WO2013146927A1 - 喫煙物品用香料含有シートの切断片 - Google Patents

喫煙物品用香料含有シートの切断片 Download PDF

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Publication number
WO2013146927A1
WO2013146927A1 PCT/JP2013/059104 JP2013059104W WO2013146927A1 WO 2013146927 A1 WO2013146927 A1 WO 2013146927A1 JP 2013059104 W JP2013059104 W JP 2013059104W WO 2013146927 A1 WO2013146927 A1 WO 2013146927A1
Authority
WO
WIPO (PCT)
Prior art keywords
cut piece
fragrance
cut
containing sheet
ratio
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2013/059104
Other languages
English (en)
French (fr)
Japanese (ja)
Inventor
達也 日下部
坂大　武志
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Japan Tobacco Inc
Original Assignee
Japan Tobacco Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Japan Tobacco Inc filed Critical Japan Tobacco Inc
Priority to RU2014143184A priority Critical patent/RU2014143184A/ru
Priority to SG11201405558SA priority patent/SG11201405558SA/en
Priority to PL13767629T priority patent/PL2832243T3/pl
Priority to EP13767629.2A priority patent/EP2832243B1/en
Publication of WO2013146927A1 publication Critical patent/WO2013146927A1/ja
Priority to PH12014501994A priority patent/PH12014501994B1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/12—Steaming, curing, or flavouring tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/281—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed
    • A24B15/282—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by indirect addition of the chemical substances, e.g. in the wrapper, in the case
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A24B15/303—Plant extracts other than tobacco

