WO1989012689A1 - Method of obtaining a mixture of ribonucleotides - Google Patents

Method of obtaining a mixture of ribonucleotides Download PDF

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Publication number
WO1989012689A1
WO1989012689A1 PCT/SU1988/000269 SU8800269W WO8912689A1 WO 1989012689 A1 WO1989012689 A1 WO 1989012689A1 SU 8800269 W SU8800269 W SU 8800269W WO 8912689 A1 WO8912689 A1 WO 8912689A1
Authority
WO
WIPO (PCT)
Prior art keywords
mixture
separation
fraction
temperature
target product
Prior art date
Application number
PCT/SU1988/000269
Other languages
English (en)
French (fr)
Russian (ru)
Inventor
Boris Borisovich Fux
Marina Evgenievna Shabanova
Svyatoslav Nikolaevich Fedorov
Jury Mikhailovich Krasnopolsky
Uldis Yanovich Mixtais
Evgeny Dmitrievich Ermolaev
Mara Augustovna Gailuma
Original Assignee
Institut Morfologii Cheloveka Akademii Meditsinski
Mezhotraslevoi Nauchno-Tekhnichesky Komplex ''mikr
Nauchno-Proizvodstvennoe Obiedinenie ''biolar'' Ak
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institut Morfologii Cheloveka Akademii Meditsinski, Mezhotraslevoi Nauchno-Tekhnichesky Komplex ''mikr, Nauchno-Proizvodstvennoe Obiedinenie ''biolar'' Ak filed Critical Institut Morfologii Cheloveka Akademii Meditsinski
Priority to DE19883891346 priority Critical patent/DE3891346T1/de
Publication of WO1989012689A1 publication Critical patent/WO1989012689A1/ru
Priority to GB9002774A priority patent/GB2231052A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • C12P19/26Preparation of nitrogen-containing carbohydrates
    • C12P19/28N-glycosides
    • C12P19/30Nucleotides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P27/00Drugs for disorders of the senses
    • A61P27/02Ophthalmic agents

