UA80456C2 - Method for removing mercury from solutions contaminated with mercury - Google Patents
Method for removing mercury from solutions contaminated with mercury Download PDFInfo
- Publication number
- UA80456C2 UA80456C2 UAA200506263A UA2005006263A UA80456C2 UA 80456 C2 UA80456 C2 UA 80456C2 UA A200506263 A UAA200506263 A UA A200506263A UA 2005006263 A UA2005006263 A UA 2005006263A UA 80456 C2 UA80456 C2 UA 80456C2
- Authority
- UA
- Ukraine
- Prior art keywords
- mercury
- solution
- filtering
- contaminated
- carbon
- Prior art date
Links
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 title claims abstract description 63
- 229910052753 mercury Inorganic materials 0.000 title claims abstract description 63
- 238000000034 method Methods 0.000 title claims description 52
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 83
- 238000001914 filtration Methods 0.000 claims abstract description 40
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 24
- 229910052783 alkali metal Inorganic materials 0.000 claims description 17
- 150000001340 alkali metals Chemical class 0.000 claims description 17
- 239000003518 caustics Substances 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 238000004438 BET method Methods 0.000 claims 1
- 238000012876 topography Methods 0.000 claims 1
- 239000000243 solution Substances 0.000 description 46
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 14
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 11
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 10
- 239000003245 coal Substances 0.000 description 10
- 239000011734 sodium Substances 0.000 description 10
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 9
- 229910052700 potassium Inorganic materials 0.000 description 9
- 239000011591 potassium Substances 0.000 description 9
- 229910000497 Amalgam Inorganic materials 0.000 description 8
- 239000003513 alkali Substances 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 5
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 5
- 239000002657 fibrous material Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 5
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- 238000000354 decomposition reaction Methods 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- 238000007429 general method Methods 0.000 description 4
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 4
- 229910001023 sodium amalgam Inorganic materials 0.000 description 4
- 235000011121 sodium hydroxide Nutrition 0.000 description 4
- DKGAVHZHDRPRBM-UHFFFAOYSA-N tert-butyl alcohol Substances CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 4
- 229910000567 Amalgam (chemistry) Inorganic materials 0.000 description 3
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- 238000002604 ultrasonography Methods 0.000 description 3
- GHVZOJONCUEWAV-UHFFFAOYSA-N [K].CCO Chemical compound [K].CCO GHVZOJONCUEWAV-UHFFFAOYSA-N 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 2
- 229910001514 alkali metal chloride Inorganic materials 0.000 description 2
- 238000004581 coalescence Methods 0.000 description 2
- 238000005868 electrolysis reaction Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- BDAWXSQJJCIFIK-UHFFFAOYSA-N potassium methoxide Chemical compound [K+].[O-]C BDAWXSQJJCIFIK-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000002723 alicyclic group Chemical group 0.000 description 1
- -1 aliphatic alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 229910052792 caesium Inorganic materials 0.000 description 1
