WO2007136956A1 - Procédé de fabrication d'un dispositif électroluminescent à l'aide d'une composition contenant du silicium - Google Patents
Procédé de fabrication d'un dispositif électroluminescent à l'aide d'une composition contenant du silicium Download PDFInfo
- Publication number
- WO2007136956A1 WO2007136956A1 PCT/US2007/067266 US2007067266W WO2007136956A1 WO 2007136956 A1 WO2007136956 A1 WO 2007136956A1 US 2007067266 W US2007067266 W US 2007067266W WO 2007136956 A1 WO2007136956 A1 WO 2007136956A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- light emitting
- optical element
- silicon
- emitting diode
- film
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 113
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- 239000000463 material Substances 0.000 claims description 37
- -1 5-cyclopentadienyl Chemical group 0.000 claims description 34
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Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L33/00—Semiconductor devices having potential barriers specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
- H01L33/48—Semiconductor devices having potential barriers specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof characterised by the semiconductor body packages
- H01L33/58—Optical field-shaping elements
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L2924/00—Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
- H01L2924/0001—Technical content checked by a classifier
- H01L2924/0002—Not covered by any one of groups H01L24/00, H01L24/00 and H01L2224/00
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L2933/00—Details relating to devices covered by the group H01L33/00 but not provided for in its subgroups
- H01L2933/0008—Processes
- H01L2933/0033—Processes relating to semiconductor body packages
- H01L2933/005—Processes relating to semiconductor body packages relating to encapsulations
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L2933/00—Details relating to devices covered by the group H01L33/00 but not provided for in its subgroups
- H01L2933/0008—Processes
- H01L2933/0033—Processes relating to semiconductor body packages
- H01L2933/0058—Processes relating to semiconductor body packages relating to optical field-shaping elements
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L33/00—Semiconductor devices having potential barriers specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
- H01L33/48—Semiconductor devices having potential barriers specially adapted for light emission; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof characterised by the semiconductor body packages
- H01L33/52—Encapsulations
- H01L33/56—Materials, e.g. epoxy or silicone resin
Definitions
- the invention relates to a method of making a light emitting device, and particularly, to a method of attaching an optical element to a light emitting diode (LED) with a photopolymerizable silicon-containing composition.
- LED light emitting diode
- the optical element may comprise a lens, an optical film such as a multilayer optical film or brightness enhancing film, a phosphor- reflector assembly, or a combination thereof.
- the light emitting device may comprise an LED mounted in a variety of ways such as in a ceramic or polymeric package, or on a circuit board.
- the optical element may contact the LED or it may be spaced apart from the LED.
- the method provides a way to attach an optical element to an LED using a photopolymerizable composition with relatively rapid cure mechanisms even at relatively low temperatures.
- FIG. 2 shows an exemplary light emitting device wherein the optical element is a lens and the LED is in a recessed cavity.
- FIG. 3 shows exemplary light emitting devices wherein the optical element is a phosphor-reflector assembly.
- the advantages of using radiation-activated hydrosilylation to cure the photopolymerizable composition include (1) the ability to cure the photopolymerizable composition without subjecting the LED, the substrate to which it is attached, or any other materials present in the package or system, to potentially harmful temperatures, (2) the ability to formulate one-part photopolymerizable compositions that display long working times in the absence of inhibitors (also known as bath life or shelf life), (3) the ability to cure the photopolymerizable composition on demand at the discretion of the user, and (4) the ability to simplify the formulation process by avoiding the need for two-part formulations as is typically required for thermally curable hydrosilylation compositions.
- the molar ratio of silicon-bonded hydrogen atoms to aliphatic unsaturation in the silicon-containing resin may range from 0.5 to 10.0 mol/mol, preferably from 0.8 to 4.0 mol/mol, and more preferably from 1.0 to 3.0 mol/mol.
- the phosphor layer may consist of a blend of different types of phosphors in a single layer or a series of layers, each containing one or more types of phosphors.
