RU2341595C2 - Устройство для выращивания кристаллов карбида кремния - Google Patents
Устройство для выращивания кристаллов карбида кремния Download PDFInfo
- Publication number
- RU2341595C2 RU2341595C2 RU2006101147/15A RU2006101147A RU2341595C2 RU 2341595 C2 RU2341595 C2 RU 2341595C2 RU 2006101147/15 A RU2006101147/15 A RU 2006101147/15A RU 2006101147 A RU2006101147 A RU 2006101147A RU 2341595 C2 RU2341595 C2 RU 2341595C2
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- Prior art keywords
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- silicon
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- gases
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- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 title claims abstract description 24
- 229910010271 silicon carbide Inorganic materials 0.000 title claims abstract description 21
- 239000013078 crystal Substances 0.000 title claims abstract description 19
- 239000007789 gas Substances 0.000 claims abstract description 116
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 52
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 52
- 239000010703 silicon Substances 0.000 claims abstract description 52
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 40
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 37
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 13
- 239000011856 silicon-based particle Substances 0.000 claims abstract description 11
- 230000008020 evaporation Effects 0.000 claims abstract description 4
- 238000001704 evaporation Methods 0.000 claims abstract description 4
- 239000000758 substrate Substances 0.000 claims description 18
- 238000005530 etching Methods 0.000 claims description 15
- 239000011521 glass Substances 0.000 claims description 8
- 230000002821 anti-nucleating effect Effects 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- 230000006698 induction Effects 0.000 claims description 4
- 239000000126 substance Substances 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 6
- 239000000203 mixture Substances 0.000 abstract description 6
- 230000001105 regulatory effect Effects 0.000 abstract 2
- 239000002912 waste gas Substances 0.000 abstract 1
- 239000002245 particle Substances 0.000 description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 8
- 238000009826 distribution Methods 0.000 description 7
- 239000001257 hydrogen Substances 0.000 description 7
- 229910052739 hydrogen Inorganic materials 0.000 description 7
- 239000012159 carrier gas Substances 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- 239000002243 precursor Substances 0.000 description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 238000009833 condensation Methods 0.000 description 4
- 230000005494 condensation Effects 0.000 description 4
- 230000008021 deposition Effects 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 229910002804 graphite Inorganic materials 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- IXCSERBJSXMMFS-UHFFFAOYSA-N hcl hcl Chemical compound Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 3
- 150000002431 hydrogen Chemical class 0.000 description 3
- 230000006911 nucleation Effects 0.000 description 3
- 238000010899 nucleation Methods 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- 239000005977 Ethylene Substances 0.000 description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 2
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 2
- 239000007792 gaseous phase Substances 0.000 description 2
- 239000001307 helium Substances 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 239000001294 propane Substances 0.000 description 2
- 229910000077 silane Inorganic materials 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 229910003902 SiCl 4 Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007833 carbon precursor Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000000112 cooling gas Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- MROCJMGDEKINLD-UHFFFAOYSA-N dichlorosilane Chemical compound Cl[SiH2]Cl MROCJMGDEKINLD-UHFFFAOYSA-N 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000004377 microelectronic Methods 0.000 description 1
- 229910021420 polycrystalline silicon Inorganic materials 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 230000000191 radiation effect Effects 0.000 description 1
