WO2005048381A1 - Multiphase nanocomposite material and method for its manufacture - Google Patents

Multiphase nanocomposite material and method for its manufacture Download PDF

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Publication number
WO2005048381A1
WO2005048381A1 PCT/US2004/001258 US2004001258W WO2005048381A1 WO 2005048381 A1 WO2005048381 A1 WO 2005048381A1 US 2004001258 W US2004001258 W US 2004001258W WO 2005048381 A1 WO2005048381 A1 WO 2005048381A1
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WO
WIPO (PCT)
Prior art keywords
phase
stabilizer
active
mechanical alloying
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2004/001258
Other languages
English (en)
French (fr)
Inventor
John Miller
Liya Wang
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TJ Technologies Inc
Original Assignee
TJ Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TJ Technologies Inc filed Critical TJ Technologies Inc
Priority to EP04703597A priority Critical patent/EP1597784A4/en
Priority to JP2006532257A priority patent/JP2007502525A/ja
Priority to CA002513587A priority patent/CA2513587A1/en
Publication of WO2005048381A1 publication Critical patent/WO2005048381A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/002—Making metallic powder or suspensions thereof amorphous or microcrystalline
    • B22F9/004—Making metallic powder or suspensions thereof amorphous or microcrystalline by diffusion, e.g. solid state reaction
    • B22F9/005—Transformation into amorphous state by milling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/07—Metallic powder characterised by particles having a nanoscale microstructure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/08—Metallic powder characterised by particles having an amorphous microstructure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/09—Mixtures of metallic powders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/12—Metallic powder containing non-metallic particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/02—Making metallic powder or suspensions thereof using physical processes
    • B22F9/04—Making metallic powder or suspensions thereof using physical processes starting from solid material, e.g. by crushing, grinding or milling
    • B22F2009/041—Making metallic powder or suspensions thereof using physical processes starting from solid material, e.g. by crushing, grinding or milling by mechanical alloying, e.g. blending, milling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/12—All metal or with adjacent metals
    • Y10T428/12014—All metal or with adjacent metals having metal particles
    • Y10T428/12021—All metal or with adjacent metals having metal particles having composition or density gradient or differential porosity

Definitions

  • the recovered material was sieved to less than 106 microns, and the typical yield for the foregoing process is generally in the range of 7-9 grams.
  • the resulting product is characterized as a poorly crystallized multiphase material showing x-ray diffraction peaks consistent with the presence of FeSn 2 and V 8 C 7 fractions as shown in Figure 1 which comprises the x-ray diffraction pattern of the Sn 4 Zr 2 Fe (VC) 5 material produced in 10 gram batches as described in Example 1.
  • the notation used to identify the materials in Figure 1 does not refer to a compound, but rather to the molar content of each component of the compound.
  • the foregoing procedure was also repeated for 2 gram batches with similar results.
  • Electrodes of the nanostructured material of the present invention were prepared by mixing the composite electrode powders with conductive carbon (approximately 5-8% by weight of carbon sold under the designation Super P), thereafter 5-12 weight percent of a PVDF binder (polyvinylidene difluoride, Aldrich) was added in a solution of n-methyl pyrrolidinone (Aldrich). The mixture of material, carbon and binder was stirred into a paste consistency and cast onto clean copper foil using the doctor blade draw down method. This electrode material was then cut into individual anodes which were then incorporated into lithium ion batteries.
  • conductive carbon approximately 5-8% by weight of carbon sold under the designation Super P
  • PVDF binder polyvinylidene difluoride, Aldrich
  • Aldrich n-methyl pyrrolidinone

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
PCT/US2004/001258 2003-01-17 2004-01-20 Multiphase nanocomposite material and method for its manufacture Ceased WO2005048381A1 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
EP04703597A EP1597784A4 (en) 2003-01-17 2004-01-20 POLYPHASE NANOCOMPOSITE MATERIAL AND METHOD OF MANUFACTURING THE SAME
JP2006532257A JP2007502525A (ja) 2003-01-17 2004-01-20 多相ナノ複合材料及びその製造方法
CA002513587A CA2513587A1 (en) 2003-01-17 2004-01-20 Multiphase nanocomposite material and method for its manufacture