- the inorganic phosphor particles in the phosphor layer may vary in size (e.g., diameter) and they may be segregated such that the average particle size is not uniform across the cross-section of the siloxane layer in which they are incorporated.
- Photoinitiators can optionally be included in the photopolymerizable composition to increase the overall rate of the curing process (or hydrosilylation reaction).
- Useful photoinitiators include, for example, monoketals of ⁇ -diketones or ⁇ -ketoaldehydes and acyloins and their corresponding ethers (such as those disclosed in U.S. Pat. No. 6,376,569 (Oxman et al.)). If used, such photoinitiators are preferably included in the photopolymerizable composition in an amount of no greater than 50,000 parts by weight, and more preferably no greater than 5000 parts by weight, per one million parts of the composition.
- Such catalyst inhibitors are preferably included in the photopolymerizable composition in an amount not to exceed the amount of the metal- containing catalyst on a mole basis.
- the optical element may comprise a lens to control the directionality of light in some way, typically upwards and away and/or at the sides of the light emitting device.
- Exemplary light emitting devices 10 comprising exemplary lenses 12 are shown in FIG. 1.
- the lens may comprise a simple lens having a spherical surface such as a hemispherical shape
- the optical element 12a may also comprise a complex lens having some combination of convex and/or concave surfaces, for example, an aplanatic lens.
- the lens may also comprise a combination of shapes, for example, it may have sawtooth-like shapes and a cusp shape 12d.
- the lens comprises a transparent material such as a polymer, glass, quartz, fused silica, ceramic, or the like.
- the lens may have a refractive index typically in the range of from about 1.4 to about 1.6, preferably about 1.5 to 1.55, depending on the particular lens.
- the lens is typically prefabricated, and as shown in FIG. 1, it may have a concave underside. In this case, the lens may be placed in contact with the photopolymerizable composition 18 while it is in a deformable state (not completely cured) and positioned relative to the LED such that air and excess composition are expelled. As shown in FIG. 1, it may have a concave underside. In this case, the lens may be placed in contact with the photopolymerizable composition 18 while it is in a deformable state (not completely cured) and positioned relative to the LED such that air and excess composition are expelled. As shown in FIG.
- a fluorescent material may be incorporated into the light emitting device for converting the color of at least some of the light emitted by the light emitting diode.
- the fluorescent material may be dispersed throughout the photopolymerizable material or disposed on the underside of the lens that is adjacent the photopolymerizable material.
- the optical element may comprise an optical film that can manage light such that the light is intentionally enhanced, manipulated, controlled, maintained, transmitted, reflected, refracted, absorbed, etc. Examples of optical films include reflective polarizing films, absorbing polarizing films, retro-reflective films, light guides, diffusive films, brightness enhancement films, glare control films, protective films, privacy films, or a combination thereof.
- the optical film may comprise any material suitable for use in optical applications. Exemplary properties include optical effectiveness over diverse portions of the ultraviolet, visible, and infrared regions, optical clarity, high index of refraction, durability, and environmental stability. In some cases, the optical film may be substantially specular, absorbing substantially no light over a predetermined wavelength region of interest; i.e., substantially all light over the region that falls on the surface of a first or second optical layer is reflected or transmitted.
- the optical film comprises a condensation or addition polymer, a blend thereof, or a polymer that is some combination thereof.
- condensation polymers include polyesters, polycarbonates, cellulose acetate esters, polyurethanes, polyamides, polyimides, poly(meth)acrylates, and the like.
- addition polymers include poly(meth)acrylates, polystyrenes, polyolefins, polypropylene, cyclic olefins, epoxies, polyvinyl chloride, polyvinylidene fluoride, polyethers, cellulose acetates, polyethersulfone, polysulfone, fluorinated ethylenepropylene (FEP), and the like.
