WO2013012268A3 - 균일한 크기의 실리카 나노입자 대량 제조 방법 - Google Patents

균일한 크기의 실리카 나노입자 대량 제조 방법 Download PDF

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Publication number
WO2013012268A3
WO2013012268A3 PCT/KR2012/005770 KR2012005770W WO2013012268A3 WO 2013012268 A3 WO2013012268 A3 WO 2013012268A3 KR 2012005770 W KR2012005770 W KR 2012005770W WO 2013012268 A3 WO2013012268 A3 WO 2013012268A3
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WO
WIPO (PCT)
Prior art keywords
silica nanoparticles
production method
uniformly sized
volume production
sized silica
Prior art date
Application number
PCT/KR2012/005770
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English (en)
French (fr)
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WO2013012268A2 (ko
WO2013012268A9 (ko
Inventor
현택환
박원철
권파
Original Assignee
서울대학교 산학협력단
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 서울대학교 산학협력단 filed Critical 서울대학교 산학협력단
Priority to JP2014521559A priority Critical patent/JP2014520755A/ja
Priority to US14/233,987 priority patent/US20140356272A1/en
Priority to EP12815496.0A priority patent/EP2735543A4/en
Priority to CN201280035270.5A priority patent/CN103930368A/zh
Publication of WO2013012268A2 publication Critical patent/WO2013012268A2/ko
Publication of WO2013012268A9 publication Critical patent/WO2013012268A9/ko
Publication of WO2013012268A3 publication Critical patent/WO2013012268A3/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Silicon Compounds (AREA)

Abstract

본 발명은 염기성 완충용액을 이용한 균일한 크기의 실리카 나노입자의 대량 제조 방법에 관한 것이다. 보다 상세하게는, 본 발명은 (i) 유기 용매에 실리카 전구체를 녹인 용액을 염기성 완충용액에 첨가하여 가열하는 단계; 및 (ii) 상기 (i) 단계에서 생성된 실리카 나노입자를 분리하는 단계를 포함하는 균일한 크기의 실리카 나노입자 제조 방법에 대한 것이다.
PCT/KR2012/005770 2011-07-21 2012-07-19 균일한 크기의 실리카 나노입자 대량 제조 방법 WO2013012268A2 (ko)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP2014521559A JP2014520755A (ja) 2011-07-21 2012-07-19 均一の大きさのシリカナノ粒子の大量製造方法
US14/233,987 US20140356272A1 (en) 2011-07-21 2012-07-19 Volume production method for uniformly sized silica nanoparticles
EP12815496.0A EP2735543A4 (en) 2011-07-21 2012-07-19 MASS PRODUCTION PROCESS FOR SILICA NANOTE PARTICLES OF UNIFORM SIZE
CN201280035270.5A CN103930368A (zh) 2011-07-21 2012-07-19 用于均匀尺寸的二氧化硅纳米粒子的批量生产方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR10-2011-0072691 2011-07-21
KR1020110072691A KR101880441B1 (ko) 2011-07-21 2011-07-21 균일한 크기의 실리카 나노입자 대량 제조 방법

Publications (3)

Publication Number Publication Date
WO2013012268A2 WO2013012268A2 (ko) 2013-01-24
WO2013012268A9 WO2013012268A9 (ko) 2013-03-14
WO2013012268A3 true WO2013012268A3 (ko) 2013-05-10

Family

ID=47558623

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2012/005770 WO2013012268A2 (ko) 2011-07-21 2012-07-19 균일한 크기의 실리카 나노입자 대량 제조 방법

Country Status (6)