Definitions

  • the methods of obtaining a mixture of drugs known to provide healing properties (“Bulletin of Exterior Biology and Medicine”, 1969, Access /, J 9, p. 23-26) are known.
  • the indicated 15 method is included in the case that the protein acid with a concentration of 5-10 mg / ml is processed at a temperature of 45 ° during the first hour.
  • the indicated method is char- acterized by a low quality product.
  • P ⁇ luchae maya mixture ⁇ ib ⁇ nu ⁇ le ⁇ id ⁇ v s ⁇ de ⁇ - 20 zhi ⁇ ⁇ imesi bel ⁇ a, vys ⁇ m ⁇ le ⁇ ulya ⁇ ny ⁇ ⁇ i ⁇ genyay ⁇ vesches ⁇ v, ⁇ e ⁇ mu v ⁇ zm ⁇ zhn ⁇ ⁇ l ⁇ its mes ⁇ n ⁇ e ⁇ imenenie as' na ⁇ uzh- ny ⁇ ⁇ vyaz ⁇ .
  • the hydration of the fermented acid in the diet is 4.5-5.5, and the patient is hydrated;
  • hydrolysis of the enzyme is a pan-regenerative ideal, while at a temperature of more than 65 ° C, partially evaporates
  • Separation of the fraction of vibrations on membranes is preferable to a temperature of 20-30 ° ⁇ and pressure
  • ⁇ sazhdenie mixture ⁇ ib ⁇ nu ⁇ le ⁇ id ⁇ v ⁇ bem ⁇ m e ⁇ an ⁇ la least 8 ⁇ a ⁇ n ⁇ g ⁇ not dae ⁇ v ⁇ zm ⁇ zhn ⁇ s ⁇ i ⁇ ln ⁇ s ⁇ yu ⁇ sv ⁇ b ⁇ di ⁇ sya ⁇ niz ⁇ m ⁇ le ⁇ ulya ⁇ ny ⁇ ⁇ i ⁇ genny ⁇ s ⁇ e of the connections 10, 10 ⁇ sazhdenie b ⁇ lee ⁇ a ⁇ nym ⁇ bem ⁇ m e ⁇ an ⁇ la not ⁇ iv ⁇ di ⁇ ⁇ increase ⁇ l ⁇ zhi ⁇ eln ⁇ g ⁇ e ⁇ e ⁇ a.
  • the inventive method allows to increase the output of the target product by 8-15 by comparison with the known method, and also to increase the cost-benefit of the product. 25 BEST MODE FOR CARRYING OUT THE INVENTION
  • the claimed method is as follows. Fermented acid is suspended in distilled water, and alkaline products are 4.5–5.5 alkaline. Then, in the case of the distributor, the add-on acid add the enzyme 30 to the fungicidal agent, heat the agent up to 62-65 ° ⁇ and the extractor is hydrated After the end of the hydrolysis, it is refrigerated, added to it ethanol and mixed. In order to separate the small precipitate that has grown after adding 35 ethanol, the mixture is micromotor-assisted. Then, the illuminated device is activated by ultrafiltration through a membrane with a size of 50-150 ⁇ , preferably at a temperature of 20-30 ° C and a pressure of 0.1-30 ° C. After office,
  • the filter for concentrate will add the distilled water and will receive an additional quantity of filter.
  • the amount of ultrafilter adds to the mixing of ethanol. After the mixture has been left to stand, the horticultural liquid is removed from the product and the sediment is washed off. The target product may be received as dry, as well as in the form of a solution. For this mixture of ribo-nucleotides, isolated after the deposition of 8-10 large-scale plants
  • the resulting target product is white
  • the total capacity of the hydrolysis is 465 ml. Then it is cooled to a temperature of 25-35 ° C, it is added 120 ml of ethanol, the filter is removed and the particulate is filtered and it is particulate.
  • the resulting yellow color filter is filtered through a black and white filter, and then through a membrane with a pressure of 2000 psi and a pressure of 98 kPa.
  • Example 2 Separated sludge (39 g of dry mix) is dissolved in a 0.55% solution of hydrochloride (995 ml) when the water is removed and the water is removed. The resulting yellow color filter is filtered through a black and white filter, and then through a membrane with a high pressure of 2200 ⁇ - 8 - ⁇ and a pressure of 78 ⁇ Pa. Dispensing the unit under stable conditions dilutes the ampoules from the neutral glass at 3 ml and waits for processing in the autoclave at a temperature of 32. Concentration of vibrators in order to
  • a mixture of drugs obtained by the claimed method is used in medical practice as a medicine for the treatment of therapeutic abnormalities.
  • the indicated mixture may be used for the treatment of myopathy, a number of immunodeficiencies, injuries, burns and other illnesses—

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Molecular Biology (AREA)
  • Genetics & Genomics (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medicinal Chemistry (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Ophthalmology & Optometry (AREA)
  • Animal Behavior & Ethology (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
PCT/SU1988/000269 1988-06-14 1988-12-20 Method of obtaining a mixture of ribonucleotides WO1989012689A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
DE19883891346 DE3891346T1 (de) 1988-12-20 1988-12-20 Verfahren zur herstellung des ribonukleotidengemisches
GB9002774A GB2231052A (en) 1988-06-14 1990-02-08 Method of preparing a mixture of ribonucleotides

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SU4432648/28 1988-06-14
SU884432648A SU1575359A1 (ru) 1988-06-14 1988-06-14 Способ получени рибонуклеотидов

Publications (1)

Publication Number Publication Date
WO1989012689A1 true WO1989012689A1 (en) 1989-12-28

Family

ID=21378060

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/SU1988/000269 WO1989012689A1 (en) 1988-06-14 1988-12-20 Method of obtaining a mixture of ribonucleotides

Country Status (11)

Country Link
US (1) US5064758A (forum.php)
JP (1) JPH03501563A (forum.php)
CN (1) CN1053090A (forum.php)
ES (1) ES2010913A6 (forum.php)
FR (1) FR2635533A1 (forum.php)
GB (1) GB2231052A (forum.php)
IN (1) IN168260B (forum.php)
IT (1) IT1229178B (forum.php)
PL (1) PL278876A1 (forum.php)
SU (1) SU1575359A1 (forum.php)
WO (1) WO1989012689A1 (forum.php)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013089835A1 (en) 2011-12-12 2013-06-20 The Board Of Trustees Of The University Of Illinois Composition and method for treating nucleic acid-related eye disease

