RU2161150C2 - Способ получения алкилакрилата (варианты) - Google Patents

Способ получения алкилакрилата (варианты) Download PDF

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Publication number
RU2161150C2
RU2161150C2 RU96123848/04A RU96123848A RU2161150C2 RU 2161150 C2 RU2161150 C2 RU 2161150C2 RU 96123848/04 A RU96123848/04 A RU 96123848/04A RU 96123848 A RU96123848 A RU 96123848A RU 2161150 C2 RU2161150 C2 RU 2161150C2
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RU
Russia
Prior art keywords
acrylic acid
water
reactor
acid
stream
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Application number
RU96123848/04A
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English (en)
Russian (ru)
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RU96123848A (ru
Inventor
Бауер Уильям (младший)
Тсенг Чепмэн Джозефина
Джузеппе Лучано Мирабелли Марио
Иесайа Вентер Иеремия
Original Assignee
Ром Энд Хаас Компани
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Publication date
Application filed by Ром Энд Хаас Компани filed Critical Ром Энд Хаас Компани
Publication of RU96123848A publication Critical patent/RU96123848A/ru
Application granted granted Critical
Publication of RU2161150C2 publication Critical patent/RU2161150C2/ru

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/317—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups
    • C07C67/327—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups by elimination of functional groups containing oxygen only in singly bound form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
RU96123848/04A 1995-12-15 1996-12-15 Способ получения алкилакрилата (варианты) RU2161150C2 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US1033495P 1995-12-15 1995-12-15
US010.334 1995-12-15

Publications (2)

Publication Number Publication Date
RU96123848A RU96123848A (ru) 1999-02-20
RU2161150C2 true RU2161150C2 (ru) 2000-12-27

Family

ID=21745257

Family Applications (1)

Application Number Title Priority Date Filing Date
RU96123848/04A RU2161150C2 (ru) 1995-12-15 1996-12-15 Способ получения алкилакрилата (варианты)

Country Status (11)

Country Link
EP (1) EP0779268B1 (enExample)
JP (2) JP3941843B2 (enExample)
KR (1) KR970042475A (enExample)
BR (1) BR9605973A (enExample)
CA (1) CA2192264A1 (enExample)
CZ (1) CZ363896A3 (enExample)
DE (2) DE69621902T2 (enExample)
ES (1) ES2177738T3 (enExample)
RU (1) RU2161150C2 (enExample)
SG (1) SG81213A1 (enExample)
TW (1) TW406070B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2259399C2 (ru) * 2003-10-22 2005-08-27 Федеральное государственное унитарное предприятие "Саратовский научно-исследовательский институт химии и технологий акриловых мономеров и полимеров с опытным заводом" Способ получения эфиров акриловой кислоты и алифатических спиртов c2-c8

