WO2003093207A3 - Verfahren zur herstellung ungesättigter halogenhaltiger kohlenwasserstoffe sowie dafür geeignete vorrichtung - Google Patents

Verfahren zur herstellung ungesättigter halogenhaltiger kohlenwasserstoffe sowie dafür geeignete vorrichtung Download PDF

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Publication number
WO2003093207A3
WO2003093207A3 PCT/EP2003/004519 EP0304519W WO03093207A3 WO 2003093207 A3 WO2003093207 A3 WO 2003093207A3 EP 0304519 W EP0304519 W EP 0304519W WO 03093207 A3 WO03093207 A3 WO 03093207A3
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WO
WIPO (PCT)
Prior art keywords
reactor
halogenic
hydrocarbons
device suitable
producing unsaturated
Prior art date
Application number
PCT/EP2003/004519
Other languages
English (en)
French (fr)
Other versions
WO2003093207A2 (de
Inventor
Michael Benje
Horst Ertl
Ingolf Mielke
Thomas Wild
Peter Kammerhofer
Peter Schwarzmaier
Original Assignee
Uhde Gmbh
Vinnolit Technologie Gmbh & Co
Michael Benje
Horst Ertl
Ingolf Mielke
Thomas Wild
Peter Kammerhofer
Peter Schwarzmaier
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Uhde Gmbh, Vinnolit Technologie Gmbh & Co, Michael Benje, Horst Ertl, Ingolf Mielke, Thomas Wild, Peter Kammerhofer, Peter Schwarzmaier filed Critical Uhde Gmbh
Priority to JP2004501348A priority Critical patent/JP4804750B2/ja
Priority to EP03732303A priority patent/EP1503975A2/de
Priority to US10/512,880 priority patent/US7309471B2/en
Priority to AU2003239827A priority patent/AU2003239827A1/en
Priority to CA002483981A priority patent/CA2483981A1/en
Publication of WO2003093207A2 publication Critical patent/WO2003093207A2/de
Publication of WO2003093207A3 publication Critical patent/WO2003093207A3/de
Priority to NO20045273A priority patent/NO20045273L/no
Priority to HK06100121A priority patent/HK1080068A1/xx

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/10—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using elemental hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J6/00—Heat treatments such as Calcining; Fusing ; Pyrolysis
    • B01J6/008—Pyrolysis reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0207—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal
    • B01J8/0214—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal in a cylindrical annular shaped bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0278—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00654—Controlling the process by measures relating to the particulate material
    • B01J2208/00707—Fouling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00119—Heat exchange inside a feeding nozzle or nozzle reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00132—Controlling the temperature using electric heating or cooling elements
    • B01J2219/00135—Electric resistance heaters
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00139—Controlling the temperature using electromagnetic heating
    • B01J2219/00141—Microwaves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00157—Controlling the temperature by means of a burner
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0803—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • B01J2219/0805—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy giving rise to electric discharges
    • B01J2219/0845—Details relating to the type of discharge
    • B01J2219/0849—Corona pulse discharge
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0873—Materials to be treated
    • B01J2219/0881—Two or more materials
    • B01J2219/0883—Gas-gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0873—Materials to be treated
    • B01J2219/0892—Materials to be treated involving catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0894—Processes carried out in the presence of a plasma
    • B01J2219/0896—Cold plasma
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Abstract

Beschrieben wird ein Verfahren zur Herstellung ethylenisch ungesättigter halogenhaltiger aliphatischer Kohlenwasserstoffe durch thermische. Spaltung von gesättigten halogenhaltigen aliphatischen Kohlenwasserstoffen. Dabei wird ein Eduktgasstrom in einen Reaktor eingeleitet, der mindestens eine in das Innere mündende Zuleitung aufweist, durch die ein aus Spaltpromotoren gebildetes und Radikale enthaltendes erhitztes Gas in den Reaktor eingespeist wird. Mit dem Verfahren ist eine Steigerung der Ausbeute der Spaltreaktion möglich.
PCT/EP2003/004519 2002-05-02 2003-04-30 Verfahren zur herstellung ungesättigter halogenhaltiger kohlenwasserstoffe sowie dafür geeignete vorrichtung WO2003093207A2 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
JP2004501348A JP4804750B2 (ja) 2002-05-02 2003-04-30 不飽和ハロゲン炭化水素を製造するための方法および該方法での使用に適するデバイス
EP03732303A EP1503975A2 (de) 2002-05-02 2003-04-30 Verfahren zur herstellung unges ttigter halogenhaltiger kohl enwasserstoffe sowie daf r geeignete vorrichtung
US10/512,880 US7309471B2 (en) 2002-05-02 2003-04-30 Method for producing unsaturated halogenic hydrocarbons and device suitable for use with said method
AU2003239827A AU2003239827A1 (en) 2002-05-02 2003-04-30 Method for producing unsaturated halogenic hydrocarbons and device suitable for use with said method
CA002483981A CA2483981A1 (en) 2002-05-02 2003-04-30 Method for producing unsaturated halogenic hydrocarbons and device suitable for use with said method
NO20045273A NO20045273L (no) 2002-05-02 2004-12-01 Fremgangsmate for fremstilling av umettet halogenholdige hydrokarboner samt dertil egnet anordning
HK06100121A HK1080068A1 (en) 2002-05-02 2006-01-04 Method for producing unsaturated halogenic hydrocarbons and device suitable for use with said method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10219723A DE10219723B4 (de) 2002-05-02 2002-05-02 Verfahren zur Herstellung ungesättigter halogenhaltiger Kohlenwasserstoffe sowie dafür geeignete Vorrichung
DE10219723.7 2002-05-02

