WO1997011143A2 - Compositions detergentes tres puissantes comprenant des sels d'esters methyliques alpha sulfones d'acide gras et utilisation des sels d'acides gras alpha sulfones pour inhiber la redeposition des salissures sur le tissu - Google Patents
Compositions detergentes tres puissantes comprenant des sels d'esters methyliques alpha sulfones d'acide gras et utilisation des sels d'acides gras alpha sulfones pour inhiber la redeposition des salissures sur le tissu Download PDFInfo
- Publication number
- WO1997011143A2 WO1997011143A2 PCT/US1996/014889 US9614889W WO9711143A2 WO 1997011143 A2 WO1997011143 A2 WO 1997011143A2 US 9614889 W US9614889 W US 9614889W WO 9711143 A2 WO9711143 A2 WO 9711143A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- detergent
- alkyl
- weight
- fatty acid
- sulfonated
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
- C11D1/831—Mixtures of non-ionic with anionic compounds of sulfonates with ethers of polyoxyalkylenes without phosphates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/86—Mixtures of anionic, cationic, and non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0036—Soil deposition preventing compositions; Antiredeposition agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/146—Sulfuric acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
- C11D1/525—Carboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain two or more hydroxy groups per alkyl group, e.g. R3 being a reducing sugar rest
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Definitions
- R 3 (0R 4 ) X —N—(R5) 2
- R 3 is selected from an alkyl, hydroxyalkyl, acylamidopropyl and alkyl phenyl group, or mixtures thereof, containing from 8 to 26 carbon atoms, preferably 8 to 16 carbon atoms
- R 4 is an alkylene or hydroxyalkylene group containing from 2 to 3 carbon atoms, preferably 2 carbon atoms, or mixtures thereof
- x is from 0 to 3, preferably 0
- each R 5 is an alkyl or hydroxyalkyl group containing from 1 to 3, preferably from 1 to 2 carbon atoms, or a polyethylene oxide group containing from 1 to 3, preferably 1, ethylene oxide groups.
- the R 5 groups can be attached to each other, e.g., through an oxygen or nitrogen atom, to form a ring structure.
- the polymeric soil release agents for which performance is enhanced by polyhydroxy fatty acid amide in the presence of anionic surfactant include those soil release agents having: (a) one or more nonionic hydrophile components consisting essentially of (1) polyoxyethylene segments with a degree of polymerization of at least 2, or (ii) oxypropylene or polyoxypropylene segments with a degree of polymerization of from 2 to 10, wherein said hydrophile segment does not encompass any oxypropylene unit unless it is bonded to adjacent moieties at each end by ether linkages, or (iii) a mixture of oxyalkylene units comprising oxyethylene and from 1 to about 30 oxypropylene units wherein said mixture contains a sufficient amount of oxyethylene units such that the hydrophile component has hydrophilicity great enough to increase the hydrophilicity of conventional polyester synthetic fiber surfaces upon deposit of the soil release agent on such surface, said hydrophile segments preferably comprising at least about 25% oxyethylene units and more preferably, especially for such components having about 20 to 30
- the choice of brightener for use in detergent compositions will depend upon a number of factors, such as the type of detergent, the nature of other components present in the detergent composition, the temperatures of wash water, the degree of agitation, and the ratio of the material washed to tub size.
- these brighteners include 4-methyl-7-diethylamino coumarin; 1, 2-bis (-benzimidazol-2-yl) ethylene; 1,3- diphenylphrazolines; 2,5-bis(benzoxazol-2-yl)thiophene; 2-styryl- naphth-[l,2-d]oxazole; and 2-(stilbene-4-yl)2-H-naphtho-[l,2- d]triazole.