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1110567C (zh) * 2000-02-17 2003-06-04 北京太宫生物技术有限责任公司 脱氧核糖核苷三磷酸的制备方法
RU2274658C2 (ru) * 2004-02-03 2006-04-20 Российский химико-технологический университет им. Д.И. Менделеева Способ получения панкреатического гидролизата рибонуклеиновой кислоты
RU2244008C1 (ru) * 2004-02-05 2005-01-10 Закрытое акционерное общество "Биоамид" Усовершенствованный способ получения нуклеината натрия
JP4810164B2 (ja) * 2004-09-03 2011-11-09 富士フイルム株式会社 核酸分離精製方法
RU2392329C1 (ru) * 2008-10-07 2010-06-20 Общество с ограниченной ответственностью "ВИТАЛАНГ" Способ получения высокополимерной рнк из дрожжей
CN112544827B (zh) * 2020-12-08 2024-01-30 南京工业大学 一种罗氏沼虾饲料添加剂及其制备方法与应用

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3920519A (en) * 1973-02-14 1975-11-18 Yuh Norimoto Enzymatic hydrolysis of ribonucleic acid
US4190649A (en) * 1976-06-03 1980-02-26 Mirko Beljanski Polyribonucleotides capable of promoting the genesis of leucocytes and blood platelets
DE1941709C3 (de) * 1969-08-16 1981-07-16 Diether Prof. Dr. Bern Jachertz Verfahren zur enzymatischen Vermehrung von informatorischer Ribonucleinsäure
EP0149775A1 (en) * 1983-12-09 1985-07-31 Otsuka Pharmaceutical Factory, Inc. Compositions of nucleic acid components

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1194709B (de) * 1960-05-25 1965-06-10 Voith Gmbh J M Drehservomotor, insbesondere zum Verstellen der Leitschaufeln von Wasserturbinen

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1941709C3 (de) * 1969-08-16 1981-07-16 Diether Prof. Dr. Bern Jachertz Verfahren zur enzymatischen Vermehrung von informatorischer Ribonucleinsäure
US3920519A (en) * 1973-02-14 1975-11-18 Yuh Norimoto Enzymatic hydrolysis of ribonucleic acid
US4190649A (en) * 1976-06-03 1980-02-26 Mirko Beljanski Polyribonucleotides capable of promoting the genesis of leucocytes and blood platelets
EP0149775A1 (en) * 1983-12-09 1985-07-31 Otsuka Pharmaceutical Factory, Inc. Compositions of nucleic acid components

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013089835A1 (en) 2011-12-12 2013-06-20 The Board Of Trustees Of The University Of Illinois Composition and method for treating nucleic acid-related eye disease
EP2790722A4 (en) * 2011-12-12 2015-09-09 Univ Illinois COMPOSITION AND METHOD FOR THE TREATMENT OF EYE DISEASES RELATED TO NUCLEIC ACID
US9867871B2 (en) 2011-12-12 2018-01-16 The Board Of Trustees Of The University Of Illinois Composition and method for treating nucleic acid-related eye disease
US10328129B2 (en) 2011-12-12 2019-06-25 The Board Of Trustees Of The University Of Illinois Composition and method for treating nucleic acid-related eye disease
US11376312B2 (en) 2011-12-12 2022-07-05 The Board Of Trustees Of The University Of Illinois Composition and method for treating nucleic acid-related eye disease

Also Published As

Publication number Publication date
GB9002774D0 (en) 1990-07-11
PL278876A1 (en) 1989-12-27
IT8920064A0 (it) 1989-04-07
US5064758A (en) 1991-11-12
SU1575359A1 (ru) 1991-05-15
CN1053090A (zh) 1991-07-17
FR2635533A1 (fr) 1990-02-23
JPH03501563A (ja) 1991-04-11
IT1229178B (it) 1991-07-23
IN168260B (forum.php) 1991-03-02
GB2231052A (en) 1990-11-07
ES2010913A6 (es) 1989-12-01

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