SU618047A3 - Способ получени окисей карбоксиалкилфосфинов - Google Patents
Способ получени окисей карбоксиалкилфосфиновInfo
- Publication number
- SU618047A3 SU618047A3 SU762391504A SU2391504A SU618047A3 SU 618047 A3 SU618047 A3 SU 618047A3 SU 762391504 A SU762391504 A SU 762391504A SU 2391504 A SU2391504 A SU 2391504A SU 618047 A3 SU618047 A3 SU 618047A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- nitrogen
- reaction
- carboxyalkylphosphines
- concentrated
- hydrochloric acid
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 12
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 9
- 229910052757 nitrogen Inorganic materials 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 5
- SAWKFRBJGLMMES-UHFFFAOYSA-N methylphosphine Chemical compound PC SAWKFRBJGLMMES-UHFFFAOYSA-N 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- DPBZYCJFTHESDI-UHFFFAOYSA-N 3-sulfanylpropanoic acid;hydrochloride Chemical compound Cl.OC(=O)CCS DPBZYCJFTHESDI-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 1
- LSKVBJHJMLFTDB-UHFFFAOYSA-N chloro(methyl)phosphane Chemical compound CPCl LSKVBJHJMLFTDB-UHFFFAOYSA-N 0.000 description 1
- USJRLGNYCQWLPF-UHFFFAOYSA-N chlorophosphane Chemical compound ClP USJRLGNYCQWLPF-UHFFFAOYSA-N 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- YOTZYFSGUCFUKA-UHFFFAOYSA-N dimethylphosphine Chemical compound CPC YOTZYFSGUCFUKA-UHFFFAOYSA-N 0.000 description 1
- JLHMVTORNNQCRM-UHFFFAOYSA-N ethylphosphine Chemical compound CCP JLHMVTORNNQCRM-UHFFFAOYSA-N 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- -1 for example Chemical compound 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 235000012907 honey Nutrition 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- REJGOFYVRVIODZ-UHFFFAOYSA-N phosphanium;chloride Chemical class P.Cl REJGOFYVRVIODZ-UHFFFAOYSA-N 0.000 description 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-O phosphonium Chemical compound [PH4+] XYFCBTPGUUZFHI-UHFFFAOYSA-O 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
- C07F9/5304—Acyclic saturated phosphine oxides or thioxides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2540283A DE2540283C3 (de) | 1975-09-10 | 1975-09-10 | Verfahren zur Herstellung von carboxylgruppenhaltigen organischen Phosphorverbindungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU618047A3 true SU618047A3 (ru) | 1978-07-30 |
Family
ID=5956081
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU762391504A SU618047A3 (ru) | 1975-09-10 | 1976-08-30 | Способ получени окисей карбоксиалкилфосфинов |
Country Status (16)
| Country | Link |
|---|---|
| JP (1) | JPS5233628A (de) |
| AT (1) | AT341542B (de) |
| BE (1) | BE845987A (de) |
| CA (1) | CA1066715A (de) |
| CH (1) | CH626627A5 (de) |
| DD (1) | DD126885A5 (de) |
| DE (1) | DE2540283C3 (de) |
| DK (1) | DK406976A (de) |
| FR (1) | FR2323695A1 (de) |
| GB (1) | GB1517865A (de) |
| IE (1) | IE43625B1 (de) |
| IT (1) | IT1076807B (de) |
| NL (1) | NL7609964A (de) |
| SE (1) | SE422802B (de) |
| SU (1) | SU618047A3 (de) |
| ZA (1) | ZA765384B (de) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4537993A (en) * | 1984-03-19 | 1985-08-27 | American Cyanamid Company | Bis(β-carboxyethyl)isobutyl, sec. butyl and t-butyl phosphine oxide and polyamides containing the same |
