WO2005017057A1 - Solventless, non-polluting radiation and thermally curable coatings - Google Patents
Solventless, non-polluting radiation and thermally curable coatings Download PDFInfo
- Publication number
- WO2005017057A1 WO2005017057A1 PCT/US2004/025176 US2004025176W WO2005017057A1 WO 2005017057 A1 WO2005017057 A1 WO 2005017057A1 US 2004025176 W US2004025176 W US 2004025176W WO 2005017057 A1 WO2005017057 A1 WO 2005017057A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- weight
- parts
- catalyst solution
- iodonium
- salt
- Prior art date
Links
- 0 *C(COc1ccc(C(c2ccccc2)O)cc1)O Chemical compound *C(COc1ccc(C(c2ccccc2)O)cc1)O 0.000 description 2
- YXALYBMHAYZKAP-UHFFFAOYSA-N O=C(C1CC2OC2CC1)OCC1CC2OC2CC1 Chemical compound O=C(C1CC2OC2CC1)OCC1CC2OC2CC1 YXALYBMHAYZKAP-UHFFFAOYSA-N 0.000 description 2
- OJYIBEYSBXIQOP-UHFFFAOYSA-N CC(C)(c(cc1)ccc1OC)c(cc1)ccc1OC Chemical compound CC(C)(c(cc1)ccc1OC)c(cc1)ccc1OC OJYIBEYSBXIQOP-UHFFFAOYSA-N 0.000 description 1
- ZWXMSIUPDZKMAZ-UHFFFAOYSA-N CCC(COc1ccc(CCc2ccc(C)cc2)cc1)O Chemical compound CCC(COc1ccc(CCc2ccc(C)cc2)cc1)O ZWXMSIUPDZKMAZ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/22—Di-epoxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/22—Di-epoxy compounds
- C08G59/30—Di-epoxy compounds containing atoms other than carbon, hydrogen, oxygen and nitrogen
- C08G59/306—Di-epoxy compounds containing atoms other than carbon, hydrogen, oxygen and nitrogen containing silicon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/32—Epoxy compounds containing three or more epoxy groups
- C08G59/3254—Epoxy compounds containing three or more epoxy groups containing atoms other than carbon, hydrogen, oxygen or nitrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/32—Epoxy compounds containing three or more epoxy groups
- C08G59/38—Epoxy compounds containing three or more epoxy groups together with di-epoxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/68—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the catalysts used
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
- C09D183/06—Polysiloxanes containing silicon bound to oxygen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0025—Crosslinking or vulcanising agents; including accelerators
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31511—Of epoxy ether
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31511—Of epoxy ether
- Y10T428/31525—Next to glass or quartz
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31511—Of epoxy ether
- Y10T428/31529—Next to metal
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
- Y10T428/31609—Particulate metal or metal compound-containing
- Y10T428/31612—As silicone, silane or siloxane
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31652—Of asbestos
- Y10T428/31663—As siloxane, silicone or silane
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AU2004264507A AU2004264507A1 (en) | 2003-08-07 | 2004-08-05 | Solventless, non-polluting radiation and thermally curable coatings |
EP20040780077 EP1651731B1 (en) | 2003-08-07 | 2004-08-05 | Solventless, non-polluting radiation or thermally curable coatings |
DE200460003395 DE602004003395T2 (de) | 2003-08-07 | 2004-08-05 | Lösungsmittelfreie, voc-freie strahlungs- oder wärmehärtbare beschichtungsstoffe |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/636,101 US6962948B2 (en) | 2003-08-07 | 2003-08-07 | Solventless, non-polluting radiation and thermal curable coatings |