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19851984A1 (de) * 1998-11-11 2000-05-18 Basf Ag Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol
DE19922722A1 (de) 1999-05-18 2000-11-23 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
US6482976B1 (en) 1999-06-17 2002-11-19 Union Carbide Chemicals & Plastics Technology Corporation Processes for conducting equilibrium-limited reactions
AU5605400A (en) * 1999-06-17 2001-01-09 Union Carbide Chemicals And Plastics Company Inc. Processes for conducting equilibrium-limited reactions
WO2005007609A1 (de) * 2003-07-11 2005-01-27 Basf Aktiengesellschaft Thermisches trennverfahren zur abtrennung wenigstens eines (meth)acrylmonomere angereichert enthaltenden stoffstroms
JP2011026608A (ja) * 2004-04-23 2011-02-10 Sumitomo Chemical Co Ltd 化学増幅型ポジ型レジスト組成物及び（メタ）アクリル酸誘導体とその製法
ATE519728T1 (de) * 2008-01-18 2011-08-15 Arkema Inc Verfahren zur rückgewinnung eines sulfonsäurekatalysators und wertprodukten aus acrylatnachlauffraktionen
WO2012071158A1 (en) 2010-11-22 2012-05-31 Rohm And Haas Company Acrylate production process
JP5748482B2 (ja) * 2011-01-14 2015-07-15 株式会社ダイセル カルボン酸エステルの製造方法
US10597350B2 (en) * 2016-05-25 2020-03-24 Dow Global Technologies Llc Process for recovering byproducts from MMA
MY200321A (en) * 2017-08-17 2023-12-20 Basf Se Process for continuously preparing n-butyl acrylate or isobutyl acrylate
JP2019156738A (ja) * 2018-03-09 2019-09-19 三菱ケミカル株式会社 （メタ）アクリル酸エステルの製造方法
FR3137090B1 (fr) * 2022-06-24 2024-05-10 Arkema France Procede de valorisation de sous-produits lourds issus de la fabrication d’acide acrylique
FR3137088B1 (fr) * 2022-06-24 2024-05-10 Arkema France Procede de valorisation en batch de sous-produits lourds issus de la fabrication d’acide acrylique
FR3137089B1 (fr) * 2022-06-24 2024-05-10 Arkema France Procede de valorisation de sous-produits lourds issus de la fabrication d’acide acrylique
FR3137091B1 (fr) * 2022-06-24 2024-05-10 Arkema France Procede de valorisation continu de sous-produits lourds issus de la fabrication d’acide acrylique
CN115490590A (zh) * 2022-08-29 2022-12-20 平湖石化有限责任公司 带丙烯酸循环的丙烯酸丁酯连续生产工艺
CN117550667B (zh) * 2023-11-30 2025-10-03 中环信(南京)环境服务有限公司 丙烯酸及酯类回收过程副产含丁醇有机含盐废水综合利用装置及工艺

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4012439A (en) * 1974-10-19 1977-03-15 Hoechst Aktiengesellschaft Continuous production of n-butylacrylate free from dibutylether
GB1515620A (en) * 1975-11-26 1978-06-28 Hoechst Ag Continuous production of alkyl acrylates free from ether
US4968834A (en) * 1990-05-07 1990-11-06 Hoechst Celanese Corporation Recovery of acrylic acid and/or ethyl acrylate from black acid

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3868410A (en) * 1972-08-03 1975-02-25 Celanese Corp Conversion of oligomeric acrylates to acrylate monomers
US3951756A (en) * 1974-11-08 1976-04-20 Celanese Corporation Purification of alkyl esters
FR2727964B1 (fr) * 1994-12-12 1997-01-24 Atochem Elf Sa Procede de recuperation des produits nobles legers contenus dans les residus de distillation des procedes de fabrication de l'acide acrylique et de ses esters
DE19547485A1 (de) * 1995-12-19 1996-05-09 Basf Ag Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4012439A (en) * 1974-10-19 1977-03-15 Hoechst Aktiengesellschaft Continuous production of n-butylacrylate free from dibutylether
GB1471800A (en) * 1974-10-19 1977-04-27 Hoechst Ag Continuous production of n-butyl acrylate free from dibutyl ether
GB1515620A (en) * 1975-11-26 1978-06-28 Hoechst Ag Continuous production of alkyl acrylates free from ether
US4968834A (en) * 1990-05-07 1990-11-06 Hoechst Celanese Corporation Recovery of acrylic acid and/or ethyl acrylate from black acid

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2259399C2 (ru) * 2003-10-22 2005-08-27 Федеральное государственное унитарное предприятие "Саратовский научно-исследовательский институт химии и технологий акриловых мономеров и полимеров с опытным заводом" Способ получения эфиров акриловой кислоты и алифатических спиртов c2-c8

Also Published As

Publication number Publication date
CA2192264A1 (en) 1997-06-16
SG81213A1 (en) 2001-06-19
JP4335925B2 (ja) 2009-09-30
KR970042475A (ko) 1997-07-24
JP3941843B2 (ja) 2007-07-04
DE69634457D1 (de) 2005-04-14
EP0779268B1 (en) 2002-06-19
DE69621902T2 (de) 2003-02-13
CZ363896A3 (en) 1997-07-16
EP0779268A1 (en) 1997-06-18
DE69621902D1 (de) 2002-07-25
DE69634457T2 (de) 2006-01-26
BR9605973A (pt) 1998-08-25
TW406070B (en) 2000-09-21
JPH09208520A (ja) 1997-08-12
JP2007153903A (ja) 2007-06-21
ES2177738T3 (es) 2002-12-16

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