Definitions

  • the present invention relates to a cut piece of a fragrance-containing sheet for smoking articles.
  • a fragrance-containing sheet in which a volatile fragrance such as menthol is dispersed in a non-volatile matrix such as a polysaccharide, polyol, or ether polymer is known (for example, Patent Document 1 and Patent Document 2).
  • the volatile fragrance is dispersed in the matrix as droplet-shaped particles of about several tens of ⁇ m, and its volatilization is suppressed.
  • the perfume-containing sheet is cut, and the cut piece is mixed with a tobacco cut and wound up on a cigarette rod, and the flavor of the flavor is added to the flavor of the tobacco cut during smoking.
  • a cut piece of a fragrance-containing sheet for smoking articles is provided.
  • the cut piece of the fragrance-containing sheet of the present invention maintains a sufficient amount of fragrance, and has a shape that suppresses volatilization of the fragrance during storage and is not easily broken by mechanical external force.
  • FIG. 1 is a diagram showing a relationship between a weight reduction rate of a fragrance and a ratio of a cross-sectional area / volume of a cut piece of the fragrance-containing sheet.
  • Drawing 2 is a figure showing the particle size before and behind forced crushing of the cut piece of a perfume content sheet.
  • Drawing 3 is a figure showing the particle size before and behind forced crushing of the cut piece of a fragrance content sheet.
  • Drawing 4 is a figure showing the particle size before and behind forced crushing of the cut piece of a perfume content sheet.
  • the cut piece of the flavor-containing sheet of the present invention is cut out from the flavor-containing sheet.
  • the perfume-containing sheet is formed by dispersing a perfume such as menthol in a non-volatile matrix such as a polysaccharide.
  • a fragrance-containing sheet is described in, for example, International Publication WO2009-142159. More specifically, the fragrance-containing sheet is one in which the fragrance is dispersed in a matrix made of a polysaccharide gel.
  • Polysaccharides include carrageenan, agar, gellan gum, tamarind gum, psyllium seed gum or konjac glucomannan alone, or carrageenan, locust bean gum, guar gum, agar, xanthan gum, gellan gum, tamarind gum, tara gum, konjac glucomannan, starch, A combination of two or more polysaccharides selected from the group consisting of cassia gum and psyllium seed gum can be exemplified. Since such a polysaccharide can be gelled by cooling, it is not necessary to add a gelling agent such as a metal chloride. Examples of the flavor include lipophilic flavors such as l-menthol and mint oil.
  • Such a perfume-containing sheet is obtained by mixing a polysaccharide and water, heating to obtain an aqueous solution of the polysaccharide, adding a perfume and preferably an emulsifier into the aqueous solution, and stirring to emulsify the perfume.
  • the obtained emulsion can be cast on a substrate and dried by heating.
  • As the emulsifier lecithin, sugar ester and the like can be used. Heating and drying can be performed at 70 ° C to 200 ° C.
  • the perfume-containing sheet thus obtained the perfume is dispersed as particles in the non-volatile matrix.
  • Such a fragrance-containing sheet can contain a fragrance in an amount of 18% by weight or more, preferably 60% by weight or more.
  • seat contains a fragrance
  • the shape of the cut piece is a hexahedron, but is preferably a rectangular parallelepiped, for example, a regular quadrangular prism, and more preferably a cube.
  • the short side is x
  • the long side is y
  • the thickness is t.
  • the short side and long side in the present invention are defined as a rectangular short side and long side formed by projecting a hexahedron in the thickness direction.
  • the ratio r of the long side / short side, the area A of the cut surface, the volume V of the cut piece, and the ratio ⁇ of the area / volume of the cut surface are expressed by the following equations.
  • the area A of a cut surface means the sum total of four cut surfaces of the cut piece produced when a fragrance
  • equation (4 ′′) into equation (1) to obtain the relationship between y, ⁇ , and r yields the following equation. r ⁇ ( ⁇ y ⁇ 2) / 2 (5)
  • the ratio of the area of the cut surface to the volume of the cut piece is 3.0 or less
  • the ratio of the length of the long side to the length of the short side is 10 or less
  • the length of the long side Is less than the diameter of the cigarette rod to be manufactured.
  • the ratio of the area of the cut surface to the volume thereof is 2.0 or less
  • the ratio of the length of the long side to the length of the short side is 5 or less
  • the length The length of the side is 1 ⁇ 2 or less of the diameter of the cigarette rod to be manufactured.
  • the shape of the cut piece is a quadrangular prism
  • the short side is 1.0 mm to 2.0 mm.
  • the cut piece of the fragrance-containing sheet obtained as described above is mixed with tobacco cut, and the mixture is wound with cigarette wrapping paper to obtain a cigarette rod.
  • the diameter of the cigarette rod is 3 mm to 10 mm.
  • Example 1 A total of 3680 parts by weight of polysaccharides (gellan gum and tamarind gum) were added to 80000 parts by weight of water, and the mixture was sufficiently stirred at 80 ° C. to dissolve the polysaccharides.
  • An aqueous emulsifier solution in which 18400 parts by weight of a flavor (l-menthol) and 74 parts by weight of an emulsifier (lecithin) are dissolved in 1398 parts by weight of water is added to this polysaccharide aqueous solution, and the resulting mixture is sufficiently emulsified by a homogenizer. It was.
  • This emulsified slurry was cast into a sheet on a substrate and dried at 70 ° C.
  • the thickness of the flavor-containing sheet after drying was 0.1 mm.
  • seat was cut
  • the mixture was wound with cigarette wrapping paper to obtain a cigarette rod (Example 1).
  • the cigarette rod obtained above was stored in a thermostat in a 50 ° C. atmosphere at a temperature of 50 ° C. for a predetermined period, and the perfume residual rate (with a charged amount of 100%) was measured as follows. The results are shown in Table 1 below.
  • the measurement solution was subjected to the following GC-FID and quantified by a calibration curve method.
  • the cut pieces of the fragrance-containing sheet have a much higher residual ratio of fragrance than when the fragrance is added directly to the tobacco cut.
  • Example 2 To 70000 parts by weight of water, 5200 parts by weight of polysaccharides (gellan gum and tamarind gum) were added and sufficiently stirred at 80 ° C. to dissolve the polysaccharides. An aqueous emulsifier solution in which 13000 parts by weight of 1-menthol, 455 parts by weight of colorants (caramel pigment and cocoa powder) and 105 parts by weight of an emulsifier (lecithin) are dissolved in 1995 parts by weight of water is added to the aqueous solution of the polysaccharide. The resulting mixture was sufficiently emulsified with a homogenizer. The obtained emulsified slurry was cast on a substrate in a sheet form and dried at 70 ° C. The thickness of the flavor-containing sheet after drying was 0.1 mm.
  • polysaccharides gellan gum and tamarind gum
  • This fragrance-containing sheet was cut into square pillars of various sizes to produce cut pieces.
  • the size of the cut piece produced at this time is as follows.
  • Each piece was left in a thermostatic bath at a temperature of 50 ° C. for accelerating the volatilization of the fragrance for 1 hour, and the weight reduction rate of the fragrance was measured.
  • the relationship between this reduction rate and the cross-sectional area / volume ratio of the cut piece is shown in FIG.
  • the cross-sectional area per volume of the cut piece may be reduced.
  • the cross-sectional area / volume of the cut piece is 3 or less, preferably 2 or less where the weight reduction rate of the fragrance is 20% or less.
  • the shape of the cut piece is first defined based on the cross-sectional area / volume ratio, and then the cross-sectional area at the time of cutting is defined, and then the long side / short side ratio It is realized by reducing the generation of the crushing cross section by making it smaller.
  • the cut piece A and the cut piece C were mixed with 5% of cigarettes and wound on a cigarette rod having a circumference length of 25.2 mm, and then the cigarette rod was cut and all the cut pieces were collected. It was confirmed that very few pieces were crushed.

