applications (12)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP13887981.2A EP3015186B1 (en) | 2013-06-28 | 2013-07-10 | Mold for ironing and method for manufacturing molded material |
SG11201507296PA SG11201507296PA (en) | 2013-06-28 | 2013-07-10 | Ironing mold and formed material manufacturing method |
CA2905000A CA2905000C (en) | 2013-06-28 | 2013-07-10 | Ironing mold and formed material manufacturing method |
KR1020157019129A KR101576009B1 (ko) | 2013-06-28 | 2013-07-10 | 아이어닝 가공용 금형 및 성형재 제조 방법 |
CN201380001573.XA CN104411424B (zh) | 2013-06-28 | 2013-07-10 | 减薄拉伸加工用模具以及成型材料制造方法 |
BR112015018879-6A BR112015018879B1 (pt) | 2013-06-28 | 2013-07-10 | molde de laminação, e, método de fabricação de material conformado |
EA201591134A EA028442B1 (ru) | 2013-06-28 | 2013-07-10 | Вытяжной формовочный инструмент и способ изготовления формованного изделия |
US14/768,866 US9527128B2 (en) | 2013-06-28 | 2013-07-10 | Ironing mold and formed material manufacturing method |
AU2013396488A AU2013396488B2 (en) | 2013-06-28 | 2013-07-10 | Ironing mold and formed material manufacturing method |
MX2015010368A MX357695B (es) | 2013-06-28 | 2013-07-10 | Molde de enderezamiento en prensa y metodo de elaboracion de material formado. |
RS20180715A RS57330B1 (sr) | 2013-06-28 | 2013-07-10 | Kalup za peglanje i postupak za izradu formiranih materijala |
PH12015501689A PH12015501689B1 (en) | 2013-06-28 | 2015-07-31 | Mold for ironing and method for manufacturing molded material |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2013135859 | 2013-06-28 | ||
JP2013-135859 | 2013-06-28 |
Publications (1)
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WO2014207947A1 true WO2014207947A1 (ja) | 2014-12-31 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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PCT/JP2013/068880 WO2014207947A1 (ja) | 2013-06-28 | 2013-07-10 | しごき加工用金型及び成形材製造方法 |
Country Status (18)
Country | Link |
---|---|
US (1) | US9527128B2 (tr) |
EP (1) | EP3015186B1 (tr) |
JP (1) | JP5395301B1 (tr) |
KR (1) | KR101576009B1 (tr) |
CN (1) | CN104411424B (tr) |
AU (1) | AU2013396488B2 (tr) |
BR (1) | BR112015018879B1 (tr) |
CA (1) | CA2905000C (tr) |
EA (1) | EA028442B1 (tr) |
HU (1) | HUE037834T2 (tr) |
MX (1) | MX357695B (tr) |
MY (1) | MY161699A (tr) |
PH (1) | PH12015501689B1 (tr) |
PT (1) | PT3015186T (tr) |
RS (1) | RS57330B1 (tr) |
SG (1) | SG11201507296PA (tr) |
TR (1) | TR201807893T4 (tr) |
WO (1) | WO2014207947A1 (tr) |
Families Citing this family (6)
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JP6066896B2 (ja) * | 2013-12-17 | 2017-01-25 | 日新製鋼株式会社 | 成形材製造方法 |
JP5613341B1 (ja) * | 2014-01-27 | 2014-10-22 | 日新製鋼株式会社 | しごき加工用金型及び成形材製造方法 |
JP6242363B2 (ja) | 2015-03-31 | 2017-12-06 | 日新製鋼株式会社 | 成形材製造方法 |
US10456820B2 (en) | 2016-03-03 | 2019-10-29 | Nippon Steel Nisshin Co., Ltd. | Method for manufacturing molded member |
JP6616027B1 (ja) * | 2019-01-30 | 2019-12-04 | 日鉄日新製鋼株式会社 | 筒状回転部品の製造方法 |
CN116351943B (zh) * | 2023-05-26 | 2023-08-15 | 镇江先锋汽车零部件有限公司 | 一种电机外壳轴承室双层叠料成型工艺 |
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Also Published As
Publication number | Publication date |
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KR101576009B1 (ko) | 2015-12-08 |
KR20150090259A (ko) | 2015-08-05 |
MX357695B (es) | 2018-07-19 |
EP3015186B1 (en) | 2018-03-28 |
EP3015186A1 (en) | 2016-05-04 |
PH12015501689A1 (en) | 2015-10-19 |
EP3015186A4 (en) | 2016-10-19 |
AU2013396488A1 (en) | 2015-09-03 |
AU2013396488B2 (en) | 2016-03-24 |
CA2905000A1 (en) | 2014-12-31 |
MY161699A (en) | 2017-05-15 |
US20160001349A1 (en) | 2016-01-07 |
EA201591134A1 (ru) | 2015-11-30 |
CN104411424B (zh) | 2016-04-06 |
PT3015186T (pt) | 2018-06-22 |
EA028442B1 (ru) | 2017-11-30 |
CN104411424A (zh) | 2015-03-11 |
RS57330B1 (sr) | 2018-08-31 |
MX2015010368A (es) | 2015-10-29 |
BR112015018879B1 (pt) | 2020-12-08 |
HUE037834T2 (hu) | 2018-09-28 |
SG11201507296PA (en) | 2015-10-29 |
JP5395301B1 (ja) | 2014-01-22 |
BR112015018879A2 (pt) | 2020-01-14 |
TR201807893T4 (tr) | 2018-06-21 |
US9527128B2 (en) | 2016-12-27 |
PH12015501689B1 (en) | 2015-10-19 |
CA2905000C (en) | 2017-05-16 |
JP2015027679A (ja) | 2015-02-12 |
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