- a Laundry detergent formulations may be prepared by adding water to a suitable vessel equipped with mixing means. The remaining ingredients are added in the order in which they are listed in the formulations set forth in the following examples. The resulting mixtures are continuously mixed until a liquid of uniform consistency is obtained. The pH may be adjusted as needed to about 8.5-8.8 using suitable alkaline or acidic reagents.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA002205592A CA2205592C (fr) | 1995-09-18 | 1996-09-17 | Compositions detergentes tres puissantes comprenant des sels d'esters methyliques alpha sulfones d'acide gras et utilisation des sels d'acides gras alpha sulfones pour inhiber la redeposition des salissures sur le tissu |
EP96932244A EP0792336A2 (fr) | 1995-09-18 | 1996-09-17 | Compositions detergentes tres puissantes comprenant des sels d'esters methyliques alpha sulfones d'acide gras et utilisation des sels d'acides gras alpha sulfones pour inhiber la redeposition des salissures sur le tissu |
BR9606651A BR9606651A (pt) | 1995-09-18 | 1996-09-17 | Composição detergente e processo para inibir a redeposição de sujeira em tecido |
AU71112/96A AU699950B2 (en) | 1995-09-18 | 1996-09-17 | Heavy duty liquid detergent compositions comprising salts of alpha sulfonated fatty acid methyl esters and use of alpha-sulphonated fatty acid salts to in hibit redeposition of soil on fabric |
US08/836,821 US5945394A (en) | 1995-09-18 | 1996-09-17 | Heavy duty liquid detergent compositions comprising salts of α-sulfonated fatty acid methyl esters and use of α-sulphonated fatty acid salts to inhibit redeposition of soil on fabric |
NZ318989A NZ318989A (en) | 1995-09-18 | 1996-09-17 | Heavy duty detergent containing an alpha-sulphonated alkyl ester of a fatty acid; inhibition of soil redeposition |
JP9512836A JPH10502969A (ja) | 1995-09-18 | 1996-09-17 | αスルホン化脂肪酸メチルエステルの塩を含んでなる重質液体洗剤組成物および織物への汚れの再付着を抑制するαスルホン化脂肪酸塩の使用 |
MX9703647A MX9703647A (es) | 1995-09-18 | 1996-09-17 | Composiciones detergentes liquidas que comprenden sales de esteres metilicos de acidos grasos alfa-sulfonados y uso de las sales de acidos grasos alfa-sufonados para inhibir la redeposicion de suciedad o manchas en los tejidos. |
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US52950195A | 1995-09-18 | 1995-09-18 | |
US08/529,501 | 1995-09-18 | ||
US59174896A | 1996-01-25 | 1996-01-25 | |
US08/591,748 | 1996-01-25 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO1997011143A2 true WO1997011143A2 (fr) | 1997-03-27 |
WO1997011143A3 WO1997011143A3 (fr) | 1997-04-24 |
Family
ID=27063032
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US1996/014889 WO1997011143A2 (fr) | 1995-09-18 | 1996-09-17 | Compositions detergentes tres puissantes comprenant des sels d'esters methyliques alpha sulfones d'acide gras et utilisation des sels d'acides gras alpha sulfones pour inhiber la redeposition des salissures sur le tissu |
Country Status (10)
Country | Link |
---|---|
EP (1) | EP0792336A2 (fr) |
JP (1) | JPH10502969A (fr) |
AR (1) | AR003618A1 (fr) |
AU (1) | AU699950B2 (fr) |
BR (1) | BR9606651A (fr) |
CA (1) | CA2205592C (fr) |
CO (1) | CO5040238A1 (fr) |
MX (1) | MX9703647A (fr) |
NZ (1) | NZ318989A (fr) |