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US44067503P 2003-01-17 2003-01-17
US60/440,675 2003-01-17
US10/759,348 US7169328B2 (en) 2003-01-17 2004-01-16 Multiphase nanocomposite material and method for its manufacture
US10/759,348 2004-01-16

Publications (1)

Publication Number Publication Date
WO2005048381A1 true WO2005048381A1 (en) 2005-05-26

Family

ID=32738333

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2004/001258 Ceased WO2005048381A1 (en) 2003-01-17 2004-01-20 Multiphase nanocomposite material and method for its manufacture

Country Status (5)

Country Link
US (1) US7169328B2 (enExample)
EP (1) EP1597784A4 (enExample)
JP (1) JP2007502525A (enExample)
CA (1) CA2513587A1 (enExample)
WO (1) WO2005048381A1 (enExample)

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EP1928046A1 (en) 2006-11-27 2008-06-04 Samsung SDI Co., Ltd. Negative active material and rechargeable lithium battery including the same
US8039152B2 (en) 2007-04-03 2011-10-18 Toyota Motor Engineering & Manufacturing North America, Inc. Tin in an active support matrix
US8835053B2 (en) 2007-03-21 2014-09-16 Samsung Sdi Co., Ltd. Negative active material containing an intermetallic compound of silicon and a first metal and a metal matrix containing copper and aluminum for rechargeable lithium battery and rechargeable lithium battery containing the negative active material
US8835051B2 (en) 2007-04-05 2014-09-16 Samsung Sdi Co., Ltd. Negative active material for rechargeable lithium battery, method for preparing same, and rechargeable lithium battery including same