| DE19613066C2 (de) * | 1996-04-01 | 1998-09-10 | Clariant Gmbh | Verfahren zur Herstellung phosphormodifizierter Epoxidharze |
| DE19613067C2 (de) * | 1996-04-01 | 1998-12-03 | Clariant Gmbh | Phosphormodifizierte Epoxidharzmischungen aus Epoxidharzen, phosphorhaltigen Verbindungen und einem Härter, ein Verfahren zu deren Herstellung und ihre Verwendung |
| DE19828863C1 (de) * | 1998-06-29 | 1999-09-02 | Clariant Gmbh | Verfahren zur Herstellung von Phosphinsäureestern und deren Verwendung |
| DE19828861C1 (de) * | 1998-06-29 | 1999-12-02 | Clariant Gmbh | Verfahren zur Herstellung von Phosphonigsäureestern und deren Verwendung |
| DE19923617C2 (de) | 1999-05-25 | 2001-10-31 | Clariant Gmbh | Verfahren zur Herstellung von Phosphinsäureestern |
| DE10153780C1 (de) | 2001-11-02 | 2002-11-28 | Clariant Gmbh | Verfahren zur Herstellung von Carboxyethylmethylphosphinsäureglykolester und ihre Verwendung |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2957931A (en) * | 1949-07-28 | 1960-10-25 | Socony Mobil Oil Co Inc | Synthesis of compounds having a carbonphosphorus linkage |
| US3029272A (en) * | 1958-10-17 | 1962-04-10 | Commercial Solvents Corp | Alkylation of phosphonates |
| DE2100779A1 (de) * | 1971-01-08 | 1972-07-20 | Farbwerke Hoechst AG vormals Meister Lucius & Brüning, 6000 Frankfurt | Verfahren zur Herstellung von Dialkylphosphinsäureestern |
-
1975
- 1975-09-10 DE DE2540283A patent/DE2540283C3/de not_active Expired
-
1976
- 1976-08-18 CH CH1053176A patent/CH626627A5/de not_active IP Right Cessation
- 1976-08-23 CA CA259,647A patent/CA1066715A/en not_active Expired
- 1976-08-26 GB GB35553/76A patent/GB1517865A/en not_active Expired
- 1976-08-30 SE SE7609574A patent/SE422802B/xx unknown
- 1976-08-30 SU SU762391504A patent/SU618047A3/ru active
- 1976-09-08 NL NL7609964A patent/NL7609964A/xx not_active Application Discontinuation
- 1976-09-08 AT AT665176A patent/AT341542B/de not_active IP Right Cessation
- 1976-09-08 IT IT51168/76A patent/IT1076807B/it active
- 1976-09-08 DD DD194694A patent/DD126885A5/xx unknown
- 1976-09-09 IE IE2019/76A patent/IE43625B1/en unknown
- 1976-09-09 JP JP51108399A patent/JPS5233628A/ja active Pending
- 1976-09-09 BE BE170461A patent/BE845987A/xx not_active IP Right Cessation
- 1976-09-09 ZA ZA765384A patent/ZA765384B/xx unknown
- 1976-09-09 DK DK406976A patent/DK406976A/da unknown
- 1976-09-10 FR FR7627378A patent/FR2323695A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| IE43625B1 (en) | 1981-04-22 |
| GB1517865A (en) | 1978-07-12 |
| AT341542B (de) | 1978-02-10 |
| DE2540283B2 (de) | 1980-07-10 |
| DE2540283C3 (de) | 1981-10-01 |
| IT1076807B (it) | 1985-04-27 |
| BE845987A (fr) | 1977-03-09 |
| DD126885A5 (de) | 1977-08-17 |
| SE422802B (sv) | 1982-03-29 |
| CA1066715A (en) | 1979-11-20 |
| FR2323695B1 (de) | 1980-05-23 |
| NL7609964A (nl) | 1977-03-14 |
| FR2323695A1 (fr) | 1977-04-08 |
| DK406976A (da) | 1977-03-11 |
| ZA765384B (en) | 1977-09-28 |
| SE7609574L (sv) | 1977-03-11 |
| DE2540283A1 (de) | 1977-03-17 |
| CH626627A5 (en) | 1981-11-30 |
| IE43625L (en) | 1977-03-10 |
| JPS5233628A (en) | 1977-03-14 |
| ATA665176A (de) | 1977-06-15 |
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