TWI483779B - 處理離子交換樹脂之方法 - Google Patents

處理離子交換樹脂之方法 Download PDF

Info

Publication number
TWI483779B
TWI483779B TW099109235A TW99109235A TWI483779B TW I483779 B TWI483779 B TW I483779B TW 099109235 A TW099109235 A TW 099109235A TW 99109235 A TW99109235 A TW 99109235A TW I483779 B TWI483779 B TW I483779B
Authority
TW
Taiwan
Prior art keywords
ion exchange
ester
exchange resin
acid
acidic ion
Prior art date
Application number
TW099109235A
Other languages
English (en)
Chinese (zh)
Other versions
TW201039918A (en
Inventor
Trevor Huw Morris
Original Assignee
Lucite Int Uk Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lucite Int Uk Ltd filed Critical Lucite Int Uk Ltd
Publication of TW201039918A publication Critical patent/TW201039918A/zh
Application granted granted Critical
Publication of TWI483779B publication Critical patent/TWI483779B/zh

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/60—Cleaning or rinsing ion-exchange beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B01J38/60—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using acids
    • B01J38/62—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using acids organic
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B01J49/53—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for cationic exchangers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/353—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by isomerisation; by change of size of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/333—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton
    • C07C67/343—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/58—Esters of straight chain acids with eighteen carbon atoms in the acid moiety
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Treatments Of Macromolecular Shaped Articles (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)
  • Catalysts (AREA)
TW099109235A 2009-03-27 2010-03-26 處理離子交換樹脂之方法 TWI483779B (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB0905257.2A GB0905257D0 (en) 2009-03-27 2009-03-27 Process for the treatment of an ion exchange resin

Publications (2)

Publication Number Publication Date
TW201039918A TW201039918A (en) 2010-11-16
TWI483779B true TWI483779B (zh) 2015-05-11

Family

ID=40671801

Family Applications (1)

Application Number Title Priority Date Filing Date
TW099109235A TWI483779B (zh) 2009-03-27 2010-03-26 處理離子交換樹脂之方法

Country Status (17)

Country Link
US (2) US8835518B2 (enExample)
EP (4) EP4049754B1 (enExample)
JP (1) JP5882193B2 (enExample)
KR (1) KR101719617B1 (enExample)
CN (1) CN102361695B (enExample)
AU (1) AU2010227277B2 (enExample)
BR (1) BRPI1009092B1 (enExample)
CA (1) CA2752790C (enExample)
ES (3) ES2980797T3 (enExample)
GB (1) GB0905257D0 (enExample)
MX (1) MX2011009543A (enExample)
MY (2) MY197873A (enExample)
NZ (1) NZ594983A (enExample)
RU (1) RU2531304C2 (enExample)
SG (2) SG2014011522A (enExample)
TW (1) TWI483779B (enExample)
WO (1) WO2010109244A2 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0905257D0 (en) * 2009-03-27 2009-05-13 Lucite Int Uk Ltd Process for the treatment of an ion exchange resin
JP6074902B2 (ja) * 2012-03-28 2017-02-08 三菱化学株式会社 精製フェノール系化合物の製造方法
CN104744212B (zh) * 2013-12-31 2018-01-16 上海星可高纯溶剂有限公司 梯度洗脱溶剂甲醇的提纯方法
JP6248742B2 (ja) * 2014-02-21 2017-12-20 三菱ケミカル株式会社 (メタ)アクリル酸エステルの精製方法及び(メタ)アクリル酸エステル重合体の製造方法
WO2017027953A1 (en) * 2015-08-20 2017-02-23 Eco-Tec Ltd. Process for stripping carbamate from ion exchange resin
CN106673962B (zh) * 2015-11-09 2019-11-15 中国石油化工股份有限公司 一种异丙醇的制备方法
US10967367B2 (en) * 2017-02-10 2021-04-06 Ddp Specialty Electronic Materials Us, Llc Method of cleaning resins
CN109967136A (zh) * 2019-03-08 2019-07-05 中核通辽铀业有限责任公司 一种固定床树脂清洗解毒一体化方法
JP7272512B2 (ja) * 2021-05-20 2023-05-12 三菱ケミカル株式会社 単量体組成物、メタクリル系樹脂組成物及び樹脂成形体
CN116440882B (zh) * 2023-01-16 2024-09-20 浙江纽龙合成材料制造有限公司 一种基于端烯基活化的疏水分离层析介质及其制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3146258A (en) * 1961-12-29 1964-08-25 Monsanto Co Purification of acrylonitrile
JP2007014871A (ja) * 2005-07-07 2007-01-25 Tohoku Univ イオン交換樹脂の再生方法
CN101311158A (zh) * 2007-05-25 2008-11-26 罗姆有限公司 使用再循环的甲醇制备甲基丙烯酸甲酯的方法

