TWI271392B - Sag control of isopipes used in making sheet glass by the fusion process - Google Patents
Sag control of isopipes used in making sheet glass by the fusion process Download PDFInfo
- Publication number
- TWI271392B TWI271392B TW091102637A TW91102637A TWI271392B TW I271392 B TWI271392 B TW I271392B TW 091102637 A TW091102637 A TW 091102637A TW 91102637 A TW91102637 A TW 91102637A TW I271392 B TWI271392 B TW I271392B
- Authority
- TW
- Taiwan
- Prior art keywords
- creep rate
- less
- mcr
- weight
- average
- Prior art date
Links
- 238000007499 fusion processing Methods 0.000 title claims abstract description 22
- 239000005357 flat glass Substances 0.000 title claims abstract description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 48
- 239000011819 refractory material Substances 0.000 claims abstract description 31
- 239000000463 material Substances 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 24
- 239000011521 glass Substances 0.000 claims description 20
- 238000004519 manufacturing process Methods 0.000 claims description 14
- 238000004088 simulation Methods 0.000 claims description 14
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims description 7
- 229910052707 ruthenium Inorganic materials 0.000 claims description 7
- 239000010936 titanium Substances 0.000 claims description 7
- 239000004408 titanium dioxide Substances 0.000 claims description 6
- 230000004927 fusion Effects 0.000 claims description 5
- 238000010586 diagram Methods 0.000 claims description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 2
- 239000000835 fiber Substances 0.000 claims 2
- 239000000126 substance Substances 0.000 claims 2
- 229910052719 titanium Inorganic materials 0.000 claims 2
- 241000219171 Malpighiales Species 0.000 claims 1
- 206010036790 Productive cough Diseases 0.000 claims 1
- 210000003802 sputum Anatomy 0.000 claims 1
- 208000024794 sputum Diseases 0.000 claims 1
- ZMBQPOYXVWCOIG-UHFFFAOYSA-N sulfonylzirconium Chemical compound O=S(=O)=[Zr] ZMBQPOYXVWCOIG-UHFFFAOYSA-N 0.000 claims 1
- 229910052845 zircon Inorganic materials 0.000 abstract description 6
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 abstract description 6
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 6
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 6
- 229910052726 zirconium Inorganic materials 0.000 description 6
- 238000007665 sagging Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 239000002803 fossil fuel Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 239000011449 brick Substances 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000006060 molten glass Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 229910052715 tantalum Inorganic materials 0.000 description 2
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 2
- KVGZZAHHUNAVKZ-UHFFFAOYSA-N 1,4-Dioxin Chemical group O1C=COC=C1 KVGZZAHHUNAVKZ-UHFFFAOYSA-N 0.000 description 1
- TUSDEZXZIZRFGC-UHFFFAOYSA-N 1-O-galloyl-3,6-(R)-HHDP-beta-D-glucose Natural products OC1C(O2)COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC1C(O)C2OC(=O)C1=CC(O)=C(O)C(O)=C1 TUSDEZXZIZRFGC-UHFFFAOYSA-N 0.000 description 1
- 241000272525 Anas platyrhynchos Species 0.000 description 1
- 229910052684 Cerium Inorganic materials 0.000 description 1
- 239000001263 FEMA 3042 Substances 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 241000282376 Panthera tigris Species 0.000 description 1
- LRBQNJMCXXYXIU-PPKXGCFTSA-N Penta-digallate-beta-D-glucose Natural products OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-PPKXGCFTSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 1
- ZTHQBROSBNNGPU-UHFFFAOYSA-M butyl sulfate(1-) Chemical compound CCCCOS([O-])(=O)=O ZTHQBROSBNNGPU-UHFFFAOYSA-M 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012761 high-performance material Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000000462 isostatic pressing Methods 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000000611 regression analysis Methods 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
- LRBQNJMCXXYXIU-NRMVVENXSA-N tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 1
- 229940033123 tannic acid Drugs 0.000 description 1
- 235000015523 tannic acid Nutrition 0.000 description 1
- 229920002258 tannic acid Polymers 0.000 description 1
