RU2015129704A - Способ получения стекла с использованием электроварки - Google Patents
Способ получения стекла с использованием электроварки Download PDFInfo
- Publication number
- RU2015129704A RU2015129704A RU2015129704A RU2015129704A RU2015129704A RU 2015129704 A RU2015129704 A RU 2015129704A RU 2015129704 A RU2015129704 A RU 2015129704A RU 2015129704 A RU2015129704 A RU 2015129704A RU 2015129704 A RU2015129704 A RU 2015129704A
- Authority
- RU
- Russia
- Prior art keywords
- glass
- manganese
- mno
- expressed
- chemical composition
- Prior art date
Links
- 239000011521 glass Substances 0.000 title claims 6
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 claims 10
- 238000000034 method Methods 0.000 claims 8
- 239000011572 manganese Substances 0.000 claims 7
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 4
- 229910052748 manganese Inorganic materials 0.000 claims 4
- 239000011734 sodium Substances 0.000 claims 4
- 239000000126 substance Substances 0.000 claims 4
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims 3
- 229910004298 SiO 2 Inorganic materials 0.000 claims 3
- 229910010413 TiO 2 Inorganic materials 0.000 claims 3
- 239000011490 mineral wool Substances 0.000 claims 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims 2
- 238000010411 cooking Methods 0.000 claims 2
- 230000009477 glass transition Effects 0.000 claims 2
- 239000000463 material Substances 0.000 claims 2
- 230000003647 oxidation Effects 0.000 claims 2
- 238000007254 oxidation reaction Methods 0.000 claims 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims 1
- 229910002651 NO3 Inorganic materials 0.000 claims 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 239000011152 fibreglass Substances 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims 1
- 229910052750 molybdenum Inorganic materials 0.000 claims 1
- 239000011733 molybdenum Substances 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 239000011819 refractory material Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 238000004017 vitrification Methods 0.000 claims 1
- 238000003466 welding Methods 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B5/00—Melting in furnaces; Furnaces so far as specially adapted for glass manufacture
- C03B5/02—Melting in furnaces; Furnaces so far as specially adapted for glass manufacture in electric furnaces, e.g. by dielectric heating
- C03B5/027—Melting in furnaces; Furnaces so far as specially adapted for glass manufacture in electric furnaces, e.g. by dielectric heating by passing an electric current between electrodes immersed in the glass bath, i.e. by direct resistance heating
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/04—Manufacture of glass fibres or filaments by using centrifugal force, e.g. spinning through radial orifices; Construction of the spinner cups therefor
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/08—Bushings, e.g. construction, bushing reinforcement means; Spinnerettes; Nozzles; Nozzle plates
- C03B37/09—Bushings, e.g. construction, bushing reinforcement means; Spinnerettes; Nozzles; Nozzle plates electrically heated
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C13/00—Fibre or filament compositions
- C03C13/06—Mineral fibres, e.g. slag wool, mineral wool, rock wool
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/062—Glass compositions containing silica with less than 40% silica by weight
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/062—Glass compositions containing silica with less than 40% silica by weight
- C03C3/064—Glass compositions containing silica with less than 40% silica by weight containing boron
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/083—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound
- C03C3/085—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound containing an oxide of a divalent metal
- C03C3/087—Glass compositions containing silica with 40% to 90% silica, by weight containing aluminium oxide or an iron compound containing an oxide of a divalent metal containing calcium oxide, e.g. common sheet or container glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C03C3/091—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/097—Glass compositions containing silica with 40% to 90% silica, by weight containing phosphorus, niobium or tantalum
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2213/00—Glass fibres or filaments
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Geochemistry & Mineralogy (AREA)
- General Chemical & Material Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Electrochemistry (AREA)
- Manufacturing & Machinery (AREA)
- Ceramic Engineering (AREA)
- Glass Compositions (AREA)
- Glass Melting And Manufacturing (AREA)
Claims (13)
1. Способ получения стекла, химический состав которого включает, по меньшей мере, 3 вес.% оксида железа, выраженного в виде Fe2O3, включающий стадию электроварки, с использованием электродов, погруженных в стекломассу из способной к стеклованию смеси материала шихты, в состав которой входит, по меньшей мере, один поставщик марганца, в котором марганец находится в степени окисления выше чем +2.
