SK280574B6 - Spôsob izolácie cukrov - Google Patents
Spôsob izolácie cukrov Download PDFInfo
- Publication number
- SK280574B6 SK280574B6 SK705-94A SK70594A SK280574B6 SK 280574 B6 SK280574 B6 SK 280574B6 SK 70594 A SK70594 A SK 70594A SK 280574 B6 SK280574 B6 SK 280574B6
- Authority
- SK
- Slovakia
- Prior art keywords
- ions
- sugar
- sodium
- sugars
- liquid waste
- Prior art date
Links
- 235000000346 sugar Nutrition 0.000 title claims abstract description 70
- 238000011084 recovery Methods 0.000 title abstract description 4
- 235000013379 molasses Nutrition 0.000 claims abstract description 33
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 24
- 238000011069 regeneration method Methods 0.000 claims abstract description 24
- 229910001415 sodium ion Inorganic materials 0.000 claims abstract description 24
- 229910001414 potassium ion Inorganic materials 0.000 claims abstract description 23
- 230000008929 regeneration Effects 0.000 claims abstract description 23
- 150000008163 sugars Chemical class 0.000 claims abstract description 23
- 239000003729 cation exchange resin Substances 0.000 claims abstract description 22
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 17
- 229910001425 magnesium ion Inorganic materials 0.000 claims abstract description 14
- 229910001424 calcium ion Inorganic materials 0.000 claims abstract description 13
- 238000004587 chromatography analysis Methods 0.000 claims abstract description 13
- -1 Mg2+ ions Chemical class 0.000 claims abstract description 7
- 238000000926 separation method Methods 0.000 claims abstract description 5
- 239000011347 resin Substances 0.000 claims description 40
- 229920005989 resin Polymers 0.000 claims description 40
- 239000011734 sodium Substances 0.000 claims description 32
- 239000011575 calcium Substances 0.000 claims description 26
- 239000010808 liquid waste Substances 0.000 claims description 24
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 19
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 13
- 125000002091 cationic group Chemical group 0.000 claims description 12
- JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 claims description 11
- 229910052708 sodium Inorganic materials 0.000 claims description 11
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical group [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000002955 isolation Methods 0.000 claims description 6
- 239000003086 colorant Substances 0.000 claims description 4
- 229940023913 cation exchange resins Drugs 0.000 claims 1
- 239000007788 liquid Substances 0.000 abstract description 20
- 239000004150 EU approved colour Substances 0.000 abstract 1
- 229940006093 opthalmologic coloring agent diagnostic Drugs 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 description 14
- 239000011777 magnesium Substances 0.000 description 14
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 10
- 229910052791 calcium Inorganic materials 0.000 description 5
- 239000011780 sodium chloride Substances 0.000 description 5
- 239000002699 waste material Substances 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 4
- 230000001172 regenerating effect Effects 0.000 description 4
- 238000010828 elution Methods 0.000 description 3
- 238000005342 ion exchange Methods 0.000 description 3
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical compound [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 description 2
- 238000013375 chromatographic separation Methods 0.000 description 2
- 238000005352 clarification Methods 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 159000000001 potassium salts Chemical class 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 241000219310 Beta vulgaris subsp. vulgaris Species 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 240000000111 Saccharum officinarum Species 0.000 description 1
- 235000007201 Saccharum officinarum Nutrition 0.000 description 1
- 235000021536 Sugar beet Nutrition 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000012539 chromatography resin Substances 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 239000003480 eluent Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 238000001032 ion-exclusion chromatography Methods 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920005553 polystyrene-acrylate Polymers 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B35/00—Extraction of sucrose from molasses
