WO2011129562A3 - 균일한 크기를 가지는 은 나노입자의 대량 제조 방법 - Google Patents

균일한 크기를 가지는 은 나노입자의 대량 제조 방법 Download PDF

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Publication number
WO2011129562A3
WO2011129562A3 PCT/KR2011/002522 KR2011002522W WO2011129562A3 WO 2011129562 A3 WO2011129562 A3 WO 2011129562A3 KR 2011002522 W KR2011002522 W KR 2011002522W WO 2011129562 A3 WO2011129562 A3 WO 2011129562A3
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Prior art keywords
silver nanoparticles
mass production
uniform size
silver
relates
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PCT/KR2011/002522
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English (en)
French (fr)
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WO2011129562A2 (ko
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현택환
박진경
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서울대학교 산학협력단
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Priority to CN2011800183897A priority Critical patent/CN102858684A/zh
Priority to EP11769028A priority patent/EP2559654A2/en
Priority to US13/640,639 priority patent/US20130133484A1/en
Priority to JP2013504810A priority patent/JP2013524021A/ja
Publication of WO2011129562A2 publication Critical patent/WO2011129562A2/ko
Publication of WO2011129562A3 publication Critical patent/WO2011129562A3/ko

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G5/00—Compounds of silver
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/30—Making metallic powder or suspensions thereof using chemical processes with decomposition of metal compounds, e.g. by pyrolysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/84—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/85—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

본 발명은 균일한 크기를 가지는 은 나노입자를 대량으로 제조하는 방법에 관한 것이다. 보다 상세하게는, 본 발명은 i) 비활성 분위기에서 은 전구체 및 계면활성제의 혼합물을 가열하여 은 나노입자를 제조하는 단계; 그리고 ii) 상기 은 나노입자를 분리하는 단계를 포함하는, 은 나노입자 제조 방법에 대한 것이다.
PCT/KR2011/002522 2010-04-12 2011-04-11 균일한 크기를 가지는 은 나노입자의 대량 제조 방법 WO2011129562A2 (ko)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN2011800183897A CN102858684A (zh) 2010-04-12 2011-04-11 批量生产具有均匀尺寸的银纳米粒子的方法
EP11769028A EP2559654A2 (en) 2010-04-12 2011-04-11 Method for the mass production of silver nanoparticles having a uniform size
US13/640,639 US20130133484A1 (en) 2010-04-12 2011-04-11 Method for the Mass Production of Silver Nanoparticles Having a Uniform Size
JP2013504810A JP2013524021A (ja) 2010-04-12 2011-04-11 均一なサイズを有する銀ナノ粒子の大量製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020100033195A KR20110113877A (ko) 2010-04-12 2010-04-12 균일한 크기를 가지는 은 나노입자의 대량 제조 방법
KR10-2010-0033195 2010-04-12

Publications (2)

Publication Number Publication Date
WO2011129562A2 WO2011129562A2 (ko) 2011-10-20
WO2011129562A3 true WO2011129562A3 (ko) 2012-04-05

Family

ID=44799142

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2011/002522 WO2011129562A2 (ko) 2010-04-12 2011-04-11 균일한 크기를 가지는 은 나노입자의 대량 제조 방법

Country Status (6)

Country Link
US (1) US20130133484A1 (ko)
EP (1) EP2559654A2 (ko)
JP (1) JP2013524021A (ko)
KR (1) KR20110113877A (ko)
CN (1) CN102858684A (ko)
WO (1) WO2011129562A2 (ko)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9982322B2 (en) 2012-08-30 2018-05-29 Corning Incorporated Solvent-free syntheses of silver products produced thereby
JP2015531432A (ja) * 2012-08-31 2015-11-02 コーニング インコーポレイテッド 銀の低温分散系合成及びそれによって製造される銀生成物
KR101515137B1 (ko) * 2013-11-08 2015-04-24 한국기초과학지원연구원 은 나노입자의 제조방법 및 이를 이용하여 제조된 소수성 구형 은 나노입자
JP6378880B2 (ja) * 2014-01-10 2018-08-22 株式会社ダイセル 銀ナノ粒子の製造方法及び銀ナノ粒子
CN105779981A (zh) * 2016-04-22 2016-07-20 广东南海启明光大科技有限公司 一种环保化学镀银液制备方法
KR102061718B1 (ko) * 2017-10-30 2020-01-02 엘에스니꼬동제련 주식회사 표면 처리된 은 분말 및 이의 제조방법
JP7175218B2 (ja) * 2019-02-27 2022-11-18 Ｄｏｗａエレクトロニクス株式会社 銀粉およびその製造方法

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JP2008019504A (ja) * 2006-07-10 2008-01-31 Samsung Electro-Mechanics Co Ltd 金属ナノ粒子の製造方法
KR20090012605A (ko) * 2007-07-30 2009-02-04 삼성전기주식회사 금속 나노입자의 제조방법
WO2009133446A1 (en) * 2008-04-28 2009-11-05 Tata Chemicals Limited A process for the preparation of silver nano particles
KR20100021972A (ko) * 2008-08-18 2010-02-26 제록스 코포레이션 은 나노입자 및 그의 제조 방법

Also Published As

Publication number Publication date
WO2011129562A2 (ko) 2011-10-20
CN102858684A (zh) 2013-01-02
KR20110113877A (ko) 2011-10-19
EP2559654A2 (en) 2013-02-20
JP2013524021A (ja) 2013-06-17
US20130133484A1 (en) 2013-05-30

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