RU93058442A - Азеотропная смесь, способы удаления фтороводорода - Google Patents
Азеотропная смесь, способы удаления фтороводородаInfo
- Publication number
- RU93058442A RU93058442A RU93058442/04A RU93058442A RU93058442A RU 93058442 A RU93058442 A RU 93058442A RU 93058442/04 A RU93058442/04 A RU 93058442/04A RU 93058442 A RU93058442 A RU 93058442A RU 93058442 A RU93058442 A RU 93058442A
- Authority
- RU
- Russia
- Prior art keywords
- hydrogen
- hydrogen fluoride
- methods
- azeotropic mixture
- mixture
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims 5
- 229910052739 hydrogen Inorganic materials 0.000 title 2
- 239000001257 hydrogen Substances 0.000 title 2
- -1 HYDROGEN HYDROGEN Chemical class 0.000 title 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N HF Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims 8
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims 8
- YMWUJEATGCHHMB-UHFFFAOYSA-N methylene dichloride Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims 4
- XWCDCDSDNJVCLO-UHFFFAOYSA-N Chlorofluoromethane Chemical compound FCCl XWCDCDSDNJVCLO-UHFFFAOYSA-N 0.000 claims 2
- RWRIWBAIICGTTQ-UHFFFAOYSA-N Difluoromethane Chemical compound FCF RWRIWBAIICGTTQ-UHFFFAOYSA-N 0.000 claims 2
- 238000004821 distillation Methods 0.000 claims 2
- 230000000875 corresponding Effects 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 239000007791 liquid phase Substances 0.000 claims 1
- 239000012071 phase Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
Claims (1)
- Фтороводород (HF) эффективно удаляется из смеси, состоящей из фтороводорода, дихлорметана, хлорфторометана и/или дифторометана, путем дистилляции смеси для удаления двухкомпонентных азеотропных смесей фтороводорода и дихлорметана, фтороводорода и хлорфторометана, фтороводорода и дифторометана, или путем разделения смеси на верхнюю жидкую фазу, обогащенную фтороводородом, и нижнюю жидкую фазу, обедненную фтороводородом, и дистилляции соответствующих фаз.
Applications Claiming Priority (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP9266792 | 1992-04-13 | ||
JP92667/1992 | 1992-04-13 | ||
JP92667/92 | 1992-04-13 | ||
JP10765692 | 1992-04-27 | ||
JP107656/92 | 1992-04-27 | ||
JP107656/1992 | 1992-04-27 |
Publications (2)
Publication Number | Publication Date |
---|---|
RU93058442A true RU93058442A (ru) | 1996-12-10 |
RU2118635C1 RU2118635C1 (ru) | 1998-09-10 |
Family
ID=26434051
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
RU93058442A RU2118635C1 (ru) | 1992-04-13 | 1993-04-09 | Азеотропная смесь и способы выделения фтороводорода |
Country Status (13)
Country | Link |
---|---|
US (2) | US5523015A (ru) |
EP (1) | EP0606482B1 (ru) |
JP (1) | JP3147380B2 (ru) |
KR (3) | KR100295306B1 (ru) |
CN (1) | CN1039313C (ru) |
AU (1) | AU663586B2 (ru) |
BR (1) | BR9305484A (ru) |
CA (1) | CA2111007C (ru) |
DE (1) | DE69319711T2 (ru) |
ES (1) | ES2118949T3 (ru) |
RU (1) | RU2118635C1 (ru) |
TW (1) | TW283659B (ru) |
WO (1) | WO1993021140A1 (ru) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3163831B2 (ja) * | 1993-04-06 | 2001-05-08 | ダイキン工業株式会社 | 1,1−ジフルオロエタンとフッ化水素の共沸混合物および1,1−ジフルオロエタンまたはフッ化水素の回収方法 |
GB9407257D0 (en) * | 1993-04-22 | 1994-06-08 | Ici Plc | Vaporisation of liquids |
