WO2004056700A1 - Procede de production de fluor - Google Patents
Procede de production de fluor Download PDFInfo
- Publication number
- WO2004056700A1 WO2004056700A1 PCT/RU2003/000359 RU0300359W WO2004056700A1 WO 2004056700 A1 WO2004056700 A1 WO 2004056700A1 RU 0300359 W RU0300359 W RU 0300359W WO 2004056700 A1 WO2004056700 A1 WO 2004056700A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- fluorine
- production
- pressure
- compounds
- salts
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/006—Processes utilising sub-atmospheric pressure; Apparatus therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0242—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical
- B01J8/025—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical in a cylindrical shaped bed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0242—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical
- B01J8/0257—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical in a cylindrical annular shaped bed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0278—Feeding reactive fluids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0285—Heating or cooling the reactor
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/20—Fluorine
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00203—Coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00389—Controlling the temperature using electric heating or cooling elements
- B01J2208/00407—Controlling the temperature using electric heating or cooling elements outside the reactor bed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00389—Controlling the temperature using electric heating or cooling elements
- B01J2208/00415—Controlling the temperature using electric heating or cooling elements electric resistance heaters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/0053—Controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00654—Controlling the process by measures relating to the particulate material
- B01J2208/00672—Particle size selection
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
- B01J2219/0236—Metal based
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0277—Metal based
Definitions
- the invention is not disclosed in the field of the receipt of the goods, but in the name - in the case of the loss of the signal from the use of metals or in the event of accident.
- Gaz ⁇ b ⁇ azny ⁇ is ⁇ lzue ⁇ sya v ⁇ mn ⁇ gi ⁇ ⁇ blas ⁇ ya ⁇ , ⁇ a ⁇ i ⁇ ⁇ a ⁇ ⁇ luchenie ⁇ s ⁇ edineny ⁇ yamym ⁇ i ⁇ vaniem, ⁇ i sva ⁇ e me ⁇ all ⁇ v for ⁇ b ⁇ az ⁇ vaniya zaschi ⁇ ny ⁇ ⁇ len ⁇ on me ⁇ alla ⁇ or ⁇ i ⁇ b ⁇ ab ⁇ e ⁇ ve ⁇ n ⁇ s ⁇ ey me ⁇ all ⁇ v and s ⁇ lav ⁇ v and ⁇ . ⁇ ., and in ⁇ a ⁇ zhe ⁇ aches ⁇ ve ⁇ aviln ⁇ g ⁇ ⁇ eagen ⁇ a in mi ⁇ ele ⁇ ni ⁇ e.
- Conventional fluids and other fluorine-containing gas compounds such as 3 or fluorine, are gas-tight in cylinders under high pressure or in the form of low-pressure liquids.
- This acid is a solid material in the presence of a heat-transfer medium that is melted or sublimated in the same manner as an elevated temperature.
- the aforementioned stable salt is anionic, comes from a thermally unstable phase in which there is a large amount of white matter.
- ⁇ s ⁇ s ⁇ be is ⁇ lzuyu ⁇ sya ⁇ idy schel ⁇ chny ⁇ me ⁇ all ⁇ v, na ⁇ ime ⁇ , ni ⁇ elya, ads ⁇ bi ⁇ uyuschie ⁇ with ⁇ b ⁇ az ⁇ vaniem ⁇ m ⁇ le ⁇ sny ⁇ s ⁇ ley ni ⁇ elya and schel ⁇ chny ⁇ me ⁇ all ⁇ v - Cs 2 ⁇ b, ⁇ ⁇ 2 b; and in the quality of the connection ⁇ use ⁇ 5 , ⁇ 5 , ⁇ 4 and ⁇ . ⁇ . 3
- the closest solution is the method of receiving and storing a separate signal [Patent of the USA 3989808, and the USA 423/503;
- alkali metal and nickel phosphoids are used, which adsorb the pho- tope with the formation of complex nickel salts. After filling the capacity of the generator with gaseous substances, it discharges it. Then, the nickel phosphide compound is heated, and a high degree of gaseous effluent is released. However, it doesn’t allow you to receive fluids with a constant gas emission rate.
