TWI320789B - Improvement in the storage stability of photoinitiators - Google Patents

Improvement in the storage stability of photoinitiators Download PDF

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Publication number
TWI320789B
TWI320789B TW092129799A TW92129799A TWI320789B TW I320789 B TWI320789 B TW I320789B TW 092129799 A TW092129799 A TW 092129799A TW 92129799 A TW92129799 A TW 92129799A TW I320789 B TWI320789 B TW I320789B
Authority
TW
Taiwan
Prior art keywords
compound
formula
composition
coating
photoinitiator
Prior art date
Application number
TW092129799A
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English (en)
Chinese (zh)
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TW200406425A (en
Inventor
Thomas Ulrich
Thomas Bolle
Kurt Dietliker
Jean-Pierre Wolf
Andre Fuchs
Original Assignee
Ciba Sc Holding Ag
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Publication date
Application filed by Ciba Sc Holding Ag filed Critical Ciba Sc Holding Ag
Publication of TW200406425A publication Critical patent/TW200406425A/zh
Application granted granted Critical
Publication of TWI320789B publication Critical patent/TWI320789B/zh

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/08—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms
    • C07D295/096—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms separated by carbocyclic rings or by carbon chains interrupted by carbocyclic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/10—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/10—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms
    • C07D295/112—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by doubly bound oxygen or sulphur atoms with the ring nitrogen atoms and the doubly bound oxygen or sulfur atoms separated by carbocyclic rings or by carbon chains interrupted by carbocyclic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/46—Polymerisation initiated by wave energy or particle radiation
    • C08F2/48—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
    • C08F2/50—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light with sensitising agents
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/101—Inks specially adapted for printing processes involving curing by wave energy or particle radiation, e.g. with UV-curing following the printing
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/0037—Production of three-dimensional images
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/004—Photosensitive materials
    • G03F7/027—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds
    • G03F7/028—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds with photosensitivity-increasing substances, e.g. photoinitiators
    • G03F7/031—Organic compounds not covered by group G03F7/029
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/0005—Production of optical devices or components in so far as characterised by the lithographic processes or materials used therefor
    • G03F7/0007—Filters, e.g. additive colour filters; Components for display devices
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/0005—Production of optical devices or components in so far as characterised by the lithographic processes or materials used therefor
    • G03F7/001—Phase modulating patterns, e.g. refractive index patterns

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polymerisation Methods In General (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Holo Graphy (AREA)
  • Paints Or Removers (AREA)
  • Ink Jet Recording Methods And Recording Media Thereof (AREA)
  • Measuring Pulse, Heart Rate, Blood Pressure Or Blood Flow (AREA)
TW092129799A 2002-10-28 2003-10-27 Improvement in the storage stability of photoinitiators TWI320789B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH18002002 2002-10-28

Publications (2)

Publication Number Publication Date
TW200406425A TW200406425A (en) 2004-05-01
TWI320789B true TWI320789B (en) 2010-02-21

Family

ID=32111465

Family Applications (1)

Application Number Title Priority Date Filing Date
TW092129799A TWI320789B (en) 2002-10-28 2003-10-27 Improvement in the storage stability of photoinitiators

Country Status (16)

Country Link
US (1) US7291654B2 (enExample)
EP (1) EP1556365B1 (enExample)
JP (1) JP4575777B2 (enExample)
KR (1) KR101059703B1 (enExample)
CN (1) CN100430385C (enExample)
AT (1) ATE338034T1 (enExample)
AU (1) AU2003283441A1 (enExample)
BR (1) BR0315786A (enExample)
CA (1) CA2501438A1 (enExample)
DE (1) DE60308052T2 (enExample)
MX (1) MXPA05004015A (enExample)
NZ (1) NZ539621A (enExample)
RU (1) RU2005116302A (enExample)
TW (1) TWI320789B (enExample)
WO (1) WO2004037799A1 (enExample)
ZA (1) ZA200502642B (enExample)