US6274781B1 (en) * | 1993-11-01 | 2001-08-14 | E. I. Du Pont De Nemours And Company | Production of dihalomethanes containing fluorine and azeotropes of dihalomethanes containing chlorine with HF |
DE69500938T2 (de) * | 1994-02-28 | 1998-04-30 | Atochem Elf Sa | Verfahren zur Trennung von Fluorwasserstoff und Difluormethan |
US5718807A (en) * | 1994-09-20 | 1998-02-17 | E. I. Du Pont De Nemours And Company | Purification process for hexafluoroethane products |
US5789633A (en) * | 1995-06-06 | 1998-08-04 | E. I. Du Pont De Nemours And Company | Azeotropic or azeotrope-like compositions of hydrofluoric acid with dihaloethanes |
US5672788A (en) * | 1995-06-07 | 1997-09-30 | E. I. Du Pont De Nemours And Company | Two-step process for manufacturing 1,1-difluoroethane |
US5714650A (en) * | 1995-06-07 | 1998-02-03 | E. I. Du Pont De Nemours And Company | Continuous manufacture of 1,1-difluoroethane |
US5763708A (en) * | 1995-09-20 | 1998-06-09 | Allied Signal Inc. | Process for the production of difluoromethane |
US5785822A (en) * | 1996-05-23 | 1998-07-28 | Alliedsignal Inc. | Process for separating difluoromethane |
WO1998000379A1 (en) * | 1996-07-03 | 1998-01-08 | Alliedsignal Inc. | Water extraction of hydrogen fluoride from a halocarbon/hydrogen fluoride azeotropic mixture |
AU3869597A (en) * | 1996-08-27 | 1998-03-19 | Daikin Industries, Ltd. | Process for producing difluoromethane |
WO1998008789A1 (fr) * | 1996-08-27 | 1998-03-05 | Daikin Industries, Ltd. | Procede de fabrication de difluoromethane |
US5800682A (en) * | 1996-10-08 | 1998-09-01 | Alliedsignal Inc. | Process for the production of difluoromethane |
FR2768717B1 (fr) * | 1997-09-24 | 1999-11-12 | Solvay | Procede de separation de fluorure d'hydrogene de ses melanges avec un hydrofluoroalcane contenant de 3 a 6 atomes de carbone |
US6488817B1 (en) * | 1998-03-31 | 2002-12-03 | Alliedsignal Inc. | Purification of hydrofluorocarbons |
US6500795B2 (en) * | 2001-01-24 | 2002-12-31 | Honeywell International Inc. | Azeotrope-like composition of 1-chloro-1,3,3,3-tetrafluoropropane and hydrogen fluoride |
US6605193B2 (en) | 2001-04-25 | 2003-08-12 | Atofina Chemicals, Inc. | Recovery of HFC-32 |
EP2093187A1 (en) * | 2001-06-01 | 2009-08-26 | Honeywell International Inc. | Process for the Removal of 1,1,1,3,3-Pentafluorobutane |
EP2054361B1 (en) * | 2006-08-24 | 2016-02-17 | E. I. du Pont de Nemours and Company | Processes for separation of fluoroolefins from hydrogen fluoride by azeotropic distillation |
CN103626626B (zh) * | 2013-11-01 | 2015-06-24 | 西安近代化学研究所 | 氟化氢和2-氯-1,1,1,2-四氟丙烷混合物的分离方法 |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2450414A (en) | 1946-11-14 | 1948-10-05 | Kinetic Chemicals Inc | Distillation process for separating products of chloroform fluorination |
US3490739A (en) * | 1965-09-16 | 1970-01-20 | Walter R Buckman | Azeotropic composition containing hexafluoroacetone,hydrogen fluoride,and trichlorotrifluoroethane |
NL6617916A (ru) * | 1965-12-22 | 1967-06-23 | ||
US3728268A (en) * | 1970-12-11 | 1973-04-17 | Du Pont | Mixtures of 1,1,2-trichloro-1,2,2-trifluoroethane,ethanol and acetone and a ternary azeotrope thereof |
US3789004A (en) * | 1971-06-28 | 1974-01-29 | Ici Ltd | Solvent compositions |