- the task which was to cut off the gas production, was to create a method for producing a gas inlet with a large extraction of high-pressure gas and gas
- the method should be simple, safe to operate.
- the degree of extraction must be at least 99%.
- ⁇ ⁇ aches ⁇ ve is ⁇ dny ⁇ s ⁇ edineny is ⁇ lzuyu ⁇ , na ⁇ ime ⁇ , s ⁇ li ma ⁇ gantsa with vys ⁇ y s ⁇ e ⁇ enyu s ⁇ de ⁇ zhaniya ⁇ a - ⁇ aliya ge ⁇ sa ⁇ ni ⁇ ela ⁇ ⁇ 2 ⁇ b, ⁇ e ⁇ a ⁇ id ma ⁇ gantsa ⁇ 4 and d ⁇ ugie s ⁇ li - na ⁇ ime ⁇ , ⁇ 3 ⁇ 7, ⁇ 2 Si ⁇ b and anal ⁇ gichnye s ⁇ edineniya them.
- Non-hazardous components and parts that are in contact with gaseous media are made from mate- rial that is subject to personal injury,
- the terms and conditions of the method are shown in the accompanying statements.
- the appliance is equipped with an electric heater 2 (external and internal), devices for measuring the temperature ( ⁇ and ⁇ 2) and pressure ( ⁇ ); ⁇ is deduced on the case indicated on the circuit as 2 .
- Examples 3–7 are used in the same apparatus and in the same manner, using the following connections in a separate source as a different dispersion. The results are presented in the table.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
- Ceramic Products (AREA)
Description
Claims
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
MXPA05006789A MXPA05006789A (es) | 2002-12-20 | 2003-08-08 | Metodo para la produccion de fluor. |
CA002511233A CA2511233A1 (en) | 2002-12-20 | 2003-08-08 | Fluorine production method |
EP03813731A EP1580163A1 (en) | 2002-12-20 | 2003-08-08 | Fluorine production method |
AU2003254983A AU2003254983A1 (en) | 2002-12-20 | 2003-08-08 | Fluorine production method |
US11/152,397 US20060099137A1 (en) | 2002-12-20 | 2005-06-13 | Fluorine production systems and methods |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
RU2002134329/15A RU2221739C1 (ru) | 2002-12-20 | 2002-12-20 | Способ получения фтора |
RU2002134329 | 2002-12-20 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US11/152,397 Continuation-In-Part US20060099137A1 (en) | 2002-12-20 | 2005-06-13 | Fluorine production systems and methods |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2004056700A1 true WO2004056700A1 (fr) | 2004-07-08 |
Family
ID=32091865
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/RU2003/000359 WO2004056700A1 (fr) | 2002-12-20 | 2003-08-08 | Procede de production de fluor |
Country Status (10)
Country | Link |
---|---|
US (1) | US20060099137A1 (ru) |
EP (1) | EP1580163A1 (ru) |
KR (1) | KR20050096098A (ru) |
CN (1) | CN1745033A (ru) |
AU (1) | AU2003254983A1 (ru) |
CA (1) | CA2511233A1 (ru) |
MX (1) | MXPA05006789A (ru) |
RU (1) | RU2221739C1 (ru) |
WO (1) | WO2004056700A1 (ru) |
ZA (1) | ZA200504995B (ru) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2006033474A1 (en) * | 2004-09-24 | 2006-03-30 | Showa Denko K.K. | Process for producing fluorine gas |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006049817A (ja) * | 2004-07-07 | 2006-02-16 | Showa Denko Kk | プラズマ処理方法およびプラズマエッチング方法 |
EP1807354B1 (en) * | 2004-09-10 | 2008-11-12 | Showa Denko Kabushiki Kaisha | Process for producing manganese fluoride |