US10/636,101 | 2003-08-07 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2005017057A1 true WO2005017057A1 (en) | 2005-02-24 |
Family
ID=34193557
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2004/025176 WO2005017057A1 (en) | 2003-08-07 | 2004-08-05 | Solventless, non-polluting radiation and thermally curable coatings |
Country Status (6)
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2017222816A1 (en) * | 2016-06-24 | 2017-12-28 | Dow Global Technologies Llc | Curable resin composition |
TWI707008B (zh) * | 2017-12-19 | 2020-10-11 | 美商羅門哈斯電子材料有限公司 | 可固化組合物及用於在可撓性基板上形成可固化塗料的方法 |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005008691A (ja) * | 2003-06-17 | 2005-01-13 | Konica Minolta Medical & Graphic Inc | 活性エネルギー線硬化型インクジェットインク及び印刷物 |
US6962948B2 (en) * | 2003-08-07 | 2005-11-08 | Polyset Company, Inc. | Solventless, non-polluting radiation and thermal curable coatings |
JP2006124636A (ja) * | 2004-06-28 | 2006-05-18 | Konica Minolta Medical & Graphic Inc | 活性光線硬化型組成物、活性光線硬化型インクジェットインク、該活性光線硬化型インクジェットインクを用いた画像形成方法及びインクジェット記録装置 |
US7288607B2 (en) * | 2004-10-12 | 2007-10-30 | E. I. Du Pont De Nemours & Co. | High solids primer composition based on epoxy ring opening curing reaction |
JP4986423B2 (ja) * | 2005-08-03 | 2012-07-25 | 日東電工株式会社 | 剥離処理基材及びその製造方法 |
ES2527101T3 (es) * | 2005-08-12 | 2015-01-20 | Markem-Imaje Corporation | Formulaciones de tintas catiónicas |
US8048981B2 (en) * | 2005-09-20 | 2011-11-01 | General Electric Company | Thermally curable compositions and method |
FR2912605B1 (fr) * | 2007-02-16 | 2011-07-15 | Xeda International | Combinaisons d'esters de l'acide abietique avec un ou plusieurs terpenes et leur utilisation pour l'enrobage des fruits et legumes |
JP5325206B2 (ja) * | 2008-03-24 | 2013-10-23 | 昭和電工株式会社 | エポキシ化合物およびその製造方法 |
US20090294724A1 (en) * | 2008-05-27 | 2009-12-03 | Appealing Products, Inc. | Anti-icing material and surface treatments |
JP5793491B2 (ja) * | 2010-03-02 | 2015-10-14 | サンスター技研株式会社 | 硬化性組成物 |
US8629688B2 (en) * | 2010-09-29 | 2014-01-14 | International Business Machines Corporation | Method for sulfur-based corrosion testing |
TWI557183B (zh) * | 2015-12-16 | 2016-11-11 | 財團法人工業技術研究院 | 矽氧烷組成物、以及包含其之光電裝置 |
KR101339772B1 (ko) * | 2011-02-28 | 2014-02-05 | 한국과학기술원 | 광경화 투명 수지 조성물 |
EP2699623B1 (de) | 2011-04-18 | 2019-12-18 | Momentive Performance Materials GmbH | Funktionalisierte polyorganosiloxane oder silane zur behandlung von lignocellulosischen werkstoffen |
MY169938A (en) * | 2012-08-31 | 2019-06-18 | Daicel Corp | Curable composition, cured product thereof, optical member and optical device |
EP3112389B1 (en) * | 2014-02-28 | 2019-06-05 | Daicel Corporation | Curable composition, cured product thereof, and wafer level lens |
CN106687499B (zh) * | 2014-09-17 | 2019-07-19 | 株式会社大赛璐 | 固化性组合物、以及使用其的光学元件 |
CN107709400B (zh) * | 2015-06-17 | 2020-05-12 | 株式会社大赛璐 | 固化性组合物 |
TWI557177B (zh) | 2015-12-16 | 2016-11-11 | 財團法人工業技術研究院 | 低介電無溶劑型樹脂組成物及基板結構 |
MX2020001733A (es) | 2017-08-18 | 2020-03-20 | Fina Technology | Polifarnesenos epoxidizados y metodos para producirlos. |
CN114181581A (zh) * | 2021-12-27 | 2022-03-15 | 深圳市法鑫忠信新材料有限公司 | 一种高硬度的涂料组合物及其制备方法 |
CN117285706A (zh) * | 2022-06-24 | 2023-12-26 | 常州正洁智造科技有限公司 | 阳离子型光固化组合物、涂料、具有光固化涂层的制品、油墨 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5073643A (en) * | 1990-08-30 | 1991-12-17 | Polyset Corporation | High yield synthesis of hydroxyl-containing cationic photoinitiators |
WO1998033645A1 (en) * | 1997-02-04 | 1998-08-06 | Polyset Company, Inc. | Die adhesive or encapsulant of epoxy siloxane and polyepoxy resin |