US3947558A (en) | 1973-08-16 | 1976-03-30 | Dow Chemical (Nederland) B.V. | Method of recovering HF from mixtures containing C1 -C3 halocarbon compounds |
US4020112A (en) * | 1975-02-06 | 1977-04-26 | E. I. Du Pont De Nemours And Company | Oxidative fluorination of phenols |
US4169807A (en) * | 1978-03-20 | 1979-10-02 | Rca Corporation | Novel solvent drying agent |
JPS59225131A (ja) | 1983-06-06 | 1984-12-18 | Showa Denko Kk | ジフルオロメタンの製造方法 |
JPS6013726A (ja) | 1983-07-04 | 1985-01-24 | Showa Denko Kk | フルオロメタンの製造方法 |
US4911792A (en) * | 1988-08-01 | 1990-03-27 | E. I. Du Pont De Nemours And Company | Process for the separation of HF via phase separation and distillation |
US4975156A (en) * | 1989-05-04 | 1990-12-04 | Atochem North America, Inc. | Process for the separation of hydrogen fluoride, 1,1-dichloro-1-fluoroethane and 1-chloro-1,1-difluoroethane from liquid mixtures thereof |
US4950364A (en) * | 1989-05-04 | 1990-08-21 | Pennwalt Corporation | Process for the separation of 1,1-dichloro-1-fluoroethane and 1,1,1,3,3-pentafluorobutane |
US5036036A (en) | 1989-06-13 | 1991-07-30 | E. I. Du Pont De Nemours And Company | Chromium oxide catalyst composition |
DE69031344D1 (de) | 1989-10-04 | 1997-10-02 | Du Pont | Verfahren zur reinigung von fluorkohlenwasserstoffen |
GB9105407D0 (en) * | 1991-03-14 | 1991-05-01 | Ici Plc | Separation process |
US5196616A (en) * | 1991-10-18 | 1993-03-23 | E. I. Du Pont De Nemours And Company | Process for separating and recovering fluorocarbons and hydrogen fluoride from mixtures thereof |
US6274781B1 (en) | 1993-11-01 | 2001-08-14 | E. I. Du Pont De Nemours And Company | Production of dihalomethanes containing fluorine and azeotropes of dihalomethanes containing chlorine with HF |
DE69500938T2 (de) * | 1994-02-28 | 1998-04-30 | Atochem Elf Sa | Verfahren zur Trennung von Fluorwasserstoff und Difluormethan |
-
1993
- 1993-04-09 KR KR1019930703863A patent/KR100295306B1/ko not_active IP Right Cessation
- 1993-04-09 RU RU93058442A patent/RU2118635C1/ru not_active IP Right Cessation
- 1993-04-09 EP EP93908071A patent/EP0606482B1/en not_active Expired - Lifetime
- 1993-04-09 AU AU39040/93A patent/AU663586B2/en not_active Ceased
- 1993-04-09 US US08/162,010 patent/US5523015A/en not_active Expired - Lifetime
- 1993-04-09 JP JP51817493A patent/JP3147380B2/ja not_active Expired - Fee Related
- 1993-04-09 DE DE69319711T patent/DE69319711T2/de not_active Expired - Fee Related
- 1993-04-09 ES ES93908071T patent/ES2118949T3/es not_active Expired - Lifetime
- 1993-04-09 KR KR1020017015229A patent/KR100352680B1/ko not_active IP Right Cessation
- 1993-04-09 BR BR9305484A patent/BR9305484A/pt not_active IP Right Cessation
- 1993-04-09 KR KR10-1998-0702434A patent/KR100338277B1/ko not_active IP Right Cessation
- 1993-04-09 WO PCT/JP1993/000455 patent/WO1993021140A1/ja active Application Filing
- 1993-04-09 CA CA002111007A patent/CA2111007C/en not_active Expired - Fee Related
- 1993-04-13 CN CN93105703A patent/CN1039313C/zh not_active Expired - Lifetime
- 1993-04-13 TW TW082102792A patent/TW283659B/zh not_active IP Right Cessation
-
2000
- 2000-06-14 US US09/593,523 patent/US6311515B1/en not_active Expired - Fee Related
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