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US7498100B2 (en) * 2003-08-08 2009-03-03 3M Innovative Properties Company Multi-phase, silicon-containing electrode for a lithium-ion battery
WO2005065281A2 (en) * 2003-12-31 2005-07-21 The Regents Of The University Of California Articles comprising high-electrical-conductivity nanocomposite material and method for fabricating same
US7851085B2 (en) * 2005-07-25 2010-12-14 3M Innovative Properties Company Alloy compositions for lithium ion batteries
US7871727B2 (en) * 2005-07-25 2011-01-18 3M Innovative Properties Company Alloy composition for lithium ion batteries
US7767349B2 (en) * 2005-07-25 2010-08-03 3M Innovative Properties Company Alloy compositions for lithium ion batteries
JP5155172B2 (ja) * 2005-10-13 2013-02-27 スリーエム イノベイティブ プロパティズ カンパニー 電気化学セルの使用方法
KR101354336B1 (ko) * 2005-12-01 2014-01-22 쓰리엠 이노베이티브 프로퍼티즈 컴파니 규소 함량이 높은 비결정성 합금을 기재로 하는 전극조성물
US7906238B2 (en) 2005-12-23 2011-03-15 3M Innovative Properties Company Silicon-containing alloys useful as electrodes for lithium-ion batteries
CN100373667C (zh) * 2006-05-17 2008-03-05 浙江大学 锂离子电池的负极材料及其制备方法
EP2125361B1 (en) * 2006-12-28 2019-01-23 3M Innovative Properties Company Nucleation layer for thin film metal layer formation
US8642216B2 (en) * 2007-01-25 2014-02-04 Samsung Sdi Co., Ltd. Composite anode active material, with intermetallic compound, method of preparing the same, and anode and lithium battery containing the material
CN101675546A (zh) * 2007-02-27 2010-03-17 3M创新有限公司 电解质、电极组合物以及由此制成的电化学电池
US20080206631A1 (en) * 2007-02-27 2008-08-28 3M Innovative Properties Company Electrolytes, electrode compositions and electrochemical cells made therefrom
US20090053589A1 (en) * 2007-08-22 2009-02-26 3M Innovative Properties Company Electrolytes, electrode compositions, and electrochemical cells made therefrom
US20080206641A1 (en) * 2007-02-27 2008-08-28 3M Innovative Properties Company Electrode compositions and electrodes made therefrom
US8630040B2 (en) * 2007-10-30 2014-01-14 3M Innovative Properties Company Multi-component films for optical display filters
KR101463112B1 (ko) * 2007-12-18 2014-11-21 삼성에스디아이 주식회사 복합체 음극 활물질, 그 제조 방법 및 이를 채용한 음극과리튬 전지
US8277974B2 (en) 2008-04-25 2012-10-02 Envia Systems, Inc. High energy lithium ion batteries with particular negative electrode compositions
US8350451B2 (en) * 2008-06-05 2013-01-08 3M Innovative Properties Company Ultrathin transparent EMI shielding film comprising a polymer basecoat and crosslinked polymer transparent dielectric layer
US9012073B2 (en) * 2008-11-11 2015-04-21 Envia Systems, Inc. Composite compositions, negative electrodes with composite compositions and corresponding batteries
US8057710B2 (en) * 2009-03-30 2011-11-15 Lg Chem, Ltd. Composite for electrode active material and secondary battery comprising the same
US8287772B2 (en) 2009-05-14 2012-10-16 3M Innovative Properties Company Low energy milling method, low crystallinity alloy, and negative electrode composition
US8257864B2 (en) * 2009-06-29 2012-09-04 3M Innovative Properties Company Method of making tin-based alloys for negative electrode compositions
EP2497144A4 (en) 2009-11-03 2014-04-23 Envia Systems Inc HIGH-CAPACITY ANODE MATERIALS FOR LITHIUM ION BATTERIES
EP2531629A1 (en) * 2010-02-04 2012-12-12 Third Millennium Metals, Llc Metal-carbon compositions
US9601228B2 (en) 2011-05-16 2017-03-21 Envia Systems, Inc. Silicon oxide based high capacity anode materials for lithium ion batteries
US9139441B2 (en) 2012-01-19 2015-09-22 Envia Systems, Inc. Porous silicon based anode material formed using metal reduction
US10553871B2 (en) 2012-05-04 2020-02-04 Zenlabs Energy, Inc. Battery cell engineering and design to reach high energy
US9780358B2 (en) 2012-05-04 2017-10-03 Zenlabs Energy, Inc. Battery designs with high capacity anode materials and cathode materials
JP2016502241A (ja) * 2012-11-21 2016-01-21 スリーエム イノベイティブ プロパティズ カンパニー ナトリウムイオン電池用のアノード組成物及びそれを製作する方法
US10020491B2 (en) 2013-04-16 2018-07-10 Zenlabs Energy, Inc. Silicon-based active materials for lithium ion batteries and synthesis with solution processing
US10886526B2 (en) 2013-06-13 2021-01-05 Zenlabs Energy, Inc. Silicon-silicon oxide-carbon composites for lithium battery electrodes and methods for forming the composites
US11476494B2 (en) 2013-08-16 2022-10-18 Zenlabs Energy, Inc. Lithium ion batteries with high capacity anode active material and good cycling for consumer electronics
CN107127340A (zh) * 2017-04-10 2017-09-05 西安铂力特激光成形技术有限公司 一种金属陶瓷零件的快速成形方法
US11094925B2 (en) 2017-12-22 2021-08-17 Zenlabs Energy, Inc. Electrodes with silicon oxide active materials for lithium ion cells achieving high capacity, high energy density and long cycle life performance
JP7375569B2 (ja) * 2019-02-06 2023-11-08 大同特殊鋼株式会社 リチウムイオン電池用負極活物質

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Cited By (5)

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Publication number Priority date Publication date Assignee Title
EP1928046A1 (en) 2006-11-27 2008-06-04 Samsung SDI Co., Ltd. Negative active material and rechargeable lithium battery including the same
US8574764B2 (en) 2006-11-27 2013-11-05 Samsung Sdi Co., Ltd. Negative active material including silicon active particles surrounded by copper, aluminum and tin metal matrix and rechargeable lithium battery including the same
US8835053B2 (en) 2007-03-21 2014-09-16 Samsung Sdi Co., Ltd. Negative active material containing an intermetallic compound of silicon and a first metal and a metal matrix containing copper and aluminum for rechargeable lithium battery and rechargeable lithium battery containing the negative active material
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US8835051B2 (en) 2007-04-05 2014-09-16 Samsung Sdi Co., Ltd. Negative active material for rechargeable lithium battery, method for preparing same, and rechargeable lithium battery including same

Also Published As

Publication number Publication date
US7169328B2 (en) 2007-01-30
JP2007502525A (ja) 2007-02-08
US20040146734A1 (en) 2004-07-29
CA2513587A1 (en) 2005-05-26
EP1597784A1 (en) 2005-11-23
EP1597784A4 (en) 2010-02-17

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