TWI580804B - 正極及蓄電裝置的製造方法 - Google Patents
正極及蓄電裝置的製造方法 Download PDFInfo
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- TWI580804B TWI580804B TW101113022A TW101113022A TWI580804B TW I580804 B TWI580804 B TW I580804B TW 101113022 A TW101113022 A TW 101113022A TW 101113022 A TW101113022 A TW 101113022A TW I580804 B TWI580804 B TW I580804B
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- Prior art keywords
- current collector
- positive electrode
- layer
- active material
- electrode current
- Prior art date
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- 238000003860 storage Methods 0.000 title claims description 55
- 238000004519 manufacturing process Methods 0.000 title claims description 20
- 238000000034 method Methods 0.000 title claims description 15
- 229910052744 lithium Inorganic materials 0.000 claims description 119
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 117
- 239000007773 negative electrode material Substances 0.000 claims description 44
- 239000007784 solid electrolyte Substances 0.000 claims description 36
- 239000000463 material Substances 0.000 claims description 32
- 239000010936 titanium Substances 0.000 claims description 32
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 25
- 239000006183 anode active material Substances 0.000 claims description 22
- 238000010438 heat treatment Methods 0.000 claims description 22
- 229910052719 titanium Inorganic materials 0.000 claims description 22
- 238000004544 sputter deposition Methods 0.000 claims description 18
- 239000000758 substrate Substances 0.000 claims description 18
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- 239000010935 stainless steel Substances 0.000 claims description 15
- 229910001220 stainless steel Inorganic materials 0.000 claims description 15
- -1 Li 14 ZnGe 4 O 16 Inorganic materials 0.000 claims description 12
- 239000013078 crystal Substances 0.000 claims description 10
- 239000011149 active material Substances 0.000 claims description 9
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 7
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- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 229910052735 hafnium Inorganic materials 0.000 claims description 6
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 claims description 6
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 6
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 5
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 5
- 229910018119 Li 3 PO 4 Inorganic materials 0.000 claims description 5
- 229910001257 Nb alloy Inorganic materials 0.000 claims description 5
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- 229910052802 copper Inorganic materials 0.000 claims description 5
- 239000010949 copper Substances 0.000 claims description 5
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- 229910052731 fluorine Inorganic materials 0.000 claims description 5
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 4
- 229910000428 cobalt oxide Inorganic materials 0.000 claims description 4
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 claims description 4
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- 239000011347 resin Substances 0.000 claims description 4
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- 229910052718 tin Inorganic materials 0.000 claims description 4
- 229910020731 Li0.35La0.55TiO3 Inorganic materials 0.000 claims description 3
- 229910007860 Li3.25Ge0.25P0.75S4 Inorganic materials 0.000 claims description 3
- 229910010640 Li6BaLa2Ta2O12 Inorganic materials 0.000 claims description 3
- 229910020346 SiS 2 Inorganic materials 0.000 claims description 3
- 229910001128 Sn alloy Inorganic materials 0.000 claims description 3
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 3
- 229910000449 hafnium oxide Inorganic materials 0.000 claims description 3
