SU362012A1 - - Google Patents

Info

Publication number

SU362012A1

SU362012A1 SU1619837A SU1619837A SU362012A1 SU 362012 A1 SU362012 A1 SU 362012A1 SU 1619837 A SU1619837 A SU 1619837A SU 1619837 A SU1619837 A SU 1619837A SU 362012 A1 SU362012 A1 SU 362012A1

Authority

SU

USSR - Soviet Union

Prior art keywords

phenethyl

ethanol

mol

solution

phenylthiourea

Prior art date

1971-02-08

Links

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• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 21
• 238000000034 method Methods 0.000 description 7
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
• QKFJKGMPGYROCL-UHFFFAOYSA-N phenyl isothiocyanate Chemical compound S=C=NC1=CC=CC=C1 QKFJKGMPGYROCL-UHFFFAOYSA-N 0.000 description 6
• 125000000217 alkyl group Chemical group 0.000 description 5
• -1 aryl isothiocyanate Chemical class 0.000 description 5
• 239000002244 precipitate Substances 0.000 description 5
• 238000002360 preparation method Methods 0.000 description 4
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
• 229940117953 phenylisothiocyanate Drugs 0.000 description 3
• 238000001953 recrystallisation Methods 0.000 description 3
• 239000000126 substance Substances 0.000 description 3
• 125000004172 4-methoxyphenyl group Chemical group [H]C1=C([H])C(OC([H])([H])[H])=C([H])C([H])=C1* 0.000 description 2
• 238000001816 cooling Methods 0.000 description 2
• 239000013078 crystal Substances 0.000 description 2
• 238000002844 melting Methods 0.000 description 2
• 230000008018 melting Effects 0.000 description 2
• VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
• 239000003960 organic solvent Substances 0.000 description 2
• 239000000047 product Substances 0.000 description 2
• UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 2
• 150000003585 thioureas Chemical class 0.000 description 2
• JYKYYPPZLPVIBY-UHFFFAOYSA-N 1-isothiocyanato-2-methylbenzene Chemical compound CC1=CC=CC=C1N=C=S JYKYYPPZLPVIBY-UHFFFAOYSA-N 0.000 description 1
• NEBAVPGEWUNSPL-UHFFFAOYSA-N 3-(N-ethoxyanilino)propanenitrile Chemical compound CCON(CCC#N)C1=CC=CC=C1 NEBAVPGEWUNSPL-UHFFFAOYSA-N 0.000 description 1
• 208000037157 Azotemia Diseases 0.000 description 1
• XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Natural products NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
• 238000010521 absorption reaction Methods 0.000 description 1
• 150000001412 amines Chemical class 0.000 description 1
• 125000003118 aryl group Chemical group 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 150000001875 compounds Chemical class 0.000 description 1
• 238000002329 infrared spectrum Methods 0.000 description 1
• 230000003993 interaction Effects 0.000 description 1
• 238000002955 isolation Methods 0.000 description 1
• 150000002540 isothiocyanates Chemical class 0.000 description 1
• 125000003261 o-tolyl group Chemical group [H]C1=C([H])C(*)=C(C([H])=C1[H])C([H])([H])[H] 0.000 description 1
• 239000000843 powder Substances 0.000 description 1
• 239000002904 solvent Substances 0.000 description 1
• 230000006641 stabilisation Effects 0.000 description 1
• 238000011105 stabilization Methods 0.000 description 1
• 239000007858 starting material Substances 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 239000000725 suspension Substances 0.000 description 1
• 208000009852 uremia Diseases 0.000 description 1