2. Способ по п. 1, такой, что химический состав стекла включает составляющие в пределах, приводимых ниже, выраженные, вес.%:
3. Способ по п. 1, такой, что указанный или любой поставщик марганца выбраны из MnO2, Mn3O4, Mn2O3, Mn2O7, перманганатов, в частности натрия, калия или даже кальция или магния или любой смеси упомянутых выше.
4. Способ по п. 1, в котором общее количество поставщика марганца, который входит в состав способной к стеклованию смеси материала шихты, является таким, что тонна упомянутой сухой смеси содержит между 1 и 20 кг, конкретно между 2 и 10 кг марганца в степени окисления выше чем +2 в пересчете на MnO2.
5. Способ по п. 1, такой, что способная к стеклованию смесь не содержит нитрата.
6. Способ по п. 1, такой, что электроды изготовлены из молибдена.
7. Способ по п. 1, такой, что во время стадии варки температура стекла, измеренная в контакте с огнеупорами бассейна и в самой горячей точке, находится в интервале, простирающемся от 1400 до 1650°С.
8. Способ по п. 1, такой, что после стадии варки стекло сформировано в минеральную вату во время стадии волокнообразования.
9. Минеральная вата, включающая стекловолокна, имеющие химический состав, включающий следующие составляющие, в пределах, приводимых ниже, выраженные, вес.%:
10. Минеральная вата согласно предшествующему пункту, имеющая химический состав, включающий следующие составляющие, в пределах, приводимых ниже, выраженные, вес.%:
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1262642A FR3000056B1 (fr) | 2012-12-21 | 2012-12-21 | Procede de fabrication de verre par fusion electrique |
| FR1262642 | 2012-12-21 | ||
| PCT/FR2013/053223 WO2014096737A1 (fr) | 2012-12-21 | 2013-12-20 | Procede de fabrication de verre par fusion electrique |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2015129704A true RU2015129704A (ru) | 2017-01-25 |
| RU2675817C2 RU2675817C2 (ru) | 2018-12-25 |
Family
ID=48521054
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2015129704A RU2675817C2 (ru) | 2012-12-21 | 2013-12-20 | Способ получения стекла с использованием электроварки |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US10000404B2 (ru) |
| EP (1) | EP2935138B1 (ru) |
| JP (1) | JP6382837B2 (ru) |
| KR (1) | KR102199540B1 (ru) |
| CN (1) | CN104854053B (ru) |
| AU (2) | AU2013366120A1 (ru) |
| BR (1) | BR112015011860B1 (ru) |
| CA (1) | CA2893455C (ru) |
| DK (1) | DK2935138T3 (ru) |
| FR (1) | FR3000056B1 (ru) |
| NZ (1) | NZ709208A (ru) |
| RU (1) | RU2675817C2 (ru) |
| WO (1) | WO2014096737A1 (ru) |
| ZA (1) | ZA201503735B (ru) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6098639B2 (ja) * | 2012-07-25 | 2017-03-22 | 旭硝子株式会社 | 着色ガラス |
| CN108675643B (zh) * | 2018-07-03 | 2022-01-11 | 泰山玻璃纤维有限公司 | 基于铁锰钛的高模量玻璃纤维组合物 |
| CN108751728B (zh) | 2018-07-03 | 2019-04-02 | 泰山玻璃纤维有限公司 | 基于玄武岩生产的高模量玻璃纤维组合物 |
| CN108516691B (zh) * | 2018-07-03 | 2019-03-19 | 泰山玻璃纤维有限公司 | 利用氧化铁、氧化锰和氧化钛提高模量的玻璃纤维组合物 |