- WIHZLLGSGQNAGK-UHFFFAOYSA-N hafnium(4+);oxygen(2-) Chemical compound [O-2].[O-2].[Hf+4] WIHZLLGSGQNAGK-UHFFFAOYSA-N 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 229910052697 platinum Inorganic materials 0.000 claims description 3
- 229910052715 tantalum Inorganic materials 0.000 claims description 3
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims description 3
- MZLGASXMSKOWSE-UHFFFAOYSA-N tantalum nitride Chemical compound [Ta]#N MZLGASXMSKOWSE-UHFFFAOYSA-N 0.000 claims description 3
- 229910018091 Li 2 S Inorganic materials 0.000 claims description 2
- 239000010941 cobalt Substances 0.000 claims description 2
- 229910017052 cobalt Inorganic materials 0.000 claims description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 2
- 229910001200 Ferrotitanium Inorganic materials 0.000 claims 2
- 229910009324 Li2S-SiS2-Li3PO4 Inorganic materials 0.000 claims 2
- 229910009328 Li2S-SiS2—Li3PO4 Inorganic materials 0.000 claims 2
- 229910007295 Li2S—SiS2—Li3PO4 Inorganic materials 0.000 claims 2
- 229910004283 SiO 4 Inorganic materials 0.000 claims 2
- 229910052727 yttrium Inorganic materials 0.000 claims 2
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 1
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- 239000003792 electrolyte Substances 0.000 description 26
- 238000000354 decomposition reaction Methods 0.000 description 19
- 238000005259 measurement Methods 0.000 description 17
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 13
- 229910001416 lithium ion Inorganic materials 0.000 description 13
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 9
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- BFZPBUKRYWOWDV-UHFFFAOYSA-N lithium;oxido(oxo)cobalt Chemical compound [Li+].[O-][Co]=O BFZPBUKRYWOWDV-UHFFFAOYSA-N 0.000 description 6
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- 229910013870 LiPF 6 Inorganic materials 0.000 description 2
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 2
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- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
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- 229910052804 chromium Inorganic materials 0.000 description 1
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- UBEWDCMIDFGDOO-UHFFFAOYSA-N cobalt(2+);cobalt(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Co+2].[Co+3].[Co+3] UBEWDCMIDFGDOO-UHFFFAOYSA-N 0.000 description 1
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- 159000000002 lithium salts Chemical class 0.000 description 1
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Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/64—Carriers or collectors
- H01M4/66—Selection of materials
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
- H01M4/1391—Processes of manufacture of electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0402—Methods of deposition of the material
- H01M4/0421—Methods of deposition of the material involving vapour deposition
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/058—Construction or manufacture
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0471—Processes of manufacture in general involving thermal treatment, e.g. firing, sintering, backing particulate active material, thermal decomposition, pyrolysis
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49002—Electrical device making
- Y10T29/49108—Electric battery cell making
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Electrochemistry (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Cell Electrode Carriers And Collectors (AREA)
- Secondary Cells (AREA)
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| JP2011090685 | 2011-04-15 |
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| CN (2) | CN105679998B (enExample) |
| TW (1) | TWI580804B (enExample) |
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| KR101264337B1 (ko) * | 2010-08-13 | 2013-05-14 | 삼성에스디아이 주식회사 | 양극 활물질 및 이를 이용한 리튬 전지 |
| JP5775598B2 (ja) * | 2011-10-31 | 2015-09-09 | 株式会社日立製作所 | リチウムイオン二次電池 |