US20020193619A1 (en) * | 2002-06-21 | 2002-12-19 | Polyset Company, Inc. | Diaryliodonium salt catalysts made from iodotoluene and a method for preparing them |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5260349A (en) * | 1991-01-04 | 1993-11-09 | Polyset Corporation | Electron beam curable epoxy compositions |
DE69425473T3 (de) * | 1993-11-05 | 2005-11-03 | Shin-Etsu Chemical Co., Ltd. | Verfahren zur Herstellung von Organo-funktionelle Gruppen enthaltenden Organopolysiloxanen und daraus hergestellte Organopolysiloxane, Mercapto- und Alkoxygruppen enthaltende Organopolysiloxane und Verfahren zu deren Herstellung |
US5757313A (en) * | 1993-11-09 | 1998-05-26 | Markem Corporation | Lacer-induced transfer printing medium and method |
US6069259A (en) * | 1998-02-06 | 2000-05-30 | Rensselaer Polytechnic Institute | Multifunctional polymerizible alkoxy siloxane oligomers |
US6602602B1 (en) * | 1999-04-26 | 2003-08-05 | Renssealer Polytechnic Institute | Epoxy-functional polymeric microbeads |
US6832036B2 (en) * | 2002-10-11 | 2004-12-14 | Polyset Company, Inc. | Siloxane optical waveguides |
US6962948B2 (en) * | 2003-08-07 | 2005-11-08 | Polyset Company, Inc. | Solventless, non-polluting radiation and thermal curable coatings |
US7019386B2 (en) * | 2004-04-27 | 2006-03-28 | Polyset Company, Inc. | Siloxane epoxy polymers for low-k dielectric applications |
-
2003
- 2003-08-07 US US10/636,101 patent/US6962948B2/en not_active Expired - Lifetime
-
2004
- 2004-08-05 AU AU2004264507A patent/AU2004264507A1/en not_active Abandoned
- 2004-08-05 DE DE200460003395 patent/DE602004003395T2/de not_active Expired - Fee Related
- 2004-08-05 AT AT04780077T patent/ATE346124T1/de not_active IP Right Cessation
- 2004-08-05 WO PCT/US2004/025176 patent/WO2005017057A1/en active IP Right Grant
- 2004-08-05 EP EP20040780077 patent/EP1651731B1/en active Active
-
2005
- 2005-03-15 US US11/079,971 patent/US7285579B2/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5073643A (en) * | 1990-08-30 | 1991-12-17 | Polyset Corporation | High yield synthesis of hydroxyl-containing cationic photoinitiators |
WO1998033645A1 (en) * | 1997-02-04 | 1998-08-06 | Polyset Company, Inc. | Die adhesive or encapsulant of epoxy siloxane and polyepoxy resin |
US20020193619A1 (en) * | 2002-06-21 | 2002-12-19 | Polyset Company, Inc. | Diaryliodonium salt catalysts made from iodotoluene and a method for preparing them |
Non-Patent Citations (1)
Title |
---|
CRIVELLO J V ET AL: "THE UV CURE OF EPOXY-SILICONE MONOMERS", POLYMERIC MATERIALS SCIENCE AND ENGINEERING, WASHINGTON, DC, US, vol. 60, 1989, pages 217 - 227, XP009035836, ISSN: 0743-0515 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2017222816A1 (en) * | 2016-06-24 | 2017-12-28 | Dow Global Technologies Llc | Curable resin composition |
TWI677477B (zh) * | 2016-06-24 | 2019-11-21 | 美商羅門哈斯電子材料有限公司 | 可固化樹脂組合物 |
KR102057469B1 (ko) * | 2016-06-24 | 2019-12-19 | 다우 글로벌 테크놀로지스 엘엘씨 | 경화성 수지 조성물 |
TWI707008B (zh) * | 2017-12-19 | 2020-10-11 | 美商羅門哈斯電子材料有限公司 | 可固化組合物及用於在可撓性基板上形成可固化塗料的方法 |
Also Published As
Publication number | Publication date |
---|---|
US7285579B2 (en) | 2007-10-23 |
US6962948B2 (en) | 2005-11-08 |
EP1651731A1 (en) | 2006-05-03 |
AU2004264507A1 (en) | 2005-02-24 |
DE602004003395D1 (de) | 2007-01-04 |
DE602004003395T2 (de) | 2007-09-13 |
EP1651731B1 (en) | 2006-11-22 |
ATE346124T1 (de) | 2006-12-15 |
US20050042458A1 (en) | 2005-02-24 |
US20050170187A1 (en) | 2005-08-04 |
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