Publications (2)

Publication Number Publication Date
WO2003093207A2 WO2003093207A2 (de) 2003-11-13
WO2003093207A3 true WO2003093207A3 (de) 2004-07-29

Family

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Family Applications (1)

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PCT/EP2003/004519 WO2003093207A2 (de) 2002-05-02 2003-04-30 Verfahren zur herstellung ungesättigter halogenhaltiger kohlenwasserstoffe sowie dafür geeignete vorrichtung

Country Status (12)

Country Link
US (1) US7309471B2 (de)
EP (1) EP1503975A2 (de)
JP (1) JP4804750B2 (de)
CN (1) CN100343208C (de)
AU (1) AU2003239827A1 (de)
CA (1) CA2483981A1 (de)
DE (1) DE10219723B4 (de)
HK (1) HK1080068A1 (de)
NO (1) NO20045273L (de)
RU (1) RU2316533C2 (de)
WO (1) WO2003093207A2 (de)
ZA (1) ZA200408235B (de)

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DE10219723B4 (de) 2002-05-02 2005-06-09 Uhde Gmbh Verfahren zur Herstellung ungesättigter halogenhaltiger Kohlenwasserstoffe sowie dafür geeignete Vorrichung
DE10319811A1 (de) * 2003-04-30 2004-11-18 Uhde Gmbh Vorrichtung zum Einkoppeln von elektromagnetischer Strahlung in einen Reaktor sowie Reaktor enthaltend diese Vorrichtung
DE10319810A1 (de) * 2003-04-30 2004-11-18 Uhde Gmbh Reaktor für radikalische Gasphasenreaktionen
US7253328B2 (en) * 2005-01-24 2007-08-07 John Stauffer Method for producing vinyl chloride monomer
TWI432456B (zh) * 2006-10-03 2014-04-01 Univation Tech Llc 用於觸媒注射之泡騰噴嘴
EP2142557B1 (de) * 2007-03-30 2012-09-05 Spawnt Private S.à.r.l. Plasmaunterstützte organofunktionalisierung von siliciumtetrahalogeniden oder von organohalogensilanen
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DE102008049261B4 (de) 2008-09-26 2018-03-22 Thyssenkrupp Industrial Solutions Ag Verfahren und Vorrichtung zur Herstellung von ethylenisch ungesättigten halogenierten Kohlenwasserstoffen
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DE102013016660A1 (de) * 2013-10-09 2015-04-09 Ralf Spitzl Verfahren und Vorrichtung zur plasmakatalytischen Umsetzung von Stoffen
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WO2002094743A2 (de) * 2001-05-19 2002-11-28 Siemens Axiva Gmbh & Co. Kg Verfahren und vorrichtung zur durchführung von radikalischen gasphasenreaktionen

Also Published As

Publication number Publication date
WO2003093207A2 (de) 2003-11-13
EP1503975A2 (de) 2005-02-09
US20050124835A1 (en) 2005-06-09
NO20045273L (no) 2005-01-21
RU2316533C2 (ru) 2008-02-10
AU2003239827A8 (en) 2003-11-17
JP4804750B2 (ja) 2011-11-02
CN1653022A (zh) 2005-08-10
HK1080068A1 (en) 2006-04-21
DE10219723A1 (de) 2003-11-20
RU2004135106A (ru) 2005-06-10
US7309471B2 (en) 2007-12-18
JP2006510573A (ja) 2006-03-30
AU2003239827A1 (en) 2003-11-17
DE10219723B4 (de) 2005-06-09
CN100343208C (zh) 2007-10-17
CA2483981A1 (en) 2003-11-13
ZA200408235B (en) 2005-07-01

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