WO2009044879A1 - 金属酸化物複合ゾル、コーティング組成物及び光学部材 - Google Patents

金属酸化物複合ゾル、コーティング組成物及び光学部材 Download PDF

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Publication number
WO2009044879A1
WO2009044879A1 PCT/JP2008/068087 JP2008068087W WO2009044879A1 WO 2009044879 A1 WO2009044879 A1 WO 2009044879A1 JP 2008068087 W JP2008068087 W JP 2008068087W WO 2009044879 A1 WO2009044879 A1 WO 2009044879A1
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Prior art keywords
oxide composite
metal oxide
coating composition
optical member
molar ratio
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PCT/JP2008/068087
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English (en)
French (fr)
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Yoshinari Koyama
Motoko Asada
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Nissan Chemical Industries, Ltd.
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Application filed by Nissan Chemical Industries, Ltd. filed Critical Nissan Chemical Industries, Ltd.
Priority to EP08836512.7A priority Critical patent/EP2213623B1/en
Priority to CN2008801099981A priority patent/CN101815675B/zh
Priority to US12/681,524 priority patent/US20100239872A1/en
Priority to JP2009536118A priority patent/JP5182533B2/ja
Publication of WO2009044879A1 publication Critical patent/WO2009044879A1/ja
Priority to US14/294,744 priority patent/US20140285897A1/en

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00—Compounds of tungsten
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
    • G02B1/14—Protective coatings, e.g. hard coatings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/006—Compounds containing, besides zirconium, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G30/00—Compounds of antimony
    • C01G30/004—Oxides; Hydroxides; Oxyacids
    • C01G30/005—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00—Compounds of tungsten
    • C01G41/006—Compounds containing, besides tungsten, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00—Compounds of tungsten
    • C01G41/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0081—Composite particulate pigments or fillers, i.e. containing at least two solid phases, except those consisting of coated particles of one compound
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
    • G02B1/11—Anti-reflection coatings
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
    • C01P2004/82—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
    • C01P2004/84—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases one phase coated with the other
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • C01P2006/82—Compositional purity water content
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • General Physics & Mathematics (AREA)
  • Nanotechnology (AREA)
  • Composite Materials (AREA)
  • Optics & Photonics (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Paints Or Removers (AREA)
  • Surface Treatment Of Optical Elements (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Silicon Compounds (AREA)
  • Eyeglasses (AREA)

Abstract

【課題】光励起によるコロイド粒子の変色がほぼ完全に抑制され、耐光性、耐候性に優れた酸化チタンを含む高い屈折率の金属酸化物複合コロイド粒子のゾルを提供する。 【解決手段】２～５０ｎｍの一次粒子径を有し、ＳｎＯ2／ＴｉＯ2モル比として０．１～１．０、ＺｒＯ2／ＴｉＯ2モル比として０．１～０．４、及びＷＯ3／ＴｉＯ2モル比として０．０３～０．１５である酸化チタン－酸化スズ－酸化ジルコニウム－酸化タングステン複合コロイド粒子による。
PCT/JP2008/068087 2007-10-03 2008-10-03 金属酸化物複合ゾル、コーティング組成物及び光学部材 WO2009044879A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP08836512.7A EP2213623B1 (en) 2007-10-03 2008-10-03 Metal oxide composite sol, coating composition, and optical member
CN2008801099981A CN101815675B (zh) 2007-10-03 2008-10-03 金属氧化物复合溶胶、涂布组合物和光学部件
US12/681,524 US20100239872A1 (en) 2007-10-03 2008-10-03 Metal oxide composite sol, coating composition, and optical member
JP2009536118A JP5182533B2 (ja) 2007-10-03 2008-10-03 金属酸化物複合ゾル、コーティング組成物及び光学部材
US14/294,744 US20140285897A1 (en) 2007-10-03 2014-06-03 Metal oxide composite sol, coating composition, and optical member

Applications Claiming Priority (8)

Application Number Priority Date Filing Date Title
JP2007260148 2007-10-03
JP2007-260149 2007-10-03
JP2007-260148 2007-10-03
JP2007260149 2007-10-03
JP2008-117586 2008-04-28
JP2008117588 2008-04-28
JP2008-117588 2008-04-28
JP2008117586 2008-04-28

Related Child Applications (2)

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US12/681,524 A-371-Of-International US20100239872A1 (en) 2007-10-03 2008-10-03 Metal oxide composite sol, coating composition, and optical member
US14/294,744 Division US20140285897A1 (en) 2007-10-03 2014-06-03 Metal oxide composite sol, coating composition, and optical member

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US (2) US20100239872A1 (ja)
EP (1) EP2213623B1 (ja)
JP (1) JP5182533B2 (ja)
KR (1) KR20100076000A (ja)
CN (1) CN101815675B (ja)
TW (1) TWI428282B (ja)
WO (1) WO2009044879A1 (ja)

Cited By (7)

* Cited by examiner, † Cited by third party
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WO2011090085A1 (ja) * 2010-01-19 2011-07-28 日産化学工業株式会社 変性酸化第二セリウムコロイド粒子及びその製造方法
JP2012027300A (ja) * 2010-07-26 2012-02-09 Seiko Epson Corp レンズの製造方法及びレンズ
WO2015129616A1 (ja) * 2014-02-27 2015-09-03 富士フイルム株式会社 水性組成物、その製造方法、ハードコートフィルム、積層フィルム、透明導電性フィルム、およびタッチパネル
JP2016074797A (ja) * 2014-10-03 2016-05-12 富士フイルム株式会社 シロキサン樹脂組成物、これを用いた透明硬化物、透明画素、マイクロレンズ、固体撮像素子
JP2016074867A (ja) * 2014-10-03 2016-05-12 富士フイルム株式会社 シロキサン樹脂組成物、これを用いた透明硬化物、透明画素、マイクロレンズ、固体撮像素子
JP2016522152A (ja) * 2013-06-03 2016-07-28 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 無機赤色顔料
WO2016121263A1 (ja) * 2015-01-29 2016-08-04 富士フイルム株式会社 シロキサン樹脂組成物、これを用いた透明硬化物、透明画素、マイクロレンズ、固体撮像素子