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US20050176841A1 (en) * 2003-12-30 2005-08-11 Krohn Roy C. UV curable ink compositions
JP4380359B2 (ja) * 2004-02-20 2009-12-09 Jsr株式会社 スペーサー形成用感放射線性樹脂組成物、スペーサーとその形成方法および液晶表示素子
US20080160209A1 (en) * 2004-12-07 2008-07-03 Toshiyuki Takabayashi Actinic Radiation Curable Magenta Ink Composition, Actinic Radiation Curable Ink, Jet Recording Magenta Ink and Method for Image Formation and Ink Jet Recording Apparatus Using Said Ink, and Actinic Radiation Curable Printing Magenta Ink
US7459014B2 (en) 2005-01-14 2008-12-02 Xerox Corporation Radiation curable inks containing curable gelator additives
US20060199028A1 (en) * 2005-03-02 2006-09-07 Dimitry Chernyshov Process for coating
US7806050B2 (en) 2006-02-06 2010-10-05 Fujifilm Corporation Ink composition, inkjet recording method, method of producing planographic printing plate, and planographic printing plate
JP4952045B2 (ja) 2006-04-28 2012-06-13 Jsr株式会社 エネルギー線硬化型インクジェット印刷用インク
EP2041217A2 (en) * 2006-07-17 2009-04-01 Ciba Holding Inc. Method of bonding
US20090298962A1 (en) * 2006-09-29 2009-12-03 Katia Studer Photolatent bases for systems based on blocked isocyanates
KR100920603B1 (ko) * 2006-12-28 2009-10-08 제일모직주식회사 감광성 수지 조성물 및 그로부터 제조되는 컬러필터
KR100881860B1 (ko) * 2007-01-17 2009-02-06 제일모직주식회사 컬러필터용 감광성 수지 조성물 및 이를 이용한 이미지센서컬러필터
US8129447B2 (en) † 2007-09-28 2012-03-06 Fujifilm Corporation Ink composition and inkjet recording method using the same
US8486591B2 (en) * 2008-10-24 2013-07-16 Cheil Industries Inc. Photosensitive resin composition for color filter and color filter prepared using the same
IT1398626B1 (it) * 2009-03-30 2013-03-08 Carbontech S R L Materiale composito e/o multistrato con lettere, numeri, parole, immagini sulla superficie e relativo procedimento per la visualizzazione di esse.
WO2010128969A1 (en) * 2009-05-08 2010-11-11 Hewlett-Packard Development Company, L.P. Functionalized perfluoropolyether material as a hydrophobic coating
JP2010275392A (ja) * 2009-05-27 2010-12-09 Mitsubishi Rayon Co Ltd 重合性混合物、それから得られる樹脂成形体及びその製造方法
JP5812613B2 (ja) * 2010-03-09 2015-11-17 キヤノン株式会社 光音響整合材及び人体組織模擬材料
CN102206394B (zh) * 2010-03-31 2014-02-12 罗门哈斯公司 含水共聚物分散液和涂料组合物
JP5809780B2 (ja) * 2010-04-02 2015-11-11 Dicグラフィックス株式会社 紫外線硬化性コーティングニス
EP2556124A1 (de) * 2010-04-09 2013-02-13 Basf Se Druckfarbe, enthaltend einen divinylester
US9373923B2 (en) 2011-11-22 2016-06-21 Savannah River Nuclear Solutions, Llc Rapid prototype extruded conductive pathways
KR20140083620A (ko) 2012-12-26 2014-07-04 제일모직주식회사 차광층용 감광성 수지 조성물 및 이를 이용한 차광층
CN103191739B (zh) * 2013-04-25 2015-07-29 上海师范大学 一种高产氢活性的金红石负载超长铜纳米线光催化剂及其制备方法和应用
JP2015002978A (ja) * 2013-05-23 2015-01-08 キヤノン株式会社 光音響用血液モデル
JP6388776B2 (ja) * 2014-03-12 2018-09-12 新日鉄住金化学株式会社 白色感光性樹脂組成物、それを用いた硬化物、及びその硬化物を構成成分として含むタッチパネル
US9482788B2 (en) 2014-12-05 2016-11-01 Pegavision Corporation UV-blocking silicone hydrogel composition and silicone hydrogel contact lens containing thereof
US10709530B2 (en) 2015-02-03 2020-07-14 Mitsui Chemicals, Inc. Photocurable composition, denture base, and plate denture
US9988539B2 (en) * 2015-11-12 2018-06-05 Ricoh Company, Ltd. Active-energy-ray-curable composition, active-energy-ray-curable ink, composition stored container, two-dimensional or three-dimensional image forming apparatus, two-dimensional or three-dimensional image forming method, cured material, and structure
EP3686252A1 (en) * 2019-01-24 2020-07-29 Agfa-Gevaert Nv Radiation curable inkjet ink for manufacturing printed circuit boards
CN110698433A (zh) * 2019-11-25 2020-01-17 怀化市恒渝新材料有限公司 一种光引发剂的纯化方法和设备
CN119916644B (zh) * 2025-04-02 2025-07-01 湖南初源新材料股份有限公司 包含炔基蒽光敏剂的感光树脂组合物及其应用