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- RCTYPNKXASFOBE-UHFFFAOYSA-M chloromercury Chemical class [Hg]Cl RCTYPNKXASFOBE-UHFFFAOYSA-M 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005087 graphitization Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000010297 mechanical methods and process Methods 0.000 description 1
- 150000002730 mercury Chemical class 0.000 description 1
- MJGFBOZCAJSGQW-UHFFFAOYSA-N mercury sodium Chemical compound [Na].[Hg] MJGFBOZCAJSGQW-UHFFFAOYSA-N 0.000 description 1
- 229940008718 metallic mercury Drugs 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002006 petroleum coke Substances 0.000 description 1
- 238000004525 petroleum distillation Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 229910052701 rubidium Inorganic materials 0.000 description 1
- IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- QDRKDTQENPPHOJ-UHFFFAOYSA-N sodium ethoxide Chemical compound [Na+].CC[O-] QDRKDTQENPPHOJ-UHFFFAOYSA-N 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B43/00—Obtaining mercury
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S210/00—Liquid purification or separation
- Y10S210/902—Materials removed
- Y10S210/911—Cumulative poison
- Y10S210/912—Heavy metal
- Y10S210/914—Mercury
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Treating Waste Gases (AREA)
- Removal Of Specific Substances (AREA)
- Water Treatment By Electricity Or Magnetism (AREA)
- Carbon And Carbon Compounds (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10255240A DE10255240A1 (de) | 2002-11-26 | 2002-11-26 | Verfahren zur Entfernung von Quecksilber aus mit Quecksilber verunreinigten Lösungen |
| PCT/EP2003/012817 WO2004048624A1 (de) | 2002-11-26 | 2003-11-17 | Verfahren zur entfernung von quecksilber aus mit quecksilber verunreinigten lösungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA80456C2 true UA80456C2 (en) | 2007-09-25 |
Family
ID=32308735
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA200506263A UA80456C2 (en) | 2002-11-26 | 2003-11-17 | Method for removing mercury from solutions contaminated with mercury |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US7332090B2 (pl) |
| EP (1) | EP1567683B1 (pl) |
| AT (1) | ATE331817T1 (pl) |
| AU (1) | AU2003288080A1 (pl) |
| DE (2) | DE10255240A1 (pl) |
| ES (1) | ES2266884T3 (pl) |
| PL (1) | PL209006B1 (pl) |
| RU (1) | RU2323269C2 (pl) |
| UA (1) | UA80456C2 (pl) |
| WO (1) | WO2004048624A1 (pl) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10255239A1 (de) * | 2002-11-26 | 2004-06-09 | Basf Ag | Verfahren zur Entfernung von Quecksilber aus mit Quecksilber verunreinigten Lösungen |
| DE102005062654A1 (de) * | 2005-12-23 | 2007-06-28 | Basf Ag | Verfahren zur Gewinnung von Alkoholaten |
| CN101472678A (zh) * | 2006-06-21 | 2009-07-01 | 巴斯夫欧洲公司 | 吸收组合物和除汞方法 |
| US7767079B2 (en) * | 2006-09-06 | 2010-08-03 | Darcy Michael J | Amalgam separator |
| GB2442950B (en) * | 2006-10-20 | 2010-06-23 | Univ Manchester | Adsorbents for treating contaminated liquids |
| KR20100133394A (ko) * | 2008-03-10 | 2010-12-21 | 바스프 에스이 | 탄화수소 스트림으로부터 수은을 제거하는 방법 |
| FR2959240B1 (fr) * | 2010-04-23 | 2014-10-24 | Inst Francais Du Petrole | Procede d'elimination des especes mercuriques presentes dans une charge hydrocarbonee |
| CN115011819B (zh) * | 2022-08-05 | 2022-10-28 | 北京博朗德科技有限公司 | 一种多级压滤破膜汞提纯装置 |
| WO2024073856A1 (en) * | 2022-10-07 | 2024-04-11 | Li-Cycle Corp. | System, apparatus and method for improving filter efficacy during recovery of one or more metals |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE221968C (pl) | ||||