- the optical films may also comprise polymers derived from metal-catalyzed polymerizations such as polyorganosiloxanes formed by hydros ilylation reactions.
- the optical film may also comprise a phosphor layer, diffusive layer, matte layer, abrasion resistant layer, layer for chemical or UV protection, support layer, magnetic shield layer, adhesive layer, primer layer, skin layer, dichroic polarizer layer, or combinations thereof.
- useful support layers include polycarbonate, polyester, acrylic, metal, or glass.
- the one or more additional layers may be extruded with other layers of the optical film, coated, or laminated.
- light emitting device 30 comprises a phosphor-reflector assembly 32 as the optical film.
- the phosphor-reflector assembly comprises a layer of a phosphor material 34 disposed on reflector 36, which may be a short pass reflector or a long pass reflector.
- the layer of a phosphor material emits visible light when illuminated by light emitted by the LED and transmitted through the reflector.
- light emitting device 38 comprises a phosphor-reflector assembly 40, the phosphor reflector assembly comprising a layer of phosphor material 42 disposed between two reflectors 44 and 46.
- Examples include the VikuitiTM BEFII and BEFIII family of prismatic films available from 3 M Company, St. Paul, Minnesota, including BEFII 90/24, BEFII 90/50, BEFIIIM 90/50, and BEFIIIT. Brightness enhancement films can act as retro-reflecting films or elements for use therewith.
- the layer may be made by coating a flowable composition onto a microstructured tool or liner and then hardening the composition.
- the flowable composition may be radiation curable and comprise a reactive diluent, oligomer, crosslinker, and an optional photoinitiator which are hardened or cured by application of UV, electron beam, or some other kind of radiation after coating onto the microstructured tool or liner.
- the flowable composition may be a composition that is made flowable at an elevated temperature and then cooled after coating onto the microstructured tool or liner. Examples of useful radiation curable compositions are described below for a microstructured layer.
- This polymerizable composition comprises a first monomer comprising a major portion of 2-propenoic acid, (l-methylethylidene)bis[(2,6- dibromo-4,l-phenylene)oxy(2-hydroxy-3,l-propanediyl)] ester; pentaerythritol tri(meth)acrylate; and phenoxyethyl (meth)acrylate.
- the particular choice of materials used for the polymerizable composition will depend upon the method used to form the microstructured layer, for example, viscosity may be an important factor.
- the particular application in which the brightness enhancement film will be employed may also be considered, for example, the film needs to have particular optical properties yet be physically and chemically durable over time.
- the second optical layer in a brightness enhancement film may be described as a base layer. This layer may comprise any material suitable for use in an optical product, i.e., one that is optically clear and designed to control the flow of light. Depending on the particular application, the second optical layer may need to be structurally strong enough so that the brightness enhancement film may be assembled into an optical device.
- the optical element may also comprise optical elements including those described as extractors or optical concentrators, in U.S. Serial Nos. 10/977577, 10/977225, 10/977248, 10/977241, 11/027404, 11/381324, 11/381329, 11/381332, 11/381984 (Attorney docket nos. 60217, 60218, 60219, 60296, 62044, 62076, 62080, 62081, and 62082), and US 2005/0023545 Al, the disclosures of which are incorporated herein by reference for all that they contain. These optical elements can be used to aid extraction of light from the LED to the surrounding medium as well as to modify the emission pattern of the light. These optical elements typically have a refractive index of about 1.75 or greater and comprise glass, diamond, silicone carbide, sapphire, zirconia, zinc oxide, polymer, or a combination thereof.
- FIG. 4 shows examples of how an exemplary optical element, ball lens 42, may be attached to LED 44 with photopolymerized composition 46.
- the ball lens and LED are in contact with each other such that attaching the optical element to the light emitting diode comprises contacting the optical element and light emitting diode.
- FIG. 4b they are physically close together and spaced apart from each other such that attaching the optical element to the light emitting diode comprises positioning the optical element within 100 nm of the light emitting diode. In both cases, the two are held together by the photopolymerized composition 46.