Country Link
US (1) US20140356272A1 (ko)
EP (1) EP2735543A4 (ko)
JP (1) JP2014520755A (ko)
KR (1) KR101880441B1 (ko)
CN (1) CN103930368A (ko)
WO (1) WO2013012268A2 (ko)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101390657B1 (ko) * 2013-02-21 2014-04-30 한림대학교 산학협력단 다중 금 나노닷 코어와 실리카 외각으로 이루어진 구형 나노입자 및 그 합성방법
KR101582109B1 (ko) 2013-12-27 2016-01-04 한양대학교 산학협력단 기능기를 갖는 실리카 입자의 제조방법 및 이에 따라 제조된 실리카 입자
US9561473B2 (en) * 2014-02-28 2017-02-07 Pall Corporation Charged hollow fiber membrane having hexagonal voids
US9737860B2 (en) * 2014-02-28 2017-08-22 Pall Corporation Hollow fiber membrane having hexagonal voids
KR101483936B1 (ko) 2014-05-16 2015-01-21 한국에너지기술연구원 피셔-트롭쉬 합성 반응용 철-카바이드/실리카 나노 복합 촉매의 제조 방법 및 그 촉매와, 이를 이용한 액체 탄화수소의 합성 방법 및 그 액체 탄화수소
CN104609431A (zh) * 2015-01-19 2015-05-13 武汉金弘扬化工科技有限公司 一种50纳米以下SiO2纳米粒子的合成方法及其粒径控制合成方法
US10434496B2 (en) 2016-03-29 2019-10-08 Agilent Technologies, Inc. Superficially porous particles with dual pore structure and methods for making the same
EP3282290B1 (en) 2016-08-09 2018-10-17 Essilor International Composition for the manufacture of an ophtalmic lens comprising an encapsulated light-absorbing additive
US10131830B1 (en) * 2017-10-03 2018-11-20 Saudi Arabian Oil Company Method for preventing formation of water-oil emulsions using additives
KR101985101B1 (ko) * 2017-10-25 2019-06-03 중앙대학교 산학협력단 실록산계 나노입자의 제조방법
CN110272052B (zh) * 2018-03-14 2022-10-04 天津工业大学 一种纳米二氧化硅微囊的新型制备方法
CN108862292A (zh) * 2018-09-10 2018-11-23 江西师范大学 一种调控二氧化硅微球粒径的方法
KR102197574B1 (ko) * 2018-10-04 2020-12-31 한남대학교 산학협력단 단분산 실리카 나노입자의 제조방법
KR102204401B1 (ko) * 2019-04-08 2021-01-15 성균관대학교산학협력단 다공성 실리카 나노 입자 및 이의 제조 방법
CN112239209B (zh) * 2019-07-18 2024-01-12 奈力生医股份有限公司 通过孔改性的介孔二氧化硅纳米颗粒进行的药物递送
KR102280900B1 (ko) 2020-04-29 2021-07-23 주식회사 엘피엔 신규한 실리콘 나노 입자의 제조방법
CN112209389A (zh) * 2020-09-11 2021-01-12 江苏大学 一种超细纳米二氧化硅球的制备方法
CN112265999A (zh) * 2020-10-30 2021-01-26 三棵树(上海)新材料研究有限公司 一种粒径可控的功能化纳米二氧化硅水分散液、制备方法及应用
CN112442407A (zh) * 2020-11-17 2021-03-05 北京大学深圳研究生院 一种减摩剂的制备方法
CN113443633B (zh) * 2021-06-28 2022-04-29 上海千溯生物科技有限公司 小尺寸内核仿病毒二氧化硅纳米粒子及其制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20080085464A (ko) * 2007-03-20 2008-09-24 엘지마이크론 주식회사 실리카 나노입자 및 그 제조방법

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8263035B2 (en) * 2006-10-26 2012-09-11 Davis Tracy M Forming nanoparticles in basic amino acid sols

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20080085464A (ko) * 2007-03-20 2008-09-24 엘지마이크론 주식회사 실리카 나노입자 및 그 제조방법

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
JIAN LIU ET AL.: "Structural control of mesoporous silicas with large nanopores in a mild buffer solution.", MICROPOROUS AND MESOPOROUS MATERIALS., vol. 116, no. 1-3, 2008, pages 330 - 338, XP025563147 *
KURTIS D. HARTLEN ET AL.: "Facile preparation of highly monodisperse small silica spheres(15 to >200nm) suitable for colloidal templating and formation of ordered arrays.", LANGMUIR., vol. 24, no. 5, 2008, pages 1714 - 1720, XP055141518 *

Also Published As

Publication number Publication date
WO2013012268A2 (ko) 2013-01-24
CN103930368A (zh) 2014-07-16
US20140356272A1 (en) 2014-12-04
EP2735543A4 (en) 2015-04-29
JP2014520755A (ja) 2014-08-25
WO2013012268A9 (ko) 2013-03-14
EP2735543A2 (en) 2014-05-28
KR101880441B1 (ko) 2018-07-20
KR20130011505A (ko) 2013-01-30

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