| US3502434A (en) * | 1966-04-22 | 1970-03-24 | Canadian Ind | Process and apparatus for removing mercury from caustic soda solutions |
| US3600285A (en) | 1969-10-21 | 1971-08-17 | Olin Corp | Mercury recovery |
| US4030912A (en) | 1973-04-11 | 1977-06-21 | Hercules Incorporated | Certain oximinyl allophanates and their use as herbicides |
| US3897331A (en) * | 1974-10-10 | 1975-07-29 | Allied Chem | Mercury recovery |
| IT1043119B (it) | 1975-10-03 | 1980-02-20 | Tecneco Spa | Metodo per la rimozione di mer curio metallico |
| DD139068A3 (de) * | 1976-12-10 | 1979-12-12 | Harri Tischendorf | Verfahren zur abtrennung von quecksilber aus alkalilaugen |
| DD221968A3 (de) * | 1977-11-15 | 1985-05-08 | Buna Chem Werke Veb | Verfahren zur zersetzung von natriumamalgen in vertikalzersetzern |
| JPS58128182A (ja) | 1982-01-22 | 1983-07-30 | Nippon Kokan Kk <Nkk> | 廃液中の有害物質除去方法 |
| DE3335127A1 (de) | 1983-09-28 | 1985-04-11 | Wacker-Chemie GmbH, 8000 München | Verfahren zur abtrennung von quecksilber aus waessrigen fluessigkeiten |
| DE3438098A1 (de) | 1984-10-18 | 1986-04-30 | Hoechst Ag, 6230 Frankfurt | Verfahren zur entfernung von quecksilber aus loesungen |
| US5080799A (en) | 1990-05-23 | 1992-01-14 | Mobil Oil Corporation | Hg removal from wastewater by regenerative adsorption |
| DE4030912A1 (de) * | 1990-09-29 | 1992-04-02 | Basf Ag | Verfahren zur abscheidung von metallionen aus prozess- und abwaessern |
| DE19521587A1 (de) | 1995-06-14 | 1996-12-19 | Bayer Ag | Verfahren und Katalysator zur Herstellung von aromatischen Aminen durch Gasphasenhydrierung |
| DE19704889C2 (de) | 1997-02-10 | 1999-11-04 | Degussa | Verfahren zur Entfernung von Quecksilber aus Alkalialkoholat-Lösungen |
| DE19818277A1 (de) * | 1998-04-23 | 1999-10-28 | Andreas Noack | Adsorptionsvorrichtung mit geringem Druckabfall zur Reinigung von Fluiden |
| WO2002001660A1 (fr) * | 2000-06-29 | 2002-01-03 | Osaka Gas Company Limited | Composition conductrice pour separateur de pile a combustible de type a polymere solide, separateur de pile a combustible de type a polymere solide, pile a combustible de type a polymere solide et systeme de pile a combustible de type a polymere solide utilisant ce separateur |
-
2002
- 2002-11-26 DE DE10255240A patent/DE10255240A1/de not_active Withdrawn
-
2003
- 2003-11-17 WO PCT/EP2003/012817 patent/WO2004048624A1/de active Search and Examination
- 2003-11-17 UA UAA200506263A patent/UA80456C2/uk unknown
- 2003-11-17 DE DE50304088T patent/DE50304088D1/de not_active Expired - Lifetime
- 2003-11-17 RU RU2005120171/02A patent/RU2323269C2/ru not_active IP Right Cessation
- 2003-11-17 AU AU2003288080A patent/AU2003288080A1/en not_active Abandoned
- 2003-11-17 ES ES03779947T patent/ES2266884T3/es not_active Expired - Lifetime
- 2003-11-17 AT AT03779947T patent/ATE331817T1/de active
- 2003-11-17 EP EP03779947A patent/EP1567683B1/de not_active Expired - Lifetime
- 2003-11-17 PL PL379028A patent/PL209006B1/pl unknown
- 2003-11-17 US US10/535,969 patent/US7332090B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| ES2266884T3 (es) | 2007-03-01 |
| ATE331817T1 (de) | 2006-07-15 |
| AU2003288080A1 (en) | 2004-06-18 |
| WO2004048624A1 (de) | 2004-06-10 |
| PL209006B1 (pl) | 2011-07-29 |
| DE50304088D1 (de) | 2006-08-10 |
| EP1567683B1 (de) | 2006-06-28 |
| US7332090B2 (en) | 2008-02-19 |
| DE10255240A1 (de) | 2004-06-09 |
| PL379028A1 (pl) | 2006-06-26 |
| US20060049109A1 (en) | 2006-03-09 |
| EP1567683A1 (de) | 2005-08-31 |
| RU2005120171A (ru) | 2006-01-20 |
| RU2323269C2 (ru) | 2008-04-27 |
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