- the optical element In most cases, it is desirable for the optical element to be optically coupled to the LED, which is typically the case when the two are physically close together, for example, when they within 100 nm of each other.
- the optical element 54 and LED 56 are attached by a small amount of the photopolymerized composition 58.
- the optical element is an extractor 59, and the extractor is attached to LED 56 with photopolymerized composition 58.
- the photopolymerizable composition may be an encapsulant such that attaching the optical element to the light emitting diode comprises encapsulating the light emitting diode.
- light emitting device 48 comprises LED 50 encapsulated with photopolymerized composition 52, and embedded in the photopolymerized composition is phosphor-reflector assembly 40.
- the light emitting device shown in FIG. 3c may be referred to as a phosphor based light source, or PLED, and is described, for example, in US 2004/0145913 Al, US 2004/0145288, and US 2004/0144987, the disclosures of which are incorporated herein by reference.
- the photopolymerizable composition may also be used to encapsulant an array of LEDs surface mounted on a variety of substrates.
- the light emitting device described herein comprises an LED that emits light, whether visible, ultraviolet, or infrared. It includes encapsulated semiconductor devices marketed as "LEDs", whether of the conventional or super-radiant variety. Vertical cavity surface emitting laser diodes are another form of LED.
- An "LED die” is an LED in its most basic form, i.e., in the form of an individual component or chip made by semiconductor wafer processing procedures. The component or chip can include electrical contacts suitable for application of power to energize the device. The individual layers and other functional elements of the component or chip are typically formed on the wafer scale, the finished wafer finally being diced into individual piece parts to yield a multiplicity of LED dies.
- Useful LEDs include monochrome and phosphor-LEDs (in which blue or UV light is converted to another color via a fluorescent phosphor).
- the LEDs may be surface mounted or side mounted, in ceramic or polymeric packages either of which may or may not have a reflecting cup, or they may be mounted on circuit boards, or on plastic electronic substrates.
- LED emission light can be any light that an LED source can emit and can range from the UV to the infrared portions of the electromagnetic spectrum depending on the composition and structure of the semiconductor layers. Where the source of the actinic radiation is the LED itself, LED emission is preferably in the range from 350-500 nm.
- the photopolymerized composition described herein is resistant to thermal and photodegradation (resistant to yellowing) and thus are particularly useful for white light sources (i.e., white light emitting devices).
- White light sources that utilize LEDs in their construction can have two basic configurations. In one, referred to herein as direct emissive LEDs, white light is generated by direct emission of different colored LEDs.
- Examples include a combination of a red LED, a green LED, and a blue LED, and a combination of a blue LED and a yellow LED.
- LED-excited phosphor-based light sources PLEDs
- a single LED generates light in a narrow range of wavelengths, which impinges upon and excites a phosphor material to produce visible light.
- the phosphor can comprise a mixture or combination of distinct phosphor materials, and the light emitted by the phosphor can include a plurality of narrow emission lines distributed over the visible wavelength range such that the emitted light appears substantially white to the unaided human eye.
- An example of a PLED is a blue LED illuminating a phosphor that converts blue to both red and green wavelengths. A portion of the blue excitation light is not absorbed by the phosphor, and the residual blue excitation light is combined with the red and green light emitted by the phosphor.
- Another example of a PLED is an ultraviolet (UV) LED illuminating a phosphor that absorbs and converts UV light to red, green, and blue light. It will be apparent to one skilled in the art that competitive absorption of the actinic radiation by the phosphor will decrease absorption by the photoinitiators slowing or even preventing cure if the system is not carefully constructed.
- the LED package used in the examples comprised a polyphthalamide body injection molded onto an aluminum lead frame.
- the package had a 9x9 mm square base that was ⁇ 2mm thick and an additional 1.5 mm thick cylindrical section on top that was ⁇ 8 mm in diameter.