| KR102233027B1 (ko) * | 2019-08-19 | 2021-03-29 | 조성훈 | 광물 섬유용 조성물 |
| FR3104568B1 (fr) * | 2019-12-11 | 2022-07-22 | Saint Gobain Isover | Procede de fabrication de laine minerale |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3348956A (en) | 1965-12-30 | 1967-10-24 | Johns Manville | Refractory fiber composition |
| GB1459178A (en) | 1972-11-21 | 1976-12-22 | Dostal K V | Glass and glass-ceramics and compositions therefor |
| JPS5627456B2 (ru) * | 1973-07-19 | 1981-06-25 | ||
| JPS605539B2 (ja) * | 1980-03-17 | 1985-02-12 | 日東紡績株式会社 | 耐アルカリ性、耐熱性無機質繊維 |
| DE3017374C1 (de) * | 1980-05-07 | 1982-08-26 | Eglasstrek Patent Promotion & Awarding GmbH, 6203 Hochheim | Vorrichtung zur Herstellung von Glasfasern |
| US4376598A (en) * | 1981-04-06 | 1983-03-15 | The United States Of America As Represented By The United States Department Of Energy | In-situ vitrification of soil |
| US4396722A (en) * | 1982-04-05 | 1983-08-02 | Owens-Corning Fiberglas Corporation | Wool glass composition |
| JPH0651579B2 (ja) * | 1986-07-25 | 1994-07-06 | 日本電気硝子株式会社 | 磁気ヘツド封着用ガラス |
| SU1512936A1 (ru) * | 1987-07-14 | 1989-10-07 | Предприятие П/Я В-2268 | Стекло |
| JPH01298041A (ja) * | 1988-05-24 | 1989-12-01 | Miyawaki Gureizu Kogyo Kk | 陶器瓦用銀色釉 |
| FR2652078B1 (fr) * | 1989-09-18 | 1992-05-22 | Saint Gobain Rech | Procede d'elaboration d'un verre destine a etre transforme en fibres continues ou discontinues. |
| SK284033B6 (sk) | 1991-08-02 | 2004-08-03 | Isover Saint-Gobain | Minerálna vlna z roztaveného minerálneho materiálu, spôsob jej výroby a zariadenie na vykonávanie tohto spôsobu |
| US5188649A (en) * | 1991-08-07 | 1993-02-23 | Pedro Buarque de Macedo | Process for vitrifying asbestos containing waste, infectious waste, toxic materials and radioactive waste |
| JPH09269098A (ja) * | 1996-04-01 | 1997-10-14 | General Shoko:Kk | 被覆管 |
| AU2445397A (en) * | 1996-04-09 | 1997-10-29 | Vortec Corporation | Manufacture of ceramic tiles from fly ash |
| US5776845A (en) | 1996-12-09 | 1998-07-07 | Ford Motor Company | High transmittance green glass with improved UV absorption |
| US6001494A (en) * | 1997-02-18 | 1999-12-14 | Technology Partners Inc. | Metal-ceramic composite coatings, materials, methods and products |
| US5807417A (en) * | 1997-07-11 | 1998-09-15 | Ford Motor Company | Nitrate-free method for manufacturing a blue glass composition |
| BR9806062A (pt) * | 1997-07-22 | 1999-08-31 | Saint Gobain Isover | Forno para a preparação de vidro por fusão elétrica, processo de fusão elétrica de vidro, e, instalação de fabricação de lã de vidro. |
| ES2163900T5 (es) | 1997-12-02 | 2011-03-18 | Rockwool International A/S | Producción de fibras vítreas artificiales. |
| UA74802C2 (en) * | 1999-12-06 | 2006-02-15 | Rgs90 | A process for producing glass, glass produced by this method and use thereof |
| US6998361B2 (en) * | 2002-03-04 | 2006-02-14 | Glass Incorporated | High temperature glass fiber insulation |