- 239000005049 silicon tetrachloride Substances 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 1
- 239000005052 trichlorosilane Substances 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
- C30B25/02—Epitaxial-layer growth
- C30B25/14—Feed and outlet means for the gases; Modifying the flow of the reactive gases
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/36—Carbides
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Silicon Compounds (AREA)
- Carbon And Carbon Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ITMI2003A001196 | 2003-06-13 | ||
| IT001196A ITMI20031196A1 (it) | 2003-06-13 | 2003-06-13 | Sistema per crescere cristalli di carburo di silicio |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2006101147A RU2006101147A (ru) | 2006-06-10 |
| RU2341595C2 true RU2341595C2 (ru) | 2008-12-20 |
Family
ID=30131205
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2006101147/15A RU2341595C2 (ru) | 2003-06-13 | 2004-06-09 | Устройство для выращивания кристаллов карбида кремния |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20060283389A1 (enExample) |
| EP (1) | EP1636404A1 (enExample) |
| JP (1) | JP2006527157A (enExample) |
| KR (1) | KR20060017810A (enExample) |
| CN (1) | CN100350082C (enExample) |
| IT (1) | ITMI20031196A1 (enExample) |
| RU (1) | RU2341595C2 (enExample) |
| WO (1) | WO2004111316A1 (enExample) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1471168B2 (en) † | 2003-04-24 | 2011-08-10 | Norstel AB | Device and method for producing single crystals by vapour deposition |
| ITMI20041677A1 (it) * | 2004-08-30 | 2004-11-30 | E T C Epitaxial Technology Ct | Processo di pulitura e processo operativo per un reattore cvd. |
| ITMI20050962A1 (it) * | 2005-05-25 | 2006-11-26 | Lpe Spa | Dispositivo per introurre gas di reazione in una camera di reazione e reattore epitassiale che lo utilizza |
| ITMI20051308A1 (it) * | 2005-07-11 | 2007-01-12 | Milano Politecnico | Metodo e reattore per crescere cristalli |
| EP2074244A4 (en) * | 2006-07-28 | 2011-11-23 | Pronomic Industry Ab | CRYSTALLINE GROWTH METHOD AND REACTOR MODEL |
| JP4962074B2 (ja) * | 2007-03-22 | 2012-06-27 | 株式会社デンソー | 炭化珪素単結晶の製造装置および製造方法 |
| JP5560093B2 (ja) * | 2009-06-30 | 2014-07-23 | 株式会社日立国際電気 | 基板処理装置及び半導体装置の製造方法及び基板製造方法 |
| JP4888548B2 (ja) * | 2009-12-24 | 2012-02-29 | 株式会社デンソー | 炭化珪素単結晶の製造装置および製造方法 |
| JP5562409B2 (ja) * | 2010-02-26 | 2014-07-30 | 株式会社日立国際電気 | 半導体装置の製造方法及び基板製造方法及び基板処理装置 |
| JP5287840B2 (ja) * | 2010-12-16 | 2013-09-11 | 株式会社デンソー | 炭化珪素単結晶の製造装置 |
| JP5212455B2 (ja) * | 2010-12-16 | 2013-06-19 | 株式会社デンソー | 炭化珪素単結晶の製造装置 |
| JP5668638B2 (ja) * | 2011-08-10 | 2015-02-12 | 株式会社デンソー | 炭化珪素単結晶の製造装置 |
| JP5578146B2 (ja) * | 2011-08-10 | 2014-08-27 | 株式会社デンソー | 炭化珪素単結晶製造装置 |
| JP5696804B2 (ja) * | 2014-03-19 | 2015-04-08 | 株式会社デンソー | 炭化珪素単結晶の製造装置 |
| DE102015100062A1 (de) * | 2015-01-06 | 2016-07-07 | Universität Paderborn | Vorrichtung und Verfahren zum Herstellen von Siliziumcarbid |
| US11209306B2 (en) | 2017-11-02 | 2021-12-28 | Fluke Corporation | Portable acoustic imaging tool with scanning and analysis capability |
| US20190129027A1 (en) | 2017-11-02 | 2019-05-02 | Fluke Corporation | Multi-modal acoustic imaging tool |
| CN112703375A (zh) | 2018-07-24 | 2021-04-23 | 弗兰克公司 | 用于投射和显示声学数据的系统和方法 |
| IT201900000223A1 (it) | 2019-01-09 | 2020-07-09 | Lpe Spa | Camera di reazione con elemento rotante e reattore per deposizione di materiale semiconduttore |
| JP7393900B2 (ja) * | 2019-09-24 | 2023-12-07 | 一般財団法人電力中央研究所 | 炭化珪素単結晶ウェハ及び炭化珪素単結晶インゴットの製造方法 |
| WO2021242509A1 (en) * | 2020-05-26 | 2021-12-02 | Unm Rainforest Innovations | Two-dimensional silicon carbide materials and fabrication methods thereof |
| KR102525767B1 (ko) * | 2021-11-11 | 2023-04-27 | 오씨아이 주식회사 | 고순도 SiC 결정체의 제조방법 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2026896C1 (ru) * | 1991-06-19 | 1995-01-20 | Институт проблем механики РАН | Устройство для плазмохимического осаждения пленок |
| WO1997001658A1 (en) * | 1995-06-26 | 1997-01-16 | Abb Research Ltd. | A device and a method for epitaxially growing objects by cvd |
| RU2162117C2 (ru) * | 1999-01-21 | 2001-01-20 | Макаров Юрий Николаевич | Способ эпитаксиального выращивания карбида кремния и реактор для его осуществления |
