WO2008105456A1 - 金属ナノ粒子分散液及びその製造方法並びに金属ナノ粒子の合成方法 - Google Patents

金属ナノ粒子分散液及びその製造方法並びに金属ナノ粒子の合成方法 Download PDF

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Publication number
WO2008105456A1
WO2008105456A1 PCT/JP2008/053399 JP2008053399W WO2008105456A1 WO 2008105456 A1 WO2008105456 A1 WO 2008105456A1 JP 2008053399 W JP2008053399 W JP 2008053399W WO 2008105456 A1 WO2008105456 A1 WO 2008105456A1
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WO
WIPO (PCT)
Prior art keywords
metal nanoparticle
dispersion solution
synthesis
producing
production
Prior art date
Application number
PCT/JP2008/053399
Other languages
English (en)
French (fr)
Inventor
Kazuhiko Yamasaki
Airi Katagiri
Masahide Arai
Yoshiaki Takata
Toshiharu Hayashi
Original Assignee
Mitsubishi Materials Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP2008038277A external-priority patent/JP5320769B2/ja
Application filed by Mitsubishi Materials Corporation filed Critical Mitsubishi Materials Corporation
Priority to CN200880006238.8A priority Critical patent/CN101622090B/zh
Priority to US12/528,625 priority patent/US9580810B2/en
Publication of WO2008105456A1 publication Critical patent/WO2008105456A1/ja
Priority to US14/725,828 priority patent/US9580811B2/en

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B22F1/0545—Dispersions or suspensions of nanosized particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C5/00—Alloys based on noble metals
    • C22C5/06—Alloys based on silver
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00—Obtaining noble metals
    • C22B11/04—Obtaining noble metals by wet processes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00—General methods of reducing to metals

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

　　本発明の目的は、形状や粒径を幅広い範囲で制御することできる金属ナノ粒子分散液の製造方法、並びに分散安定性に優れた金属ナノ粒子分散液及びその製造方法を提供することにある。また、本発明の目的は、導電材料として有用な２～６×１０－６Ω・ｃｍの体積抵抗率が得られる、金属ナノ粒子分散液及びその製造方法を提供することにある。さらに、本発明の目的は、腐食性材料を含まずに不溶性の金属塩から金属ナノ粒子を合成し、導電材料として用いるのに好適な金属ナノ粒子を製造し得る金属ナノ粒子の合成方法を提供することにある。
PCT/JP2008/053399 2007-02-27 2008-02-27 金属ナノ粒子分散液及びその製造方法並びに金属ナノ粒子の合成方法 WO2008105456A1 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN200880006238.8A CN101622090B (zh) 2007-02-27 2008-02-27 金属纳米颗粒分散液及其制备方法以及金属纳米颗粒的合成方法
US12/528,625 US9580810B2 (en) 2007-02-27 2008-02-27 Dispersion of metal nanoparticles, method for producing the same, and method for synthesizing metal nanoparticles
US14/725,828 US9580811B2 (en) 2007-02-27 2015-05-29 Dispersion of metal nanoparticles, method for producing the same, and method for synthesizing metal nanoparticles

Applications Claiming Priority (28)

Application Number Priority Date Filing Date Title
JP2007047246 2007-02-27
JP2007-047246 2007-02-27
JP2008007650 2008-01-17
JP2008-007658 2008-01-17
JP2008007658 2008-01-17
JP2008-007669 2008-01-17
JP2008007656 2008-01-17
JP2008-007650 2008-01-17
JP2008-007656 2008-01-17
JP2008007670 2008-01-17
JP2008007669 2008-01-17
JP2008011340 2008-01-22
JP2008011334 2008-01-22
JP2008-011340 2008-01-22
JP2008-011343 2008-01-22
JP2008-011334 2008-01-22
JP2008011343 2008-01-22
JP2008-038283 2008-02-20
JP2008-038277 2008-02-20
JP2008038281 2008-02-20
JP2008038283 2008-02-20
JP2008038277A JP5320769B2 (ja) 2007-02-27 2008-02-20 金属ナノ粒子の合成方法
JP2008-038285 2008-02-20
JP2008038285 2008-02-20
JP2008-038281 2008-02-20
JP2008-038280 2008-02-20
JP2008038280 2008-02-20
JP2008-007670 2008-07-17

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US12/528,625 A-371-Of-International US9580810B2 (en) 2007-02-27 2008-02-27 Dispersion of metal nanoparticles, method for producing the same, and method for synthesizing metal nanoparticles
US14/725,828 Continuation US9580811B2 (en) 2007-02-27 2015-05-29 Dispersion of metal nanoparticles, method for producing the same, and method for synthesizing metal nanoparticles

Publications (1)

Publication Number Publication Date
WO2008105456A1 true WO2008105456A1 (ja) 2008-09-04