Landscapes

  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Fats And Perfumes (AREA)
PCT/JP2013/059104 2012-03-28 2013-03-27 喫煙物品用香料含有シートの切断片 Ceased WO2013146927A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
RU2014143184A RU2014143184A (ru) 2012-03-28 2013-03-27 Отрезок ароматизированного листа для курительного изделия
SG11201405558SA SG11201405558SA (en) 2012-03-28 2013-03-27 Cut piece of flavor-containing sheet for smoking article
PL13767629T PL2832243T3 (pl) 2012-03-28 2013-03-27 Odcięty fragment arkusza zawierającego zapach
EP13767629.2A EP2832243B1 (en) 2012-03-28 2013-03-27 Cut-piece of flavour containing sheet
PH12014501994A PH12014501994B1 (en) 2012-03-28 2014-09-05 Cut piece of flavor-containing sheet for smoking article

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2012074877 2012-03-28
JP2012-074877 2012-03-28

Publications (1)

Publication Number Publication Date
WO2013146927A1 true WO2013146927A1 (ja) 2013-10-03

Family

ID=49260176

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2013/059104 Ceased WO2013146927A1 (ja) 2012-03-28 2013-03-27 喫煙物品用香料含有シートの切断片

Country Status (9)

Country Link
EP (1) EP2832243B1 (https=)
JP (2) JPWO2013146927A1 (https=)
MY (1) MY167285A (https=)
PH (1) PH12014501994B1 (https=)
PL (1) PL2832243T3 (https=)
RU (2) RU2014143184A (https=)
SG (2) SG11201405558SA (https=)
TW (1) TW201345444A (https=)
WO (1) WO2013146927A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016005478A (ja) * 2012-03-28 2016-01-14 日本たばこ産業株式会社 喫煙物品用香料含有シートの切断片

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5993526B1 (ja) 2016-01-14 2016-09-14 株式会社Ｍｉｚｋａｎ Ｈｏｌｄｉｎｇｓ ぽん酢醤油調味料
JP7171910B2 (ja) * 2019-05-21 2022-11-15 日本たばこ産業株式会社 加熱型香味吸引器用香料含有シートおよび加熱型香味吸引器
KR102747912B1 (ko) * 2021-11-22 2025-01-02 주식회사 케이티앤지 수용성 향료를 포함하는 고체 분산체를 함유하는 필터 및 이를 포함하는 흡연물품

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0664646U (ja) * 1993-02-23 1994-09-13 株式会社ニューモメント 装飾用の芳香材
WO2009021018A1 (en) 2007-08-07 2009-02-12 Lorillard Licensing Company, L.L.C. Flavor sheet for smoking article
WO2009142159A1 (ja) 2008-05-19 2009-11-26 日本たばこ産業株式会社 シガレット用香料含有材料、その製造方法およびシガレット

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EP0691083B1 (en) * 1994-01-26 1998-12-16 Japan Tobacco Inc. Flavor generating article
US20050172976A1 (en) * 2002-10-31 2005-08-11 Newman Deborah J. Electrically heated cigarette including controlled-release flavoring
US8439047B2 (en) * 2003-12-22 2013-05-14 Philip Morris Usa Inc. Composite mesoporous/microporous materials and their use in smoking articles for removing certain gas phase constituents from tobacco smoke
RU2336000C2 (ru) * 2006-06-13 2008-10-20 Государственное научное учреждение Всероссийский научно-исследовательский институт табака, махорки и табачных изделий Способ обработки табачного сырья
US8469037B2 (en) * 2008-02-08 2013-06-25 Philip Morris Usa Inc. Pre-portioned moist product and method of making
CN102325472B (zh) * 2008-12-19 2015-07-29 美国无烟烟草有限责任公司 烟草颗粒和生产烟草颗粒的方法
WO2010113702A1 (ja) * 2009-04-03 2010-10-07 日本たばこ産業株式会社 非燃焼型喫煙物品用シートおよび非燃焼型喫煙物品、並びにそれらの製造方法
JP5315455B2 (ja) * 2010-03-26 2013-10-16 日本たばこ産業株式会社 揮発性香料デリバリー量を高めたシガレット
SG11201405558SA (en) * 2012-03-28 2014-11-27 Japan Tobacco Inc Cut piece of flavor-containing sheet for smoking article

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0664646U (ja) * 1993-02-23 1994-09-13 株式会社ニューモメント 装飾用の芳香材
WO2009021018A1 (en) 2007-08-07 2009-02-12 Lorillard Licensing Company, L.L.C. Flavor sheet for smoking article
WO2009142159A1 (ja) 2008-05-19 2009-11-26 日本たばこ産業株式会社 シガレット用香料含有材料、その製造方法およびシガレット

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP2832243A4

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016005478A (ja) * 2012-03-28 2016-01-14 日本たばこ産業株式会社 喫煙物品用香料含有シートの切断片

Also Published As

Publication number Publication date
SG10201607097QA (en) 2016-10-28
SG11201405558SA (en) 2014-11-27
TW201345444A (zh) 2013-11-16
EP2832243B1 (en) 2019-09-11
JPWO2013146927A1 (ja) 2015-12-14
RU2670411C1 (ru) 2018-10-22
EP2832243A4 (en) 2015-12-02
MY167285A (en) 2018-08-15
RU2014143184A (ru) 2016-05-20
JP2016005478A (ja) 2016-01-14
EP2832243A1 (en) 2015-02-04
PH12014501994B1 (en) 2019-04-24
JP6012826B2 (ja) 2016-10-25
PL2832243T3 (pl) 2020-04-30
PH12014501994A1 (en) 2014-11-24

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