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DE3738567A1 (de) * 1987-03-12 1988-09-22 Merck Patent Gmbh Coreaktive fotoinitiatoren
DE3880868D1 (en) * 1987-03-26 1993-06-17 Ciba Geigy Ag Neue alpha-aminoacetophenone als photoinitiatoren.
US5795985A (en) 1996-03-05 1998-08-18 Ciba Specialty Chemicals Corporation Phenyl alkyl ketone substituted by cyclic amine and a process for the preparation thereof
US6620857B2 (en) * 1996-07-02 2003-09-16 Ciba Specialty Chemicals Corporation Process for curing a polymerizable composition
ES2194362T3 (es) * 1997-09-17 2003-11-16 Ciba Sc Holding Ag Morfolinonas en calidad de estabilizadores a la luz.
US6416307B1 (en) * 1998-09-25 2002-07-09 Q2100, Inc. Plastic lens systems, compositions, and methods
JP4164919B2 (ja) * 1998-11-30 2008-10-15 チッソ株式会社 光重合開始剤および光重合性開始剤組成物
CN1187388C (zh) * 2000-05-26 2005-02-02 阿克佐诺贝尔股份有限公司 光敏涂料组合物
EP1369459A4 (en) * 2001-02-19 2008-05-21 Jsr Corp RADIATION-SENSITIVE COMPOSITION WHICH MAY HAVE A DISTRIBUTION OF THE REFRACTIVE INDEX
EP1620500B1 (en) * 2003-05-06 2012-07-11 Basf Se Photo-cured and stabilized coatings

Also Published As

Publication number Publication date
ZA200502642B (en) 2006-07-26
DE60308052T2 (de) 2007-04-05
DE60308052D1 (de) 2006-10-12
NZ539621A (en) 2006-03-31
CA2501438A1 (en) 2004-05-06
MXPA05004015A (es) 2005-06-08
JP4575777B2 (ja) 2010-11-04
WO2004037799A1 (en) 2004-05-06
KR101059703B1 (ko) 2011-08-29
AU2003283441A1 (en) 2004-05-13
US7291654B2 (en) 2007-11-06
CN100430385C (zh) 2008-11-05
EP1556365B1 (en) 2006-08-30
ATE338034T1 (de) 2006-09-15
TW200406425A (en) 2004-05-01
JP2006515833A (ja) 2006-06-08
US20060100298A1 (en) 2006-05-11
EP1556365A1 (en) 2005-07-27
RU2005116302A (ru) 2006-01-20
BR0315786A (pt) 2005-09-13
KR20050065637A (ko) 2005-06-29
CN1708488A (zh) 2005-12-14

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