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PCT/JP2008/053399 WO2008105456A1 (ja) 2007-02-27 2008-02-27 金属ナノ粒子分散液及びその製造方法並びに金属ナノ粒子の合成方法

Country Status (2)

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KR (1) KR101474040B1 (ja)
WO (1) WO2008105456A1 (ja)

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010095796A (ja) * 2008-10-14 2010-04-30 Xerox Corp カルボン酸安定化銀ナノ粒子を製造するためのプロセス
JP2010116625A (ja) * 2008-10-17 2010-05-27 Mitsubishi Materials Corp 金属ナノ粒子の合成方法
JP2010116626A (ja) * 2008-10-17 2010-05-27 Mitsubishi Materials Corp 金属ナノ粒子の合成方法
JP2011021271A (ja) * 2008-12-26 2011-02-03 Dowa Electronics Materials Co Ltd 微小銀粒子粉末とその製造方法および該粉末を使用した銀ペーストとその利用方法
WO2012071117A1 (en) * 2010-11-23 2012-05-31 Carestream Health, Inc. Nanowire preparation methods, compositions, and articles
CN102576580A (zh) * 2009-09-08 2012-07-11 E.I.内穆尔杜邦公司 用于光伏电池的导体
CN102744416A (zh) * 2011-04-19 2012-10-24 同济大学 一种二十面体晶态纳米镍钴合金的制备方法
EP2610023A1 (en) * 2010-08-27 2013-07-03 DOWA Electronics Materials Co., Ltd. Low-temperature sinterable silver nanoparticle composition and electronic component formed using that composition
JP2015078437A (ja) * 2008-12-26 2015-04-23 Ｄｏｗａエレクトロニクス株式会社 微小銀粒子粉末および該粉末を使用した銀ペーストの製造方法
WO2016129368A1 (ja) * 2015-02-13 2016-08-18 三菱マテリアル株式会社 銀粉及びペースト状組成物並びに銀粉の製造方法
CN109865844A (zh) * 2018-03-16 2019-06-11 南京林业大学 一种片状钴粉的制备方法
CN110653380A (zh) * 2019-10-31 2020-01-07 合肥工业大学 一种常温下在醇相中快速制备金纳米颗粒的方法
CN111702186A (zh) * 2020-07-23 2020-09-25 苏州大学 一种尺寸可调的金纳米粒子的制备方法
CN112033924A (zh) * 2020-08-25 2020-12-04 盐城工学院 2-羟基丙酸-金银复合纳米粒子、制备方法及其应用
JPWO2023013572A1 (ja) * 2021-08-03 2023-02-09

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KR101069480B1 (ko) * 2010-01-04 2011-09-30 인하대학교 산학협력단 슈퍼 커패시터용 금속 옥살레이트 나노구조 제조방법
KR101701819B1 (ko) 2011-09-08 2017-02-13 김명진 금속의 제조방법
KR101741158B1 (ko) 2015-09-09 2017-05-29 성균관대학교산학협력단 꽃-모양 금속 나노 입자 및 이의 제조 방법
KR101829915B1 (ko) * 2016-06-28 2018-02-19 성균관대학교산학협력단 금속 나노와이어 및 이의 제조 방법
CN109478442B (zh) * 2016-08-25 2020-06-19 Dic株式会社 金属纳米粒子水分散液
KR102061576B1 (ko) 2018-02-23 2020-01-02 광운대학교 산학협력단 은-팔라듐 합금 나노입자 제조 방법
KR102061575B1 (ko) 2018-02-23 2020-01-02 광운대학교 산학협력단 금-은-팔라듐 합금 나노입자 제조 방법
KR102247820B1 (ko) * 2019-04-26 2021-05-04 충북대학교 산학협력단 항균성 고분자 복합체 및 그 제조방법
KR102279083B1 (ko) * 2020-09-25 2021-07-16 서울과학기술대학교 산학협력단 바인더 프리 구리 페이스트 및 이를 이용한 소결 접합방법

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JP2000087122A (ja) * 1998-09-14 2000-03-28 Mitsubishi Materials Corp 金属微粒子分散液とその製造方法
JP2003160876A (ja) * 2001-11-22 2003-06-06 Sumitomo Osaka Cement Co Ltd 無電解メッキ用触媒および金属メッキパターンの形成方法
JP2006045655A (ja) * 2004-08-09 2006-02-16 Mitsubishi Materials Corp 銀ナノ粒子とその製造方法

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JP5032005B2 (ja) * 2005-07-05 2012-09-26 三井金属鉱業株式会社 高結晶銀粉及びその高結晶銀粉の製造方法

Patent Citations (3)