| EP1558533B1 (en) * | 2002-11-06 | 2018-01-10 | Rockwool International A/S | Processes of forming mineral fibres |
| FR2883866B1 (fr) * | 2005-04-01 | 2007-05-18 | Saint Gobain Isover Sa | Laine minerale, produit isolant et procede de fabrication |
| EA021658B1 (ru) * | 2009-07-13 | 2015-08-31 | Роквул Интернэшнл А/С | Минеральные волокна и их применение |
| MY159835A (en) * | 2010-04-12 | 2017-02-15 | Usg Interiors Llc | Mineral wool from recyclable materials |
| CN101851064A (zh) | 2010-06-23 | 2010-10-06 | 浮山县晋盛新型建筑材料有限责任公司 | 一种蓝色微晶玻璃及其制备方法 |
| AT509991B1 (de) * | 2010-12-22 | 2012-01-15 | Asamer Basaltic Fibers Gmbh | Rohmaterial zur herstellung von basaltfasern |
| PL2697178T3 (pl) * | 2011-04-13 | 2020-03-31 | Rockwool International A/S | Procesy kształtowania sztucznych włókien szklistych |
| EA025519B1 (ru) * | 2011-12-16 | 2016-12-30 | Роквул Интернэшнл А/С | Композиция расплава для изготовления искусственных стекловидных волокон |
-
2012
- 2012-12-21 FR FR1262642A patent/FR3000056B1/fr active Active
-
2013
- 2013-12-20 US US14/654,189 patent/US10000404B2/en active Active
- 2013-12-20 AU AU2013366120A patent/AU2013366120A1/en not_active Abandoned
- 2013-12-20 JP JP2015548738A patent/JP6382837B2/ja active Active
- 2013-12-20 KR KR1020157015960A patent/KR102199540B1/ko active IP Right Grant
- 2013-12-20 CA CA2893455A patent/CA2893455C/fr active Active
- 2013-12-20 CN CN201380066969.2A patent/CN104854053B/zh active Active
- 2013-12-20 DK DK13821881.3T patent/DK2935138T3/da active
- 2013-12-20 NZ NZ709208A patent/NZ709208A/en unknown
- 2013-12-20 EP EP13821881.3A patent/EP2935138B1/fr active Active
- 2013-12-20 WO PCT/FR2013/053223 patent/WO2014096737A1/fr active Application Filing
- 2013-12-20 RU RU2015129704A patent/RU2675817C2/ru active
- 2013-12-20 BR BR112015011860-7A patent/BR112015011860B1/pt active IP Right Grant
-
2015
- 2015-05-26 ZA ZA2015/03735A patent/ZA201503735B/en unknown
-
2017
- 2017-08-11 AU AU2017213544A patent/AU2017213544B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| DK2935138T3 (da) | 2021-06-28 |
| KR20150100662A (ko) | 2015-09-02 |
| WO2014096737A1 (fr) | 2014-06-26 |
| CN104854053A (zh) | 2015-08-19 |
| CA2893455C (fr) | 2021-06-15 |
| NZ709208A (en) | 2017-11-24 |
| ZA201503735B (en) | 2016-04-28 |
| CA2893455A1 (fr) | 2014-06-26 |
| AU2017213544A1 (en) | 2017-08-31 |
| JP2016501822A (ja) | 2016-01-21 |
| US10000404B2 (en) | 2018-06-19 |
| BR112015011860A2 (pt) | 2017-07-11 |
| JP6382837B2 (ja) | 2018-08-29 |
| FR3000056B1 (fr) | 2016-03-25 |
| AU2013366120A1 (en) | 2015-07-16 |
| FR3000056A1 (fr) | 2014-06-27 |
| RU2675817C2 (ru) | 2018-12-25 |
| AU2017213544B2 (en) | 2019-08-29 |
| EP2935138B1 (fr) | 2021-04-28 |
| BR112015011860B1 (pt) | 2021-07-27 |
| EP2935138A1 (fr) | 2015-10-28 |
| CN104854053B (zh) | 2019-04-16 |
| KR102199540B1 (ko) | 2021-01-08 |
| US20150315068A1 (en) | 2015-11-05 |
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