- 238000004876 x-ray fluorescence Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B17/00—Forming molten glass by flowing-out, pushing-out, extruding or drawing downwardly or laterally from forming slits or by overflowing over lips
- C03B17/06—Forming glass sheets
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/48—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
- C04B35/481—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates containing silicon, e.g. zircon
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B17/00—Forming molten glass by flowing-out, pushing-out, extruding or drawing downwardly or laterally from forming slits or by overflowing over lips
- C03B17/06—Forming glass sheets
- C03B17/064—Forming glass sheets by the overflow downdraw fusion process; Isopipes therefor
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3232—Titanium oxides or titanates, e.g. rutile or anatase
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3244—Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3409—Boron oxide, borates, boric acids, or oxide forming salts thereof, e.g. borax
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Composite Materials (AREA)
- Manufacturing & Machinery (AREA)
- Structural Engineering (AREA)
- Compositions Of Oxide Ceramics (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US25092100P | 2000-12-01 | 2000-12-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TWI271392B true TWI271392B (en) | 2007-01-21 |
Family
ID=22949717
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW091102637A TWI271392B (en) | 2000-12-01 | 2002-02-05 | Sag control of isopipes used in making sheet glass by the fusion process |
Country Status (9)
| Country | Link |
|---|---|
| US (3) | US6974786B2 (OSRAM) |
| EP (2) | EP2181975B1 (OSRAM) |
| JP (2) | JP4471190B2 (OSRAM) |
| KR (1) | KR100586110B1 (OSRAM) |
| CN (3) | CN1486286B (OSRAM) |
| AU (1) | AU2002230542A1 (OSRAM) |
| DE (1) | DE60135872D1 (OSRAM) |
| TW (1) | TWI271392B (OSRAM) |
| WO (1) | WO2002044102A1 (OSRAM) |
Families Citing this family (66)
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|---|---|---|---|---|
| CN1486286B (zh) * | 2000-12-01 | 2013-02-20 | 康宁股份有限公司 | 熔融法生产平板玻璃所用的等静压板的下沉控制 |
| US7541304B2 (en) * | 2001-11-30 | 2009-06-02 | Corning Incorporated | Sag control of isopipes used in making sheet glass by the fusion process |
| US7681414B2 (en) * | 2001-08-08 | 2010-03-23 | Corning Incorporated | Overflow downdraw glass forming method and apparatus |
| US9233869B2 (en) | 2001-08-08 | 2016-01-12 | Corning Incorporated | Overflow downdraw glass forming method and apparatus |
| CN100534938C (zh) * | 2001-08-08 | 2009-09-02 | 布鲁斯科技公司 | 玻璃板成形装置 |
| JP4511187B2 (ja) * | 2001-12-21 | 2010-07-28 | コーニング インコーポレイテッド | オーバーフロー式ダウンドロー融着プロセスによる板ガラスを作成するためのプロセス |
| US6895782B2 (en) * | 2002-08-08 | 2005-05-24 | Richard B. Pitbladdo | Overflow downdrawn glass forming method and apparatus |
| JP4281107B2 (ja) * | 2003-04-16 | 2009-06-17 | 日本電気硝子株式会社 | 板ガラスの成形装置 |
| US7238635B2 (en) * | 2003-12-16 | 2007-07-03 | Corning Incorporated | Creep resistant zircon refractory material used in a glass manufacturing system |
| US7690221B2 (en) * | 2004-02-23 | 2010-04-06 | Corning Incorporated | Sheet width control for overflow downdraw sheet glass forming apparatus |
| US8042361B2 (en) * | 2004-07-20 | 2011-10-25 | Corning Incorporated | Overflow downdraw glass forming method and apparatus |
| KR101232591B1 (ko) | 2004-12-30 | 2013-02-12 | 코닝 인코포레이티드 | 내화성 물질 |
| WO2006091389A2 (en) * | 2005-02-24 | 2006-08-31 | Corning Incorporated | Apparatus and method for making a glass sheet |
| TWI317352B (en) | 2005-02-24 | 2009-11-21 | Corning Inc | Apparatua and method for making a glass sheet |
| US20060236722A1 (en) * | 2005-04-26 | 2006-10-26 | Robert Delia | Forming apparatus with extensions attached thereto used in a glass manufacturing system |
| US7409839B2 (en) * | 2005-04-29 | 2008-08-12 | Corning Incorporated | Method and apparatus for making a glass sheet |
| US7748236B2 (en) * | 2005-12-27 | 2010-07-06 | Corning Incorporated | Overflow downdraw glass forming method and apparatus |
| KR101451997B1 (ko) * | 2006-06-05 | 2014-10-21 | 코닝 인코포레이티드 | 제노타임 결정 구조를 갖는 단일상 이트륨 포스페이트 및 이의 제조방법 |
| FR2907116B1 (fr) | 2006-10-16 | 2008-12-19 | Saint Gobain Ct Recherches | Produit fritte a base de zircon+nb2o5 ou ta2o5 |