- C13B35/02—Extraction of sucrose from molasses by chemical means
- C13B35/06—Extraction of sucrose from molasses by chemical means using ion exchange
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
- C13B20/144—Purification of sugar juices using ion-exchange materials using only cationic ion-exchange material
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Saccharide Compounds (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Non-Alcoholic Beverages (AREA)
- Treatment Of Water By Ion Exchange (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08075634 US5443650B2 (en) | 1993-06-11 | 1993-06-11 | Process for softening a sugar-containing aqueous solution such as sugar juice or molasses |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| SK70594A3 SK70594A3 (en) | 1995-03-08 |
| SK280574B6 true SK280574B6 (sk) | 2000-04-10 |
Family
ID=22127050
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SK705-94A SK280574B6 (sk) | 1993-06-11 | 1994-06-08 | Spôsob izolácie cukrov |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US5443650B2 (cs) |
| EP (1) | EP0629707B1 (cs) |
| CN (1) | CN1043903C (cs) |
| AT (1) | ATE178099T1 (cs) |
| AU (1) | AU668305B2 (cs) |
| CA (1) | CA2125749A1 (cs) |
| CZ (1) | CZ289046B6 (cs) |
| DE (1) | DE69417292T2 (cs) |
| DK (1) | DK0629707T3 (cs) |
| ES (1) | ES2130375T3 (cs) |
| GR (1) | GR3030118T3 (cs) |
| MA (1) | MA23222A1 (cs) |
| PH (1) | PH31548A (cs) |
| PL (1) | PL303771A1 (cs) |
| RU (1) | RU2122031C1 (cs) |
| SK (1) | SK280574B6 (cs) |
| UA (1) | UA27814C2 (cs) |
| ZA (1) | ZA944017B (cs) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5554227A (en) * | 1993-11-12 | 1996-09-10 | Societe Nouvelle De Recherches Et D'applications Industrielles D'echangeurs D'ions Applexion | Process of manufacturing crystal sugar from an aqueous sugar juice such as cane juice or sugar beet juice |
| IT1275974B1 (it) * | 1995-03-27 | 1997-10-24 | Resindion S R L | Procedimento di trattamento con una resina scambiatrice di ioni di una soluzione zuccherina derivata da barbabietola |
| FR2753456B1 (fr) * | 1996-09-18 | 1998-12-31 | Generale Sucriere Sa | Procede de regeneration de resines echangeuses d'ions dans le processus de decalcification des jus de sucrerie |
| AUPO821397A0 (en) * | 1997-07-24 | 1997-08-14 | Commonwealth Scientific And Industrial Research Organisation | Process for the purification of nutrients from food process streams |
| AU726559C (en) * | 1997-07-24 | 2001-08-30 | Commonwealth Scientific And Industrial Research Organisation | Process for the purification of nutrients from food process streams |
| US7150885B2 (en) * | 1998-10-09 | 2006-12-19 | Mitsui Sugar Co., Ltd. | Preventives/remedies for infection, anti-endtoxin agents, vaccine adjuvants and growth promoters |
| AU781362B2 (en) * | 1999-04-07 | 2005-05-19 | Ufion (Proprietary) Limited | Treatment of sugar juice |
| IL147529A0 (en) * | 2002-01-09 | 2002-08-14 | Oladur Ltd | A method for the production of soybean sugars and the product produced thereof |
| FR2844209B1 (fr) * | 2002-09-06 | 2007-10-19 | Applexion Ste Nouvelle De Rech | Procede de purification par nanofiltration d'une solution aqueuse sucree contenant des anions et cations monovalents et polyvalents |
| FR2844151B1 (fr) * | 2002-09-06 | 2006-05-26 | Applexion Ste Nouvelle De Rech | Procede de decalcification d'une solution aqueuse et utilisation de ce procede pour la decalcification de lactoserum ou d'un permeat d'ultrafiltration de lactoserum |
| US6790245B2 (en) * | 2002-10-07 | 2004-09-14 | Benetech, Inc. | Control of dust |
| RU2247153C1 (ru) * | 2003-07-02 | 2005-02-27 | Рязанов Евгений Михайлович | Способ очистки растворов, содержащих сахарозу |
| FR2907687B1 (fr) * | 2006-10-30 | 2008-12-26 | Applexion | Procede de purification de sialyllactose par chromatographie |
| CN101835727B (zh) * | 2007-08-30 | 2013-08-07 | 埃欧金能源公司 | 从糖的水溶液中除去钙并获得硫酸盐的方法 |
| CN101403017B (zh) * | 2008-10-31 | 2011-06-08 | 华南理工大学 | 一种二混蜜脱钾钠树脂的再生方法 |
