WO2012020986A3 - 무기화합물의 제조장치 및 이를 사용한 무기화합물의 제조방법 - Google Patents

무기화합물의 제조장치 및 이를 사용한 무기화합물의 제조방법 Download PDF

Info

Publication number
WO2012020986A3
WO2012020986A3 PCT/KR2011/005844 KR2011005844W WO2012020986A3 WO 2012020986 A3 WO2012020986 A3 WO 2012020986A3 KR 2011005844 W KR2011005844 W KR 2011005844W WO 2012020986 A3 WO2012020986 A3 WO 2012020986A3
Authority
WO
WIPO (PCT)
Prior art keywords
inorganic compounds
inorganic
slurry
stream
same
Prior art date
Application number
PCT/KR2011/005844
Other languages
English (en)
French (fr)
Other versions
WO2012020986A2 (ko
Inventor
노현국
이은상
박광수
박홍규
정왕모
오상승
정주형
Original Assignee
주식회사 엘지화학
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 주식회사 엘지화학 filed Critical 주식회사 엘지화학
Priority to JP2013524041A priority Critical patent/JP5657118B2/ja
Priority to CN201180036297.1A priority patent/CN103025419B/zh
Priority to EP11816602.4A priority patent/EP2604335A4/en
Publication of WO2012020986A2 publication Critical patent/WO2012020986A2/ko
Publication of WO2012020986A3 publication Critical patent/WO2012020986A3/ko
Priority to US13/743,018 priority patent/US20130129596A1/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/008—Processes carried out under supercritical conditions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/06—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002—Nozzle-type elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/38—Condensed phosphates
    • C01B25/40—Polyphosphates
    • C01B25/41—Polyphosphates of alkali metals
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/45—Phosphates containing plural metal, or metal and ammonium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G1/00—Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G15/00—Compounds of gallium, indium or thallium
    • C01G15/006—Compounds containing, besides gallium, indium, or thallium, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G17/00—Compounds of germanium
    • C01G17/006—Compounds containing, besides germanium, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/12—Manganates manganites or permanganates
    • C01G45/1221—Manganates or manganites with a manganese oxidation state of Mn(III), Mn(IV) or mixtures thereof
    • C01G45/1242—Manganates or manganites with a manganese oxidation state of Mn(III), Mn(IV) or mixtures thereof of the type [Mn2O4]-, e.g. LiMn2O4, Li[MxMn2-x]O4
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/04—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/04—Oxides; Hydroxides
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

본 발명은 수열법에 의해 무기물 슬러리를 연속적으로 제조하는 장치로서, 전구체 액상 또는 슬러리 스트림, 초임계 액상 스트림, 반응기 등을 구비하고 수열법에 의해 무기물 슬러리를 연속적으로 제조하는 반응기를 포함하고 있으며, 상기 반응기에서 전구체 액상 또는 슬러리 스트림의 유입 방향은 무기물 슬러리를 포함하는 무기물 슬러리 스트림(inorganic material stream)의 배출 방향을 기준으로 0도 내지 60도의 범위 내에 있는 것을 특징으로 하는 수열 합성 장치 및 상기 장치를 사용하여 무기물을 제조하는 방법을 제공한다.
PCT/KR2011/005844 2010-08-11 2011-08-10 무기화합물의 제조장치 및 이를 사용한 무기화합물의 제조방법 WO2012020986A2 (ko)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP2013524041A JP5657118B2 (ja) 2010-08-11 2011-08-10 無機化合物の生成デバイス、およびそれを用いた無機化合物の生成方法
CN201180036297.1A CN103025419B (zh) 2010-08-11 2011-08-10 用于制备无机化合物的装置和使用其制备无机化合物的方法
EP11816602.4A EP2604335A4 (en) 2010-08-11 2011-08-10 Production device for inorganic compounds and a production method for inorganic compounds using the same
US13/743,018 US20130129596A1 (en) 2010-08-11 2013-01-16 Device for preparing inorganic compound and method for preparing inorganic compound using the same

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR20100077475 2010-08-11
KR10-2010-0077475 2010-08-11

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US13/743,018 Continuation US20130129596A1 (en) 2010-08-11 2013-01-16 Device for preparing inorganic compound and method for preparing inorganic compound using the same

Publications (2)

Publication Number Publication Date
WO2012020986A2 WO2012020986A2 (ko) 2012-02-16
WO2012020986A3 true WO2012020986A3 (ko) 2012-05-31