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CN102781821B (zh) 2010-01-19 2015-01-07 日产化学工业株式会社 硅烷表面处理金属氧化物微粒和其制造方法
FR2967992B1 (fr) * 2010-11-26 2015-05-29 Commissariat Energie Atomique Preparation de sols d'oxydes metalliques stables, utiles notamment pour la fabrication de films minces a proprietes optiques et resistants a l'abrasion
US20130253161A1 (en) * 2010-12-08 2013-09-26 Masaaki Amako Methods Of Modifying Metal-Oxide Nanoparticles
CN103717535B (zh) * 2011-06-03 2016-02-10 日产化学工业株式会社 含有二氧化硅-二氧化锡复合氧化物被覆二氧化钛的金属氧化物粒子
DE102011083960A1 (de) 2011-10-04 2013-04-04 Carl Zeiss Vision International Gmbh Zusammensetzung für die Herstellung einer Beschichtung mit hoher Haft- und Kratzfestigkeit
CN103922397B (zh) * 2013-01-15 2017-05-31 日挥触媒化成株式会社 改性氧化锆微粒粉末、改性氧化锆微粒分散溶胶及其制造方法
JP5889261B2 (ja) * 2013-10-18 2016-03-22 第一稀元素化学工業株式会社 酸化ジルコニウム−酸化チタン複合ゾル及びその製造方法
KR101713941B1 (ko) * 2015-01-15 2017-03-08 정청식 금속물질 발열용액이 도포된 장판
US10444416B2 (en) * 2015-12-24 2019-10-15 Board Of Trustees Of Northern Illinois University Near infrared absorbing agent and method of making near infrared absorbing agent
US10941250B2 (en) * 2016-03-11 2021-03-09 Panasonic Intellectual Property Management Co., Ltd. Antistatic material, method for producing same, and antistatic film
CN108698851B (zh) * 2016-03-31 2020-11-10 日产化学工业株式会社 被膜形成用组合物及其制造方法
WO2017170275A1 (ja) * 2016-03-31 2017-10-05 日産化学工業株式会社 両親媒性の有機シラン化合物が結合した無機酸化物微粒子、その有機溶媒分散液及び被膜形成用組成物
CN106590032A (zh) * 2016-12-09 2017-04-26 湖南科莱新材料有限公司 一种铈黄复合功能材料及制备方法
JP7060583B2 (ja) * 2017-03-31 2022-04-26 日揮触媒化成株式会社 鉄含有ルチル型酸化チタン微粒子分散液の製造方法、鉄含有ルチル型酸化チタン微粒子およびその用途
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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011090085A1 (ja) * 2010-01-19 2011-07-28 日産化学工業株式会社 変性酸化第二セリウムコロイド粒子及びその製造方法
JP2012027300A (ja) * 2010-07-26 2012-02-09 Seiko Epson Corp レンズの製造方法及びレンズ
JP2016522152A (ja) * 2013-06-03 2016-07-28 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 無機赤色顔料
WO2015129616A1 (ja) * 2014-02-27 2015-09-03 富士フイルム株式会社 水性組成物、その製造方法、ハードコートフィルム、積層フィルム、透明導電性フィルム、およびタッチパネル
JP2015160885A (ja) * 2014-02-27 2015-09-07 富士フイルム株式会社 水性組成物とその製造方法、ハードコートフィルム、積層フィルム、透明導電性フィルム、およびタッチパネル
JP2016074797A (ja) * 2014-10-03 2016-05-12 富士フイルム株式会社 シロキサン樹脂組成物、これを用いた透明硬化物、透明画素、マイクロレンズ、固体撮像素子
JP2016074867A (ja) * 2014-10-03 2016-05-12 富士フイルム株式会社 シロキサン樹脂組成物、これを用いた透明硬化物、透明画素、マイクロレンズ、固体撮像素子
WO2016121263A1 (ja) * 2015-01-29 2016-08-04 富士フイルム株式会社 シロキサン樹脂組成物、これを用いた透明硬化物、透明画素、マイクロレンズ、固体撮像素子
JPWO2016121263A1 (ja) * 2015-01-29 2017-08-03 富士フイルム株式会社 シロキサン樹脂組成物、これを用いた透明硬化物、透明画素、マイクロレンズ、固体撮像素子
JP2019173016A (ja) * 2015-01-29 2019-10-10 富士フイルム株式会社 シロキサン樹脂組成物、これを用いた透明硬化物、透明画素、マイクロレンズ、固体撮像素子

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TW200934733A (en) 2009-08-16
EP2213623A1 (en) 2010-08-04
JP5182533B2 (ja) 2013-04-17
CN101815675B (zh) 2013-01-16
US20140285897A1 (en) 2014-09-25
KR20100076000A (ko) 2010-07-05
EP2213623A4 (en) 2012-12-05
JPWO2009044879A1 (ja) 2011-02-10
US20100239872A1 (en) 2010-09-23
TWI428282B (zh) 2014-03-01
CN101815675A (zh) 2010-08-25
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