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JP2000087122A (ja) * 1998-09-14 2000-03-28 Mitsubishi Materials Corp 金属微粒子分散液とその製造方法
JP2003160876A (ja) * 2001-11-22 2003-06-06 Sumitomo Osaka Cement Co Ltd 無電解メッキ用触媒および金属メッキパターンの形成方法
JP2006045655A (ja) * 2004-08-09 2006-02-16 Mitsubishi Materials Corp 銀ナノ粒子とその製造方法

Cited By (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010095796A (ja) * 2008-10-14 2010-04-30 Xerox Corp カルボン酸安定化銀ナノ粒子を製造するためのプロセス
JP2010116625A (ja) * 2008-10-17 2010-05-27 Mitsubishi Materials Corp 金属ナノ粒子の合成方法
JP2010116626A (ja) * 2008-10-17 2010-05-27 Mitsubishi Materials Corp 金属ナノ粒子の合成方法
JP2011021271A (ja) * 2008-12-26 2011-02-03 Dowa Electronics Materials Co Ltd 微小銀粒子粉末とその製造方法および該粉末を使用した銀ペーストとその利用方法
US9721694B2 (en) 2008-12-26 2017-08-01 Dowa Electronics Materials Co., Ltd. Fine silver particle powder, method for manufacturing the same, silver paste using the powder and method of use of the paste
JP2015078437A (ja) * 2008-12-26 2015-04-23 Ｄｏｗａエレクトロニクス株式会社 微小銀粒子粉末および該粉末を使用した銀ペーストの製造方法
US9034214B2 (en) 2008-12-26 2015-05-19 Dowa Electronics Materials Co., Ltd. Fine silver particle powder, method for manufacturing the same, silver paste using the powder, and method of use of the paste
CN102576580A (zh) * 2009-09-08 2012-07-11 E.I.内穆尔杜邦公司 用于光伏电池的导体
EP2610023A4 (en) * 2010-08-27 2015-07-22 Dowa Electronics Materials Co Ltd FRITTABLE SILVER NANOPARTICLE COMPOSITION AT LOW TEMPERATURE AND ELECTRONIC COMPONENT FORMED USING THE SAME
EP2610023A1 (en) * 2010-08-27 2013-07-03 DOWA Electronics Materials Co., Ltd. Low-temperature sinterable silver nanoparticle composition and electronic component formed using that composition
WO2012071117A1 (en) * 2010-11-23 2012-05-31 Carestream Health, Inc. Nanowire preparation methods, compositions, and articles
US8613888B2 (en) 2010-11-23 2013-12-24 Carestream Health, Inc. Nanowire preparation methods, compositions, and articles
CN102744416A (zh) * 2011-04-19 2012-10-24 同济大学 一种二十面体晶态纳米镍钴合金的制备方法
CN102744416B (zh) * 2011-04-19 2013-12-25 同济大学 一种二十面体晶态纳米镍钴合金的制备方法
US11587695B2 (en) 2015-02-13 2023-02-21 Mitsubishi Materials Corporation Silver powder, paste composition, and method of producing silver powder
JP2016148089A (ja) * 2015-02-13 2016-08-18 三菱マテリアル株式会社 銀粉及びペースト状組成物並びに銀粉の製造方法
WO2016129368A1 (ja) * 2015-02-13 2016-08-18 三菱マテリアル株式会社 銀粉及びペースト状組成物並びに銀粉の製造方法
CN109865844A (zh) * 2018-03-16 2019-06-11 南京林业大学 一种片状钴粉的制备方法
CN109865844B (zh) * 2018-03-16 2022-03-15 南京林业大学 一种片状钴粉的制备方法
CN110653380A (zh) * 2019-10-31 2020-01-07 合肥工业大学 一种常温下在醇相中快速制备金纳米颗粒的方法
CN110653380B (zh) * 2019-10-31 2022-08-19 合肥工业大学 一种常温下在醇相中快速制备金纳米颗粒的方法
CN111702186A (zh) * 2020-07-23 2020-09-25 苏州大学 一种尺寸可调的金纳米粒子的制备方法
CN111702186B (zh) * 2020-07-23 2023-03-24 苏州大学 一种尺寸可调的金纳米粒子的制备方法
CN112033924A (zh) * 2020-08-25 2020-12-04 盐城工学院 2-羟基丙酸-金银复合纳米粒子、制备方法及其应用
WO2023013572A1 (ja) * 2021-08-03 2023-02-09 三菱マテリアル株式会社 金属インク、金属インクの製造方法、及び金属層の製造方法
JPWO2023013572A1 (ja) * 2021-08-03 2023-02-09
JP7517615B2 (ja) 2021-08-03 2024-07-17 三菱マテリアル株式会社 金属インク、金属インクの製造方法、及び金属層の製造方法

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KR20090115854A (ko) 2009-11-09

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