Family

ID=45568045

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2011/005844 WO2012020986A2 (ko) 2010-08-11 2011-08-10 무기화합물의 제조장치 및 이를 사용한 무기화합물의 제조방법

Country Status (6)

Country Link
US (1) US20130129596A1 (ko)
EP (1) EP2604335A4 (ko)
JP (1) JP5657118B2 (ko)
KR (1) KR101269544B1 (ko)
CN (1) CN103025419B (ko)
WO (1) WO2012020986A2 (ko)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101655921B1 (ko) * 2011-11-07 2016-09-09 주식회사 엘지화학 양극 활물질의 제조장치 및 이에 구비되는 교반장치
KR101490204B1 (ko) * 2012-05-04 2015-02-06 주식회사 엘지화학 무기 화합물의 제조 장치 및 이를 사용한 무기 화합물의 제조방법
KR101498467B1 (ko) * 2012-05-07 2015-03-04 주식회사 엘지화학 무기 화합물의 제조 장치 및 이를 사용한 무기화합물의 제조방법
KR101498469B1 (ko) * 2012-05-07 2015-03-04 주식회사 엘지화학 무기 화합물의 제조 장치 및 이를 사용한 무기화합물의 제조방법
KR101655927B1 (ko) * 2012-05-30 2016-09-08 주식회사 엘지화학 양극 활물질 제조용 교반장치 및 이를 포함하는 양극 활물질의 제조장치
KR101720367B1 (ko) * 2012-05-30 2017-03-27 주식회사 엘지화학 양극 활물질 제조용 필터링 장치
KR101640629B1 (ko) * 2012-05-30 2016-07-18 주식회사 엘지화학 초임계 연속수열 합성 장치 및 방법
KR101643444B1 (ko) * 2012-05-30 2016-07-27 주식회사 엘지화학 양극 활물질 제조용 교반장치
KR101471433B1 (ko) * 2012-05-31 2014-12-10 주식회사 엘지화학 무기 입자의 제조방법
KR101522526B1 (ko) 2012-11-26 2015-05-26 주식회사 엘지화학 무기 입자의 제조방법 및 그로부터 얻어진 무기 입자
KR101565298B1 (ko) * 2012-11-27 2015-11-03 주식회사 엘지화학 무기화합물의 제조장치 및 이를 사용한 무기화합물의 제조방법
KR101565303B1 (ko) 2012-11-27 2015-11-03 주식회사 엘지화학 수열 합성 장치 및 이를 사용한 양극 활물질의 제조방법
KR101596272B1 (ko) * 2013-01-03 2016-02-22 주식회사 엘지화학 리튬 복합 전이금속 산화물 제조용 장치, 이를 이용하여 제조된 리튬 복합 전이금속 산화물, 및 그 제조방법
EP3092067A1 (en) * 2014-01-08 2016-11-16 Teknologisk Institut Method of preparing a catalyst structure
FR3016536A1 (fr) * 2014-01-21 2015-07-24 Innoveox Dispositif d'injection d'oxydant pour une installation de traitement d'un effluent aqueux par oxydation hydrothermale
CN112374473B (zh) * 2020-11-11 2022-04-19 深圳大学 一种基于含酚废水合成酚类有机物掺杂g-C3N4的方法
US20220251728A1 (en) * 2021-02-08 2022-08-11 Uchicago Argonne, Llc Continuous hydrothermal manufacturing method for concentration-gradient monocrystalline battery material

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11267607A (ja) * 1998-03-26 1999-10-05 Ube Ind Ltd 廃棄物の処理方法およびその装置
JP2001246239A (ja) * 2000-03-06 2001-09-11 Kurita Water Ind Ltd 水熱反応方法および装置
JP2002102672A (ja) * 2000-09-29 2002-04-09 Kurita Water Ind Ltd 水熱反応装置および方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9413202D0 (en) * 1994-06-30 1994-08-24 Univ Bradford Method and apparatus for the formation of particles
GB9703673D0 (en) * 1997-02-21 1997-04-09 Bradford Particle Design Ltd Method and apparatus for the formation of particles
JP2001290231A (ja) * 2000-04-06 2001-10-19 Fuji Photo Film Co Ltd ハロゲン化銀乳剤の製造方法及び装置
JP2003107608A (ja) * 2001-09-28 2003-04-09 Fuji Photo Film Co Ltd ハロゲン化銀乳剤の製造方法及び装置
US7125453B2 (en) * 2002-01-31 2006-10-24 General Electric Company High temperature high pressure capsule for processing materials in supercritical fluids
GB0402963D0 (en) * 2004-02-11 2004-03-17 Univ Nottingham Counter current mixing device for two different fluids
JP5405126B2 (ja) * 2006-02-17 2014-02-05 エルジー・ケム・リミテッド リチウム−金属複合酸化物の製造方法
JP4840916B2 (ja) * 2006-07-06 2011-12-21 独立行政法人産業技術総合研究所 高温高圧マイクロミキサー
JP5985134B2 (ja) * 2009-01-23 2016-09-06 関東電化工業株式会社 無機微粒子の製造方法及びその製造装置