| EP2672832B1 (en) | 2011-02-08 | 2020-03-25 | The Product Makers (Australia) Pty Ltd | Sugar extracts |
| US9017767B2 (en) | 2012-06-13 | 2015-04-28 | Benetech, Inc. | Method of suppressing dust in piles and railcars using plasticized cellulose ethers |
| US9267063B2 (en) | 2012-11-19 | 2016-02-23 | Benetech, Inc. | Dust suppression formulas using plasticized cellulose ethers |
| RU2621995C1 (ru) * | 2016-09-21 | 2017-06-08 | Федеральное государственное бюджетное научное учреждение "Краснодарский научно-исследовательский институт хранения и переработки сельскохозяйственной продукции" (ФГБНУ КНИИХП) | Способ очистки диффузионного сока |
| CN112795710A (zh) * | 2020-12-08 | 2021-05-14 | 武汉美味源生物工程有限公司 | 制糖过程中离子交换树脂的再生方法 |
| CN112593017A (zh) * | 2020-12-15 | 2021-04-02 | 新疆冠农果茸股份有限公司 | 一种用于甜菜制糖糖分高效分离方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB141155A (en) * | 1919-02-21 | 1920-04-15 | Harold Thomas Shakespeare | A new or improved handle for saucepans or like receptacles |
| FR1404591A (fr) * | 1964-05-21 | 1965-07-02 | Magyar Cukoripar Ki | Procédé pour régénérer les échangeurs d'ions et pour réduire la teneur en ions alcalins des jus de sortie des sucreries, en vue de leur utilisation pour l'adoucissement des jus dilués, au moyen d'un échange d'ions |
| DE2362211C3 (de) * | 1973-12-14 | 1978-05-11 | Sueddeutsche Zucker Ag, 6800 Mannheim | Verfahren zur Aufarbeitung von Melassen |
| DE2511904C3 (de) * | 1975-03-19 | 1980-05-22 | Sueddeutsche Zucker-Ag, 6800 Mannheim | Verfahren zur Aufarbeitung von Melassen |
| US4140541A (en) * | 1977-03-25 | 1979-02-20 | Karel Popper | Treatment of crude sugar juices by ion exchange |
| US4519845A (en) * | 1984-02-09 | 1985-05-28 | Uop Inc. | Separation of sucrose from molasses |
| US5110369A (en) * | 1990-10-24 | 1992-05-05 | Mobil Solar Energy Corporation | Cable interconnections for solar cell modules |
-
1993
- 1993-06-11 US US08075634 patent/US5443650B2/en not_active Expired - Lifetime
-
1994
- 1994-06-07 CZ CZ19941393A patent/CZ289046B6/cs not_active IP Right Cessation
- 1994-06-08 SK SK705-94A patent/SK280574B6/sk not_active IP Right Cessation
- 1994-06-08 ZA ZA944017A patent/ZA944017B/xx unknown
- 1994-06-09 MA MA23535A patent/MA23222A1/fr unknown
- 1994-06-09 PH PH48411A patent/PH31548A/en unknown
- 1994-06-10 ES ES94401313T patent/ES2130375T3/es not_active Expired - Lifetime
- 1994-06-10 CN CN94106564A patent/CN1043903C/zh not_active Expired - Fee Related
- 1994-06-10 EP EP94401313A patent/EP0629707B1/fr not_active Expired - Lifetime
- 1994-06-10 AU AU64676/94A patent/AU668305B2/en not_active Ceased
- 1994-06-10 AT AT94401313T patent/ATE178099T1/de not_active IP Right Cessation
- 1994-06-10 DE DE69417292T patent/DE69417292T2/de not_active Expired - Fee Related
- 1994-06-10 PL PL94303771A patent/PL303771A1/xx unknown
- 1994-06-10 UA UA94005250A patent/UA27814C2/uk unknown
- 1994-06-10 DK DK94401313T patent/DK0629707T3/da active
- 1994-06-10 RU RU94020736A patent/RU2122031C1/ru not_active IP Right Cessation
- 1994-06-13 CA CA002125749A patent/CA2125749A1/fr not_active Abandoned
-
1999
- 1999-04-30 GR GR990401200T patent/GR3030118T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA2125749A1 (fr) | 1994-12-12 |
| UA27814C2 (uk) | 2000-10-16 |
| EP0629707B1 (fr) | 1999-03-24 |
| EP0629707A2 (fr) | 1994-12-21 |
| CZ289046B6 (cs) | 2001-10-17 |
| ES2130375T3 (es) | 1999-07-01 |
| GR3030118T3 (en) | 1999-07-30 |
| AU668305B2 (en) | 1996-04-26 |
| US5443650B1 (en) | 1998-05-26 |
| MA23222A1 (fr) | 1994-12-31 |
| CN1111678A (zh) | 1995-11-15 |
| PH31548A (en) | 1998-11-03 |
| CN1043903C (zh) | 1999-06-30 |
| ZA944017B (en) | 1995-02-09 |
| ATE178099T1 (de) | 1999-04-15 |
| US5443650B2 (en) | 2000-05-30 |
| SK70594A3 (en) | 1995-03-08 |
| CZ139394A3 (en) | 1995-02-15 |
| DK0629707T3 (da) | 1999-10-11 |
| DE69417292D1 (de) | 1999-04-29 |
| AU6467694A (en) | 1994-12-15 |
| RU2122031C1 (ru) | 1998-11-20 |
| DE69417292T2 (de) | 1999-09-02 |
| US5443650A (en) | 1995-08-22 |
| EP0629707A3 (fr) | 1995-02-15 |
| PL303771A1 (en) | 1995-01-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Patent lapsed due to non-payment of maintenance fees |
Effective date: 20090608 |