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| US8986597B2 (en) | 2007-10-31 | 2015-03-24 | Corning Incorporated | Low creep refractory ceramic and method of making |
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| FR2929941B1 (fr) | 2008-04-15 | 2011-03-04 | Saint Gobain Ct Recherches | Produit fritte dope a base de zircon |
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| US8028544B2 (en) * | 2009-02-24 | 2011-10-04 | Corning Incorporated | High delivery temperature isopipe materials |
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| JP5366088B2 (ja) * | 2009-09-16 | 2013-12-11 | セイコーインスツル株式会社 | サーマルヘッドおよびプリンタ |
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| JP5797294B2 (ja) * | 2013-03-29 | 2015-10-21 | AvanStrate株式会社 | ガラス板の製造方法 |
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| KR102347707B1 (ko) | 2016-04-07 | 2022-01-06 | 코닝 인코포레이티드 | 연속적인 유리 리본을 성형하기 위한 성형체 및 이를 포함하는 유리 성형 장치 |
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| US3181958A (en) * | 1961-10-20 | 1965-05-04 | Taylors Sons Co Chas | Refractory composition |
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| US3285757A (en) | 1964-05-19 | 1966-11-15 | American Thermocatalytic Corp | Cement composition |
| US3357124A (en) * | 1965-04-26 | 1967-12-12 | David I Stepacoff | Fishing lure |
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| JPS5027850A (OSRAM) | 1973-07-11 | 1975-03-22 | ||
| FR2648455B1 (fr) * | 1989-06-15 | 1993-04-23 | Produits Refractaires | Produits refractaires fondus et coules a forte teneur en zircone |
| EP0447509B1 (en) | 1989-09-08 | 1998-01-07 | Corhart Refractories Corporation | Zircon refractories with improved thermal shock resistance |
| US5116789A (en) * | 1991-08-12 | 1992-05-26 | Corning Incorporated | Strontium aluminosilicate glasses for flat panel displays |
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| US7238635B2 (en) * | 2003-12-16 | 2007-07-03 | Corning Incorporated | Creep resistant zircon refractory material used in a glass manufacturing system |
-
2001
- 2001-11-30 CN CN018217885A patent/CN1486286B/zh not_active Expired - Lifetime
- 2001-11-30 WO PCT/US2001/045300 patent/WO2002044102A1/en not_active Ceased
- 2001-11-30 EP EP08164339A patent/EP2181975B1/en not_active Expired - Lifetime
- 2001-11-30 EP EP01990780A patent/EP1345867B1/en not_active Expired - Lifetime
- 2001-11-30 CN CN2009101594561A patent/CN101798231B/zh not_active Expired - Lifetime
- 2001-11-30 AU AU2002230542A patent/AU2002230542A1/en not_active Abandoned
- 2001-11-30 JP JP2002546050A patent/JP4471190B2/ja not_active Expired - Lifetime
- 2001-11-30 KR KR1020037007314A patent/KR100586110B1/ko not_active Expired - Lifetime
- 2001-11-30 DE DE60135872T patent/DE60135872D1/de not_active Expired - Lifetime
- 2001-11-30 CN CN201310011686XA patent/CN102992592A/zh active Pending
-
2002
- 2002-02-05 TW TW091102637A patent/TWI271392B/zh not_active IP Right Cessation
-
2003
- 2003-05-29 US US10/449,701 patent/US6974786B2/en not_active Expired - Lifetime
-
2005
- 2005-12-05 US US11/294,315 patent/US7259119B2/en not_active Expired - Lifetime
-
2007
- 2007-02-12 US US11/705,314 patent/US7414001B2/en not_active Expired - Lifetime
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- 2009-12-24 JP JP2009292005A patent/JP5319513B2/ja not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| CN101798231B (zh) | 2013-10-16 |
| JP5319513B2 (ja) | 2013-10-16 |
| EP1345867A4 (en) | 2006-08-30 |
| US20070142207A1 (en) | 2007-06-21 |
| JP2010111577A (ja) | 2010-05-20 |
| AU2002230542A1 (en) | 2002-06-11 |
| CN1486286B (zh) | 2013-02-20 |
| EP1345867B1 (en) | 2008-09-17 |
| CN101798231A (zh) | 2010-08-11 |
| US7259119B2 (en) | 2007-08-21 |
| US20040055338A1 (en) | 2004-03-25 |
| US6974786B2 (en) | 2005-12-13 |
| KR100586110B1 (ko) | 2006-06-07 |
| WO2002044102A1 (en) | 2002-06-06 |
| KR20040016825A (ko) | 2004-02-25 |
| CN102992592A (zh) | 2013-03-27 |
| EP1345867A1 (en) | 2003-09-24 |
| EP2181975A1 (en) | 2010-05-05 |
| EP2181975B1 (en) | 2012-07-11 |
| US7414001B2 (en) | 2008-08-19 |
| JP4471190B2 (ja) | 2010-06-02 |
| JP2004523448A (ja) | 2004-08-05 |
| DE60135872D1 (de) | 2008-10-30 |
| CN1486286A (zh) | 2004-03-31 |
| US20060094585A1 (en) | 2006-05-04 |
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