| US10044061B2 (en) * | 2014-06-11 | 2018-08-07 | Los Alamos National Security, Llc | Methods for growth of lithium-rich antiperovskite electrolyte films and use thereof |
| DE102015007291A1 (de) * | 2015-06-10 | 2016-12-15 | Forschungszentrum Jülich GmbH | Verfahren zur Herstellung nanostrukturierter Schichten |
| KR102572999B1 (ko) | 2016-12-09 | 2023-08-30 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 2차 전지 및 그 제작 방법 |
| JP6400771B1 (ja) * | 2017-04-11 | 2018-10-03 | 株式会社石井表記 | ヒータ付き減圧ユニット及び電池製造用装置 |
| CN109935836B (zh) * | 2017-12-19 | 2024-06-18 | 成都大超科技有限公司 | 集流体结构、锂电池电芯及其锂电池 |
| FR3076062B1 (fr) | 2017-12-21 | 2020-07-17 | Commissariat A L'energie Atomique Et Aux Energies Alternatives | Realisation d'un collecteur de dispositif microelectronique |
| US12142765B2 (en) | 2019-01-25 | 2024-11-12 | Semiconductor Energy Laboratory Co., Ltd. | All-solid-state battery and manufacturing method thereof |
| JP7525475B2 (ja) | 2019-03-26 | 2024-07-30 | 株式会社半導体エネルギー研究所 | 固体二次電池およびその作製方法 |
| CN114097121A (zh) | 2019-04-30 | 2022-02-25 | 株式会社半导体能源研究所 | 固态二次电池 |
| US20220209214A1 (en) | 2019-04-30 | 2022-06-30 | Semiconductor Energy Laboratory Co., Ltd. | Manufacturing apparatus for solid-state secondary battery and method for manufacturing solid-state secondary battery |
| WO2020250078A1 (ja) | 2019-06-12 | 2020-12-17 | 株式会社半導体エネルギー研究所 | 固体二次電池 |
| KR20220044723A (ko) | 2019-08-09 | 2022-04-11 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 음극, 이차 전지, 및 고체 이차 전지 |
| US12394799B2 (en) | 2019-10-18 | 2025-08-19 | Semiconductor Energy Laboratory Co., Ltd. | Secondary battery and manufacturing method thereof |
| FI130048B (fi) * | 2020-04-17 | 2022-12-30 | Pulsedeon Oy | Menetelmä litiumia ja kiinteitä epäorgaanisia elektrolyyttejä hyödyntävän energian varastointilaitteen valmistukseen |
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| TW200808990A (en) * | 2004-12-08 | 2008-02-16 | Symmorphix Inc | Deposition of LiCoO2 |
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| US4916035A (en) * | 1987-08-06 | 1990-04-10 | Matsushita Electric Industrial Co., Ltd. | Photoelectrochemical cells having functions as a solar cell and a secondary cell |
| JPH08130015A (ja) * | 1994-10-27 | 1996-05-21 | Mitsubishi Cable Ind Ltd | 負極材及びその負極とＬｉ二次電池 |
| JPH11162451A (ja) * | 1997-11-27 | 1999-06-18 | Matsushita Electric Ind Co Ltd | リチウム二次電池と、そのリチウム二次電池の負極用ペーストの製造方法ならびにその製造方法による負極用ペーストを備えたリチウム二次電池 |
| JP4213474B2 (ja) * | 2001-04-24 | 2009-01-21 | パナソニック株式会社 | 二次電池とその製造方法 |
| US6517968B2 (en) * | 2001-06-11 | 2003-02-11 | Excellatron Solid State, Llc | Thin lithium film battery |
| WO2004093223A2 (en) | 2003-04-14 | 2004-10-28 | Massachusetts Institute Of Technology | Integrated thin film batteries on silicon integrated circuits |
| JP2005235686A (ja) * | 2004-02-23 | 2005-09-02 | Sony Corp | 正極および電池、並びにそれらの製造方法 |
| CN101073171B (zh) * | 2004-12-08 | 2010-09-22 | 希莫菲克斯公司 | LiCoO2的沉积 |
| US7862927B2 (en) * | 2007-03-02 | 2011-01-04 | Front Edge Technology | Thin film battery and manufacturing method |
| KR20090125256A (ko) * | 2007-03-26 | 2009-12-04 | 사임베트 코퍼레이션 | 리튬 막박 전지용 기재 |
| KR100962032B1 (ko) * | 2007-12-11 | 2010-06-08 | 지에스나노텍 주식회사 | 전극의 표면적 및 전극과 전해질의 접촉면적을 증가시킨박막형 전지 및 그의 제조방법 |
| JP5195049B2 (ja) | 2008-06-06 | 2013-05-08 | トヨタ自動車株式会社 | リチウムイオン二次電池およびその製造方法 |
| CN101814633A (zh) * | 2009-02-19 | 2010-08-25 | 邓梁 | 填注凝固法制造锂电池正极、负极及含有该正极、负极的锂电池 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| TW200808990A (en) * | 2004-12-08 | 2008-02-16 | Symmorphix Inc | Deposition of LiCoO2 |
Also Published As
| Publication number | Publication date |
|---|---|
| TW201245477A (en) | 2012-11-16 |
| CN102738516A (zh) | 2012-10-17 |
| JP2012230889A (ja) | 2012-11-22 |
| US8404001B2 (en) | 2013-03-26 |
| CN102738516B (zh) | 2016-03-30 |
| CN105679998A (zh) | 2016-06-15 |
| CN105679998B (zh) | 2019-09-10 |
| KR20120117656A (ko) | 2012-10-24 |
| JP2017069220A (ja) | 2017-04-06 |
| US20120260478A1 (en) | 2012-10-18 |
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