WO (1) | WO1997011143A2 (fr) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2006088928A1 (fr) * | 2005-02-14 | 2006-08-24 | The Dial Corporation | Composition surfactante contenant un sulfate d'alcool-ethoxy destinee a s'utiliser dans des detergents a lessive et processus de fabrication correspondant |
WO2015091110A3 (fr) * | 2013-12-17 | 2015-08-13 | Henkel Ag & Co. Kgaa | Détergent contenant du méthylestersulfonate (mes) et du méthylesteréthoxylate (mee) |
EP2489722A4 (fr) * | 2009-10-15 | 2016-06-01 | Lion Corp | Composition détergente liquide |
WO2016160407A1 (fr) * | 2015-03-31 | 2016-10-06 | Stepan Company | Détergents à base de tensioactifs ester gras alpha-sulfonés |
EP3441447A1 (fr) * | 2017-08-09 | 2019-02-13 | Henkel AG & Co. KGaA | Éther de cellulose non ionique en tant que renforçateur d'élimination de salissures lors du nettoyage de surfaces dures |
EP3990603B1 (fr) | 2019-06-28 | 2022-12-07 | Unilever Global Ip Limited | Composition de détergent |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5481719B2 (ja) * | 2007-12-28 | 2014-04-23 | ライオン株式会社 | 粒状洗剤組成物 |
JP5481720B2 (ja) * | 2007-12-28 | 2014-04-23 | ライオン株式会社 | 粒状洗剤組成物 |
ATE534721T1 (de) * | 2009-09-14 | 2011-12-15 | Procter & Gamble | Reinigungsmittelzusammensetzung |
MY165144A (en) * | 2011-04-18 | 2018-02-28 | Lion Corp | Liquid detergent |
CN106047529A (zh) * | 2016-06-30 | 2016-10-26 | 安徽泰隆成亚集团股份有限公司 | 环保浓缩型衣料用液体洗涤剂 |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA795748A (en) * | 1968-10-01 | Stepan Chemical Company | Heavy-duty synthetic detergent compositions | |
CH490486A (de) * | 1962-04-24 | 1970-05-15 | Stepan Chemical Co | Waschmittel |
FR2107437A5 (fr) * | 1970-09-09 | 1972-05-05 | Unilever Nv | |
FR2235193A1 (en) * | 1973-06-30 | 1975-01-24 | Henkel & Cie Gmbh | Non-eutrophicating detergent composition - containing salts of alpha-sulphonated long chain fatty esters |
EP0302402A2 (fr) * | 1987-08-07 | 1989-02-08 | Henkel Kommanditgesellschaft auf Aktien | Agents de lavage et de nettoyage pour le linge |
EP0336740A2 (fr) * | 1988-04-06 | 1989-10-11 | Unilever Plc | Composition détergente |
EP0363872A2 (fr) * | 1988-10-12 | 1990-04-18 | Lion Corporation | Détergent granulé à densité élevée |
WO1991013959A1 (fr) * | 1990-03-05 | 1991-09-19 | The Procter & Gamble Company | Compositions de detergents de lavage de vaisselle liquides pour lavages delicats |
WO1995010585A1 (fr) * | 1993-10-12 | 1995-04-20 | Stepan Company | Compositions detergentes liquides comprenant des sels d'esters methyliques alpha sulfones d'acide gras et des agents tensio-actifs anioniques |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6059960B2 (ja) * | 1980-11-28 | 1985-12-27 | ライオン株式会社 | 粉セツケン組成物 |
JPH06330084A (ja) * | 1993-05-21 | 1994-11-29 | Lion Corp | 洗浄剤組成物 |
-
1996
- 1996-09-17 AU AU71112/96A patent/AU699950B2/en not_active Ceased
- 1996-09-17 JP JP9512836A patent/JPH10502969A/ja active Pending
- 1996-09-17 CA CA002205592A patent/CA2205592C/fr not_active Expired - Lifetime
- 1996-09-17 NZ NZ318989A patent/NZ318989A/en unknown
- 1996-09-17 BR BR9606651A patent/BR9606651A/pt not_active Application Discontinuation
- 1996-09-17 MX MX9703647A patent/MX9703647A/es unknown
- 1996-09-17 EP EP96932244A patent/EP0792336A2/fr not_active Withdrawn
- 1996-09-17 WO PCT/US1996/014889 patent/WO1997011143A2/fr not_active Application Discontinuation
- 1996-09-18 AR ARP960104404A patent/AR003618A1/es unknown
- 1996-09-18 CO CO96049859A patent/CO5040238A1/es unknown