JP2007176768A (ja) * | 2005-12-28 | 2007-07-12 | Showa Denko Kk | フッ素ガスの製造方法 |
JP2007176770A (ja) * | 2005-12-28 | 2007-07-12 | Showa Denko Kk | 高純度フッ素ガスの製造方法および高純度フッ素ガス製造装置 |
TW200934729A (en) * | 2007-12-11 | 2009-08-16 | Solvay Fluor Gmbh | Process for the purification of elemental fluorine |
TW200932340A (en) * | 2007-12-11 | 2009-08-01 | Solvay Fluor Gmbh | Method for recovery of fluorine |
TW200932681A (en) * | 2007-12-11 | 2009-08-01 | Solvay Fluor Gmbh | Method for preparing manganese tetrafluoride |
CN113336194B (zh) * | 2021-05-14 | 2022-07-05 | 浙江凯圣氟化学有限公司 | 一种络合剂分离无水氟化氢中金属离子的方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1904391A1 (de) * | 1968-02-01 | 1969-09-18 | Elektrokemisk As | Verfahren zur Rueckgewinnung von Fluor aus festen kohlenstoffhaltigen Abfallstoffen |
US3989808A (en) * | 1975-07-28 | 1976-11-02 | The United States Of America As Represented By The United States Energy Research And Development Administration | Method of preparing pure fluorine gas |
SU1432001A1 (ru) * | 1986-11-12 | 1988-10-23 | Московский химико-технологический институт им.Д.И.Менделеева | Способ получени чистого газообразного фтора |
-
2002
- 2002-12-20 RU RU2002134329/15A patent/RU2221739C1/ru not_active IP Right Cessation
-
2003
- 2003-08-08 CA CA002511233A patent/CA2511233A1/en not_active Abandoned
- 2003-08-08 AU AU2003254983A patent/AU2003254983A1/en not_active Abandoned
- 2003-08-08 CN CNA038256681A patent/CN1745033A/zh active Pending
- 2003-08-08 MX MXPA05006789A patent/MXPA05006789A/es not_active Application Discontinuation
- 2003-08-08 WO PCT/RU2003/000359 patent/WO2004056700A1/ru not_active Application Discontinuation
- 2003-08-08 KR KR1020057011581A patent/KR20050096098A/ko not_active Application Discontinuation
- 2003-08-08 EP EP03813731A patent/EP1580163A1/en not_active Withdrawn
-
2005
- 2005-06-13 US US11/152,397 patent/US20060099137A1/en not_active Abandoned
- 2005-06-20 ZA ZA200504995A patent/ZA200504995B/en unknown
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1904391A1 (de) * | 1968-02-01 | 1969-09-18 | Elektrokemisk As | Verfahren zur Rueckgewinnung von Fluor aus festen kohlenstoffhaltigen Abfallstoffen |
US3989808A (en) * | 1975-07-28 | 1976-11-02 | The United States Of America As Represented By The United States Energy Research And Development Administration | Method of preparing pure fluorine gas |
SU1432001A1 (ru) * | 1986-11-12 | 1988-10-23 | Московский химико-технологический институт им.Д.И.Менделеева | Способ получени чистого газообразного фтора |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2006033474A1 (en) * | 2004-09-24 | 2006-03-30 | Showa Denko K.K. | Process for producing fluorine gas |
US7572428B2 (en) | 2004-09-24 | 2009-08-11 | Showa Denko K.K. | Process for producing fluorine gas |
Also Published As
Publication number | Publication date |
---|---|
US20060099137A1 (en) | 2006-05-11 |
CA2511233A1 (en) | 2004-07-08 |
RU2221739C1 (ru) | 2004-01-20 |
MXPA05006789A (es) | 2006-03-09 |
AU2003254983A1 (en) | 2004-07-14 |
CN1745033A (zh) | 2006-03-08 |
ZA200504995B (en) | 2006-05-31 |
KR20050096098A (ko) | 2005-10-05 |
EP1580163A1 (en) | 2005-09-28 |
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