Family Cites Families (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE549516A (enExample) 1955-07-19
BE590370A (enExample) 1959-04-29 1900-01-01
US4237303A (en) * 1979-04-30 1980-12-02 The Dow Chemical Company Removal of oxazole from acrylonitrile
JPS57187042A (en) * 1981-05-15 1982-11-17 Nippon Petrochem Co Ltd Regeneration method for ion exchange resin
JPS58183641A (ja) 1982-04-19 1983-10-26 Asahi Chem Ind Co Ltd (メタ)アクリル酸メチルの精製法
US4447641A (en) * 1982-07-26 1984-05-08 Standard Oil Company (Indiana) Process for preparation of alpha, beta-unsaturated esters using AMS-1B borosilicate crystalline molecular sieve
US4581471A (en) * 1983-04-12 1986-04-08 The British Petroleum Company P.L.C. Process for the production of unsaturated carboxylic acids and/or esters
JPS606635A (ja) * 1983-06-24 1985-01-14 Mitsubishi Petrochem Co Ltd 1,2−不飽和カルボン酸および/またはそのエステルの精製法
DE3501761A1 (de) * 1985-01-21 1986-07-24 Henkel KGaA, 4000 Düsseldorf Verfahren zur vorveresterung freier fettsaeuren in rohfetten und/oder -oelen
JPS6242748A (ja) * 1985-08-14 1987-02-24 Mitsui Toatsu Chem Inc イオン交換樹脂の再生方法
US4733004A (en) 1986-06-23 1988-03-22 Ashland Oil, Inc. Continuous esterification of methacrylic acid and product recovery
JPH0722714B2 (ja) * 1986-10-27 1995-03-15 三井東圧化学株式会社 イオン交換樹脂の再生方法
JPS63127952A (ja) 1986-11-14 1988-05-31 Fujitsu Ltd 媒体搬送機構
JPH0764787B2 (ja) * 1987-04-16 1995-07-12 株式会社日本触媒 高純度メタクリル酸エステルの製造方法
CA1308737C (en) 1987-04-16 1992-10-13 Syoichi Matsumoto Process for producing methacrylic ester
US4970344A (en) * 1987-07-02 1990-11-13 Conoco Inc. Reactivation of spent alkanolamine
JP2640495B2 (ja) * 1988-05-25 1997-08-13 三菱レイヨン株式会社 メタクリル酸メチルの精製法
US5043518A (en) 1989-07-31 1991-08-27 Exxon Chemical Patents Inc. Process for regenerating a catalyst and resultant regenerated catalyst and production of olefins by catalytic ether decomposition using regenerated catalyst
US5006258A (en) * 1989-10-26 1991-04-09 Conoco Inc. Regeneration of acidic cationic exchange resin used in the reactivation of spent alkanolamine
JPH1072379A (ja) * 1996-08-30 1998-03-17 Mitsubishi Rayon Co Ltd イソブチレンおよびメタクリル酸エステルの製造方法
GB9807498D0 (en) * 1998-04-08 1998-06-10 Ici Plc Production of unsaturated acids therfore and catalysts therfor
JP3792449B2 (ja) 1999-09-01 2006-07-05 三菱レイヨン株式会社 メタクリル酸の精製法
JP4416889B2 (ja) * 1999-12-15 2010-02-17 株式会社日本触媒 固体触媒の廃棄方法
RU2300515C2 (ru) * 2001-12-04 2007-06-10 Мицубиси Кемикал Корпорейшн Способ получения (мет)акриловых кислот каталитическим окислением пропилена или изобутилена (варианты), способ разложения побочного продукта (варианты), установка для осуществления способа
JP2003277317A (ja) * 2002-01-15 2003-10-02 Mitsubishi Chemicals Corp 高純度(メタ)アクリル酸の製造方法
JP2003261504A (ja) * 2002-03-06 2003-09-19 Mitsubishi Rayon Co Ltd (メタ)アクリル酸エステルの製造方法
US20040006244A1 (en) * 2002-05-22 2004-01-08 Manzer Leo Ernest Process for making ethyencially unsaturated acids and acids
JP2005179483A (ja) * 2003-12-18 2005-07-07 Mitsubishi Chemicals Corp Thf重合触媒の再生方法
WO2007088702A1 (ja) * 2006-01-31 2007-08-09 Revo International Inc. 脂肪酸アルキルエステルの製造方法および脂肪酸アルキルエステルの製造装置
WO2008078769A1 (ja) * 2006-12-27 2008-07-03 Lion Corporation 脂肪酸低級アルキルエステルの製造方法
DE102007023197A1 (de) 2007-05-22 2008-11-27 Bayer Materialscience Ag Polyester-Prepolymere
US8907121B2 (en) * 2008-12-18 2014-12-09 Lucite International Uk Limited Methyl methacrylate purification process
GB0905257D0 (en) * 2009-03-27 2009-05-13 Lucite Int Uk Ltd Process for the treatment of an ion exchange resin