| WO2001027361A1 (en) * | 1999-10-08 | 2001-04-19 | Cree, Inc. | Method and apparatus for growing silicon carbide crystals |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4866005A (en) * | 1987-10-26 | 1989-09-12 | North Carolina State University | Sublimation of silicon carbide to produce large, device quality single crystals of silicon carbide |
| FI97920C (fi) * | 1991-02-27 | 1997-03-10 | Okmetic Oy | Tapa puhdistaa puolijohdevalmiste |
| JPH05208900A (ja) * | 1992-01-28 | 1993-08-20 | Nisshin Steel Co Ltd | 炭化ケイ素単結晶の成長装置 |
| FI98308C (fi) * | 1994-08-29 | 1997-05-26 | Okmetic Oy | Kiinnitysaine kappaleen kiinnittämiseksi alustaansa |
| US6030661A (en) * | 1995-08-04 | 2000-02-29 | Abb Research Ltd. | Device and a method for epitaxially growing objects by CVD |
| SE9503428D0 (sv) * | 1995-10-04 | 1995-10-04 | Abb Research Ltd | A method for epitaxially growing objects and a device for such a growth |
| SE9503426D0 (sv) * | 1995-10-04 | 1995-10-04 | Abb Research Ltd | A device for heat treatment of objects and a method for producing a susceptor |
| SE9603586D0 (sv) * | 1996-10-01 | 1996-10-01 | Abb Research Ltd | A device for epitaxially growing objects and method for such a growth |
| US6039812A (en) * | 1996-10-21 | 2000-03-21 | Abb Research Ltd. | Device for epitaxially growing objects and method for such a growth |
| JP4053125B2 (ja) * | 1998-01-19 | 2008-02-27 | 住友電気工業株式会社 | SiC単結晶の合成方法 |
| EP0933450B1 (en) * | 1998-01-19 | 2002-04-17 | Sumitomo Electric Industries, Ltd. | Method of making SiC single crystal and apparatus for making SiC single crystal |
| US6045613A (en) * | 1998-10-09 | 2000-04-04 | Cree, Inc. | Production of bulk single crystals of silicon carbide |
| US6486081B1 (en) * | 1998-11-13 | 2002-11-26 | Applied Materials, Inc. | Gas distribution system for a CVD processing chamber |
| US6406539B1 (en) * | 1999-04-28 | 2002-06-18 | Showa Denko K.K, | Process for producing silicon carbide single crystal and production apparatus therefor |
| JP3959952B2 (ja) * | 2000-11-10 | 2007-08-15 | 株式会社デンソー | 炭化珪素単結晶の製造方法及び製造装置 |
| JP3864696B2 (ja) * | 2000-11-10 | 2007-01-10 | 株式会社デンソー | 炭化珪素単結晶の製造方法及び製造装置 |
| US6663025B1 (en) * | 2001-03-29 | 2003-12-16 | Lam Research Corporation | Diffuser and rapid cycle chamber |
| JP4742448B2 (ja) * | 2001-06-06 | 2011-08-10 | 株式会社デンソー | 炭化珪素単結晶の製造方法及び製造装置 |
| JP4329282B2 (ja) * | 2001-06-22 | 2009-09-09 | 株式会社デンソー | 炭化珪素単結晶の製造方法 |
| US6613143B1 (en) * | 2001-07-06 | 2003-09-02 | Technologies And Devices International, Inc. | Method for fabricating bulk GaN single crystals |
| US7147713B2 (en) * | 2003-04-30 | 2006-12-12 | Cree, Inc. | Phase controlled sublimation |
-
2003
- 2003-06-13 IT IT001196A patent/ITMI20031196A1/it unknown
-
2004
- 2004-06-09 EP EP04739749A patent/EP1636404A1/en not_active Withdrawn
- 2004-06-09 CN CNB2004800164824A patent/CN100350082C/zh not_active Expired - Lifetime
- 2004-06-09 RU RU2006101147/15A patent/RU2341595C2/ru not_active IP Right Cessation
- 2004-06-09 KR KR1020057022349A patent/KR20060017810A/ko not_active Withdrawn
- 2004-06-09 WO PCT/EP2004/006244 patent/WO2004111316A1/en not_active Ceased
- 2004-06-09 JP JP2006515874A patent/JP2006527157A/ja active Pending
-
2005
- 2005-04-27 US US11/116,145 patent/US20060283389A1/en not_active Abandoned
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2026896C1 (ru) * | 1991-06-19 | 1995-01-20 | Институт проблем механики РАН | Устройство для плазмохимического осаждения пленок |
| WO1997001658A1 (en) * | 1995-06-26 | 1997-01-16 | Abb Research Ltd. | A device and a method for epitaxially growing objects by cvd |
| RU2162117C2 (ru) * | 1999-01-21 | 2001-01-20 | Макаров Юрий Николаевич | Способ эпитаксиального выращивания карбида кремния и реактор для его осуществления |
| WO2001027361A1 (en) * | 1999-10-08 | 2001-04-19 | Cree, Inc. | Method and apparatus for growing silicon carbide crystals |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20060017810A (ko) | 2006-02-27 |
| CN1806069A (zh) | 2006-07-19 |
| US20060283389A1 (en) | 2006-12-21 |
| WO2004111316A1 (en) | 2004-12-23 |
| JP2006527157A (ja) | 2006-11-30 |
| ITMI20031196A0 (it) | 2003-06-13 |
| ITMI20031196A1 (it) | 2004-12-14 |
| RU2006101147A (ru) | 2006-06-10 |
| CN100350082C (zh) | 2007-11-21 |
| EP1636404A1 (en) | 2006-03-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20090610 |