- the package had an internal well that was ⁇ 6 mm in diameter at the top of the well and ⁇ 4 mm at the bottom of the well.
- the sidewall of the well was sloped at approximately a 70-degree angle and there was a small shelf in the sidewall between the top and bottom section of the well.
- the aluminum leads in the package were exposed at the bottom of the well, one large aluminum bond pad covering more than half of the base of the well and two smaller aluminum bond pads.
- the packages were not populated with LEDs.
- the package described above was filled with the photopolymerizable composition described above to be flush with the top of the well.
- the polyphthalamide package with photopolymerizable composition was irradiated for 140 seconds under a UVP Blak-Ray Lamp Model XX- 15 fitted with two 16 inch Sylvania F15T8/350BL bulbs emitting primarily at 350nm. After irradiation, the photopolymerizable composition, or encapsulant, had gelled and was very sticky. Onto the surface of the LED package and encapsulant was placed a small ⁇ 9x9mm square piece of a brightness enhancing film BEFII (available from 3 M Company) with the linear prisms facing outward.
- BEFII brightness enhancing film
- the film appeared fully wetted with the encapsulant and was placed into a 120 0 C oven for 10 minutes to finish curing the silicone encapsulant. After removing the package from the oven, it was visually inspected and the film was optically coupled to the encapsulant surface. The film was probed with a tweezer and was adhered to the surface of the encapsulant.
- the film appeared fully wetted with the encapsulant and was placed into a 120 0 C oven for 10 minutes to finish curing the silicone encapsulant. After removing the package from the oven, it was visually inspected and the film was optically coupled to the encapsulant surface. The film was probed with a tweezer and was firmly attached to the surface of the encapsulant.
- the package described above was filled with the photopolymerizable composition described above to be flush with the top of the well.
- the polyphthalamide package with photopolymerizable composition was irradiated for 140 seconds under a UVP Blak-Ray
- Lamp Model XX- 15 fitted with two 16 inch Sylvania F15T8/350BL bulbs emitting primarily at 350nm. After irradiation the encapsulant had gelled and was very sticky.
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Abstract
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
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EP07761165A EP2030256A1 (fr) | 2006-05-17 | 2007-04-24 | Procédé de fabrication d'un dispositif électroluminescent à l'aide d'une composition contenant du silicium |
JP2009511138A JP2009537991A (ja) | 2006-05-17 | 2007-04-24 | ケイ素含有組成物を有する発光デバイスの製造方法 |
CN2007800177531A CN101443926B (zh) | 2006-05-17 | 2007-04-24 | 利用含硅组合物制备发光器件的方法 |
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US11/383,916 | 2006-05-17 | ||
US11/383,916 US20070269586A1 (en) | 2006-05-17 | 2006-05-17 | Method of making light emitting device with silicon-containing composition |
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WO2007136956A1 true WO2007136956A1 (fr) | 2007-11-29 |
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PCT/US2007/067266 WO2007136956A1 (fr) | 2006-05-17 | 2007-04-24 | Procédé de fabrication d'un dispositif électroluminescent à l'aide d'une composition contenant du silicium |
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US (1) | US20070269586A1 (fr) |
EP (1) | EP2030256A1 (fr) |
JP (1) | JP2009537991A (fr) |
KR (1) | KR20090008338A (fr) |
CN (1) | CN101443926B (fr) |
TW (1) | TW200802991A (fr) |
WO (1) | WO2007136956A1 (fr) |
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Also Published As
Publication number | Publication date |
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CN101443926A (zh) | 2009-05-27 |
US20070269586A1 (en) | 2007-11-22 |
KR20090008338A (ko) | 2009-01-21 |
TW200802991A (en) | 2008-01-01 |
CN101443926B (zh) | 2012-05-30 |
EP2030256A1 (fr) | 2009-03-04 |
JP2009537991A (ja) | 2009-10-29 |
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