TWI561505B - Method of producing di(trimethylolpropane) - Google Patents

Method of producing di(trimethylolpropane)

Info

Publication number
TWI561505B
TWI561505B TW100132288A TW100132288A TWI561505B TW I561505 B TWI561505 B TW I561505B TW 100132288 A TW100132288 A TW 100132288A TW 100132288 A TW100132288 A TW 100132288A TW I561505 B TWI561505 B TW I561505B
Authority
TW
Taiwan
Prior art keywords
trimethylolpropane
producing
Prior art date
Application number
TW100132288A
Other languages
English (en)
Other versions
TW201219357A (en
Inventor
Masami Matsumoto
Hiroaki Shigeta
Nozomi Nakagawa
Ikutaro Kuzuhara
Original Assignee
Mitsubishi Gas Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Gas Chemical Co filed Critical Mitsubishi Gas Chemical Co
Publication of TW201219357A publication Critical patent/TW201219357A/zh
Application granted granted Critical
Publication of TWI561505B publication Critical patent/TWI561505B/zh

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
    • C07C29/38—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04—Saturated ethers
    • C07C43/13—Saturated ethers containing hydroxy or O-metal groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
TW100132288A 2010-09-07 2011-09-07 Method of producing di(trimethylolpropane) TWI561505B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2010200087 2010-09-07

Publications (2)

Publication Number Publication Date
TW201219357A TW201219357A (en) 2012-05-16
TWI561505B true TWI561505B (en) 2016-12-11

Family

ID=45810654

Family Applications (1)

Application Number Title Priority Date Filing Date
TW100132288A TWI561505B (en) 2010-09-07 2011-09-07 Method of producing di(trimethylolpropane)

Country Status (7)

Country Link
US (1) US9169184B2 (zh)
EP (1) EP2623489B1 (zh)
JP (1) JP5817730B2 (zh)
KR (1) KR101852214B1 (zh)
CN (1) CN103108856B (zh)
TW (1) TWI561505B (zh)
WO (1) WO2012033055A1 (zh)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102011118953B4 (de) * 2011-11-19 2014-06-05 Oxea Gmbh Destillatives Verfahren zur Gewinnung von Di-Trimethylolpropan
DE102011118993A1 (de) * 2011-11-19 2013-05-23 Oxea Gmbh Verfahren zur Gewinnung von Di-Trimethylpropan und mit Trimethylpropan angereicherten Produktströmen aus den Nebenströmen der Trimethylolpropanherstellung
DE102011118956A1 (de) * 2011-11-19 2013-05-23 Oxea Gmbh Verfahren zur Gewinnung von Di-Trimethylolpropan und mit Trimethylolpropan angereicherten Produktströmen aus den Nebenströmen der Trimethylolpropanherstellung
CN105111077B (zh) * 2015-07-23 2017-03-29 百川化工(如皋)有限公司 一种回收三羟甲基丙烷轻组分中溶剂的方法
RU2616004C1 (ru) * 2016-03-10 2017-04-12 Открытое акционерное общество "Нефтяная компания "Роснефть" Способ переработки высококипящих побочных продуктов процесса получения этриола
CN106589333B (zh) * 2016-12-19 2018-08-31 江西高信有机化工有限公司 一种基于tmp精馏重质残液为原料制备醇酸树脂的方法
CN109485554A (zh) * 2018-11-27 2019-03-19 濮阳市永安化工有限公司 从三羟甲基丙烷重组分中分离出双三羟甲基丙烷的方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1572761A (zh) * 2003-06-13 2005-02-02 三菱瓦斯化学株式会社 二（三羟甲基丙烷）的制备方法
CN1911886A (zh) * 2006-08-24 2007-02-14 王强 双三羟甲基丙烷和/或三羟甲基丙烷甲缩醛生产工艺
CN101550070A (zh) * 2008-12-30 2009-10-07 浠水县福瑞德化工有限责任公司 双三羟甲基丙烷生产工艺

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3097245A (en) 1959-01-13 1963-07-09 Trojan Powder Co Process for the preparation of trimethylolalkane
JPS4924044B1 (zh) * 1969-11-29 1974-06-20
US3829507A (en) * 1971-03-16 1974-08-13 Celanese Corp Di-trimethylolpropane
SE370388B (zh) 1972-11-23 1974-10-14 Perstorp Ab
JPH08157401A (ja) 1994-12-07 1996-06-18 Koei Chem Co Ltd トリメチロールプロパン及びジトリメチロールプロパンの製造方法
JP4003018B2 (ja) 1997-08-07 2007-11-07 三菱瓦斯化学株式会社 多価アルコールの製造法
JP2002041231A (ja) 2000-05-17 2002-02-08 Hitachi Ltd 画面入力型表示装置
EP1178030A3 (en) 2000-08-03 2002-03-27 Mitsubishi Gas Chemical Company, Inc. Process for recovering ditrimethylolpropane
JP2002047232A (ja) 2000-08-03 2002-02-12 Mitsubishi Gas Chem Co Inc ジトリメチロールプロパンの回収法
JP2002047233A (ja) * 2000-08-03 2002-02-12 Mitsubishi Gas Chem Co Inc ジトリメチロールプロパンの分離方法
JP2002047231A (ja) 2000-08-03 2002-02-12 Mitsubishi Gas Chem Co Inc ジトリメチロールプロパンの製造法
JP4687008B2 (ja) 2003-06-13 2011-05-25 三菱瓦斯化学株式会社 ジトリメチロールプロパンの製造法
JP2005049708A (ja) * 2003-07-30 2005-02-24 Kyocera Mita Corp 液体現像装置及びこれを用いた画像形成装置
US8492596B2 (en) 2007-10-30 2013-07-23 Mitsubishi Gas Chemical Company, Inc. Process for production of ditrimethylolpropane

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1572761A (zh) * 2003-06-13 2005-02-02 三菱瓦斯化学株式会社 二（三羟甲基丙烷）的制备方法
CN1911886A (zh) * 2006-08-24 2007-02-14 王强 双三羟甲基丙烷和/或三羟甲基丙烷甲缩醛生产工艺
CN101550070A (zh) * 2008-12-30 2009-10-07 浠水县福瑞德化工有限责任公司 双三羟甲基丙烷生产工艺

Also Published As

Publication number Publication date
KR20130109107A (ko) 2013-10-07
EP2623489A1 (en) 2013-08-07
WO2012033055A1 (ja) 2012-03-15
JPWO2012033055A1 (ja) 2014-01-20
EP2623489A4 (en) 2015-05-06
CN103108856B (zh) 2015-01-21
KR101852214B1 (ko) 2018-04-25
EP2623489B1 (en) 2016-05-25
CN103108856A (zh) 2013-05-15
US20130184497A1 (en) 2013-07-18
TW201219357A (en) 2012-05-16
US9169184B2 (en) 2015-10-27
JP5817730B2 (ja) 2015-11-18

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Legal Events

Date Code Title Description
MM4A Annulment or lapse of patent due to non-payment of fees