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11267607A (ja) * 1998-03-26 1999-10-05 Ube Ind Ltd 廃棄物の処理方法およびその装置
JP2001246239A (ja) * 2000-03-06 2001-09-11 Kurita Water Ind Ltd 水熱反応方法および装置
JP2002102672A (ja) * 2000-09-29 2002-04-09 Kurita Water Ind Ltd 水熱反応装置および方法

Also Published As

Publication number Publication date
US20130129596A1 (en) 2013-05-23
JP5657118B2 (ja) 2015-01-21
JP2013545588A (ja) 2013-12-26
EP2604335A2 (en) 2013-06-19
WO2012020986A2 (ko) 2012-02-16
EP2604335A4 (en) 2017-05-17
CN103025419B (zh) 2016-08-03
KR20120015278A (ko) 2012-02-21
KR101269544B1 (ko) 2013-06-04
CN103025419A (zh) 2013-04-03

Similar Documents

Publication Publication Date Title
WO2012020986A3 (ko) 무기화합물의 제조장치 및 이를 사용한 무기화합물의 제조방법
WO2015094948A8 (en) Production of upgraded petroleum by supercritical water
WO2012087628A3 (en) Production of polycrystalline silicon by the thermal decomposition of dichlorosilane in a fluidized bed reactor
EP2193865A4 (en) METHOD FOR PRODUCING MAGNETIC FUZINE PARTICLES, MAGNETIC FUZZES OBTAINED THEREOF, AND METHOD FOR PRODUCING PRODUCTS MADE FROM MAGNETIC FLUID OR MAGNETIC MATERIAL
EP2530049A4 (en) METHOD FOR PRODUCING A PULVER FROM ALUMINUM NITRIDE BALLS AND ALUMINUM NITRIDE BALL POWDER PRODUCED IN THIS METHOD
BR112013014790A2 (pt) processo para produzir propileno a partir de gás de síntese pela produção e desidratação de propanol fermentativo
WO2006104925A3 (en) Metal powders and methods for producing the same
WO2010117204A3 (ko) 이온성 액체를 이용한 금속 나노구조체의 제조방법
NZ629687A (en) Biorefining method
WO2010102980A9 (en) Process for preparing substituted 2-nitrobiphenyls
MX340657B (es) Suspension acuosa de silice amorfa y metodo para su produccion.
WO2012059485A3 (en) Continuous production and reaction of a diazo compound
UA111064C2 (uk) Спосіб одержання легких олефінів із синтез-газу
WO2011140513A3 (en) Patterned nanowires
WO2015084497A3 (en) Method and system of dehydrating a feed stream processed in a distillation tower
WO2015017478A3 (en) SYNTHESIS OF CdSe/ZnS CORE/SHELL SEMICONDUCTOR NANOWIRES
WO2018013043A8 (en) Synthesis of vanadium pentoxide nanosheets
WO2012074691A3 (en) Process and apparatus for recovering catalytic product
WO2013049314A3 (en) Production of polycrystalline silicon by the thermal decomposition of silane in a fluidized bed reactor
MX2014015409A (es) Metodo para la granulacion de un liquido en particular para la granulacion de la urea.
WO2008115150A3 (en) Process for synthesis of clay particles
WO2013065070A8 (en) Amorphous form of cabazitaxel and process for its preparation
MX2009013743A (es) Sistema y proceso para producir alcohol.
WO2012129065A3 (en) Process to improve formulations of hydrocarbon conversion catalysts through removal and modification of detrimental particles and reuse of modified fractions
WO2012161502A3 (ko) 실리카 캡슐화된 단분자 나노효소입자 제조방법 및 이를 통해 제조된 단분자 나노효소입자

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 201180036297.1

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 11816602

Country of ref document: EP

Kind code of ref document: A2

WWE Wipo information: entry into national phase

Ref document number: 2011816602

Country of ref document: EP

ENP Entry into the national phase

Ref document number: 2013524041

Country of ref document: JP

Kind code of ref document: A

NENP Non-entry into the national phase

Ref country code: DE