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3146258A (en) * 1961-12-29 1964-08-25 Monsanto Co Purification of acrylonitrile
JP2007014871A (ja) * 2005-07-07 2007-01-25 Tohoku Univ イオン交換樹脂の再生方法
CN101311158A (zh) * 2007-05-25 2008-11-26 罗姆有限公司 使用再循环的甲醇制备甲基丙烯酸甲酯的方法

Also Published As

Publication number Publication date
EP4049754C0 (en) 2024-04-03
NZ594983A (en) 2014-03-28
BRPI1009092A2 (pt) 2016-03-01
JP5882193B2 (ja) 2016-03-09
EP4219008A1 (en) 2023-08-02
RU2531304C2 (ru) 2014-10-20
US9821304B2 (en) 2017-11-21
EP2411147A2 (en) 2012-02-01
EP4219008B1 (en) 2024-11-20
SG173817A1 (en) 2011-09-29
US20140343176A1 (en) 2014-11-20
US8835518B2 (en) 2014-09-16
JP2012521867A (ja) 2012-09-20
WO2010109244A2 (en) 2010-09-30
EP3862085C0 (en) 2023-06-07
EP3862085B1 (en) 2023-06-07
WO2010109244A3 (en) 2011-01-13
EP2411147B1 (en) 2022-04-20
ES2980797T3 (es) 2024-10-03
MX2011009543A (es) 2011-09-28
CA2752790C (en) 2018-05-15
RU2011143366A (ru) 2013-05-10
BRPI1009092B1 (pt) 2019-01-02
ES2922635T3 (es) 2022-09-19
ES2951977T3 (es) 2023-10-26
KR101719617B1 (ko) 2017-04-04
EP4049754A1 (en) 2022-08-31
EP3862085A1 (en) 2021-08-11
CN102361695B (zh) 2016-10-26
SG2014011522A (en) 2014-06-27
CA2752790A1 (en) 2010-09-30
MY197873A (en) 2023-07-21
KR20110133620A (ko) 2011-12-13
TW201039918A (en) 2010-11-16
GB0905257D0 (en) 2009-05-13
AU2010227277A1 (en) 2011-09-22
EP4049754B1 (en) 2024-04-03
EP4219008C0 (en) 2024-11-20
US20120059073A1 (en) 2012-03-08
AU2010227277B2 (en) 2014-09-18
CN102361695A (zh) 2012-02-22
MY173714A (en) 2020-02-18

Similar Documents

Publication Publication Date Title
US9821304B2 (en) Process for the treatment of an ion exchange resin
US8907121B2 (en) Methyl methacrylate purification process
JP6824253B2 (ja) メタクロレインをベースとするアルキルメタクリレートからのメタクリル酸の合成
JP2012521867A5 (enExample)
JP6036402B2 (ja) (メタ)アクリル酸エステルの製造方法
CN106458831A (zh) 用于制造低voc聚结助剂的方法
JPS58183641A (ja) (メタ)アクリル酸メチルの精製法
JP2007516942A (ja) アクリロニトリル生成物流からアクロレインを除去する方法
JP5389011B2 (ja) トリメチロールプロパンの色数の改善方法
JP7750140B2 (ja) (メタ)アクリル酸エステルの製造方法
CN117700449A (zh) 一种4-(羟基甲基膦酰基)-2-羰基丁酸的制备方法