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA795748A (en) * | 1968-10-01 | Stepan Chemical Company | Heavy-duty synthetic detergent compositions | |
CH490486A (de) * | 1962-04-24 | 1970-05-15 | Stepan Chemical Co | Waschmittel |
FR2107437A5 (fr) * | 1970-09-09 | 1972-05-05 | Unilever Nv | |
FR2235193A1 (en) * | 1973-06-30 | 1975-01-24 | Henkel & Cie Gmbh | Non-eutrophicating detergent composition - containing salts of alpha-sulphonated long chain fatty esters |
EP0302402A2 (fr) * | 1987-08-07 | 1989-02-08 | Henkel Kommanditgesellschaft auf Aktien | Agents de lavage et de nettoyage pour le linge |
EP0336740A2 (fr) * | 1988-04-06 | 1989-10-11 | Unilever Plc | Composition détergente |
EP0363872A2 (fr) * | 1988-10-12 | 1990-04-18 | Lion Corporation | Détergent granulé à densité élevée |
WO1991013959A1 (fr) * | 1990-03-05 | 1991-09-19 | The Procter & Gamble Company | Compositions de detergents de lavage de vaisselle liquides pour lavages delicats |
WO1995010585A1 (fr) * | 1993-10-12 | 1995-04-20 | Stepan Company | Compositions detergentes liquides comprenant des sels d'esters methyliques alpha sulfones d'acide gras et des agents tensio-actifs anioniques |
Non-Patent Citations (4)
Title |
---|
DATABASE WPI Week 8228 Derwent Publications Ltd., London, GB; AN 82-58580E XP002045729 & JP 57 092 098 A (LION CORP) , 8 June 1982 * |
PATENT ABSTRACTS OF JAPAN vol. 94, no. 011 & JP 06 330084 A (LION CORP), 29 November 1994, * |
See also references of EP0792336A2 * |
SMITH N R: "ALPHA-SULFO METHYL ESTERS" HAPPI HOUSEHOLD AND PERSONAL PRODUCTS INDUSTRY, vol. 26, no. 3, March 1989, page 58, 60 XP000008005 * |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2006088928A1 (fr) * | 2005-02-14 | 2006-08-24 | The Dial Corporation | Composition surfactante contenant un sulfate d'alcool-ethoxy destinee a s'utiliser dans des detergents a lessive et processus de fabrication correspondant |
WO2006089013A1 (fr) * | 2005-02-14 | 2006-08-24 | The Dial Corporation | Composition de detergent amelioree presentant un plus grand pouvoir blanchissant |
US7754669B2 (en) | 2005-02-14 | 2010-07-13 | The Dial Corporation | Detergent composition with enhanced whitening power |
EP2489722A4 (fr) * | 2009-10-15 | 2016-06-01 | Lion Corp | Composition détergente liquide |
KR101791707B1 (ko) | 2009-10-15 | 2017-10-30 | 라이온 가부시키가이샤 | 액체 세정제 조성물 |
WO2015091110A3 (fr) * | 2013-12-17 | 2015-08-13 | Henkel Ag & Co. Kgaa | Détergent contenant du méthylestersulfonate (mes) et du méthylesteréthoxylate (mee) |
WO2016160407A1 (fr) * | 2015-03-31 | 2016-10-06 | Stepan Company | Détergents à base de tensioactifs ester gras alpha-sulfonés |
EP3441447A1 (fr) * | 2017-08-09 | 2019-02-13 | Henkel AG & Co. KGaA | Éther de cellulose non ionique en tant que renforçateur d'élimination de salissures lors du nettoyage de surfaces dures |
EP3990603B1 (fr) | 2019-06-28 | 2022-12-07 | Unilever Global Ip Limited | Composition de détergent |
Also Published As
Publication number | Publication date |
---|---|
AR003618A1 (es) | 1998-08-05 |
JPH10502969A (ja) | 1998-03-17 |
EP0792336A2 (fr) | 1997-09-03 |
AU699950B2 (en) | 1998-12-17 |
CA2205592C (fr) | 2001-12-11 |
BR9606651A (pt) | 1997-09-30 |
MX9703647A (es) | 1997-08-30 |
CA2205592A1 (fr) | 1997-03-27 |
CO5040238A1 (es) | 2001-05-29 |
NZ318989A (en) | 1999-10-28 |
AU7111296A (en) | 1997-04-09 |
WO1997011143A3 (fr) | 1997-04-24 |
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