RU2014123398A - Способ изготовления прозрачного керамического предмета при помощи гранулирования в псевдоожиженном слое - Google Patents
Способ изготовления прозрачного керамического предмета при помощи гранулирования в псевдоожиженном слое Download PDFInfo
- Publication number
- RU2014123398A RU2014123398A RU2014123398/03A RU2014123398A RU2014123398A RU 2014123398 A RU2014123398 A RU 2014123398A RU 2014123398/03 A RU2014123398/03 A RU 2014123398/03A RU 2014123398 A RU2014123398 A RU 2014123398A RU 2014123398 A RU2014123398 A RU 2014123398A
- Authority
- RU
- Russia
- Prior art keywords
- ceramic powder
- carried out
- ceramic
- dispersion
- granulate
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
- C04B35/111—Fine ceramics
- C04B35/115—Translucent or transparent products
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/44—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/44—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminates
- C04B35/443—Magnesium aluminate spinel
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/58—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
- C04B35/581—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on aluminium nitride
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/6261—Milling
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/62625—Wet mixtures
- C04B35/6263—Wet mixtures characterised by their solids loadings, i.e. the percentage of solids
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/62645—Thermal treatment of powders or mixtures thereof other than sintering
- C04B35/62655—Drying, e.g. freeze-drying, spray-drying, microwave or supercritical drying
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/62695—Granulation or pelletising
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
- C04B35/645—Pressure sintering
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
- C04B35/645—Pressure sintering
- C04B35/6455—Hot isostatic pressing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
- C04B2235/3225—Yttrium oxide or oxide-forming salts thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5427—Particle size related information expressed by the size of the particles or aggregates thereof millimeter or submillimeter sized, i.e. larger than 0,1 mm
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5436—Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5445—Particle size related information expressed by the size of the particles or aggregates thereof submicron sized, i.e. from 0,1 to 1 micron
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/604—Pressing at temperatures other than sintering temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/608—Green bodies or pre-forms with well-defined density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/76—Crystal structural characteristics, e.g. symmetry
- C04B2235/762—Cubic symmetry, e.g. beta-SiC
- C04B2235/764—Garnet structure A3B2(CO4)3
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/77—Density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9646—Optical properties
- C04B2235/9653—Translucent or transparent ceramics other than alumina
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
1. Способ изготовления прозрачного керамического предмета с реальным линейным пропусканием RIT>10% в области длин волн от 300 нм до 4000 нм при толщине стенки этого керамического предмета 2 мм, отличающийся следующими стадиями процесса:получение шликера путем дисперигирования керамического порошка, который имеет размер частиц d<5 мкм, предпочтительно между 5 нм и 500 нм,получение из этого шликера гранулята, который имеет размер частиц d<1 мм, предпочтительно между 50 мкм и 500 мкм, более предпочтительно между 80 мкм и 300 мкм, при помощи гранулирования в псевдоожиженном слое,простое, нециклическое прессование гранулята с получением необожженной заготовки,спекание необожженной заготовки с получением спеченного изделия, ипоследующее уплотнение спеченного изделия.2. Способ по п. 1, отличающийся тем, что дисперигирование керамического порошка осуществляется с водой и поверхностно-активными веществами.3. Способ по п. 1, отличающийся тем, что при диспергировании осуществляется размалывание керамического порошка.4. Способ по одному из пп. 1-3, отличающийся тем, что дисперигирование и размалывание керамического порошка осуществляется в бисерной мельнице.5. Способ по п. 1, отличающийся тем, что необожженная заготовка формуется при помощи одноосного и/или холодного изостатического прессования.6. Способ по п. 1, отличающийся тем, что последующее уплотнение осуществляется при помощи горячего изостатического прессования (HIP).7. Способ по п. 1, отличающийся тем, что спеченное изделие шлифуется и полируется до оптического качества.
Claims (7)
1. Способ изготовления прозрачного керамического предмета с реальным линейным пропусканием RIT>10% в области длин волн от 300 нм до 4000 нм при толщине стенки этого керамического предмета 2 мм, отличающийся следующими стадиями процесса:
получение шликера путем дисперигирования керамического порошка, который имеет размер частиц d50<5 мкм, предпочтительно между 5 нм и 500 нм,
получение из этого шликера гранулята, который имеет размер частиц d50<1 мм, предпочтительно между 50 мкм и 500 мкм, более предпочтительно между 80 мкм и 300 мкм, при помощи гранулирования в псевдоожиженном слое,
простое, нециклическое прессование гранулята с получением необожженной заготовки,
спекание необожженной заготовки с получением спеченного изделия, и
последующее уплотнение спеченного изделия.
2. Способ по п. 1, отличающийся тем, что дисперигирование керамического порошка осуществляется с водой и поверхностно-активными веществами.
3. Способ по п. 1, отличающийся тем, что при диспергировании осуществляется размалывание керамического порошка.
4. Способ по одному из пп. 1-3, отличающийся тем, что дисперигирование и размалывание керамического порошка осуществляется в бисерной мельнице.
5. Способ по п. 1, отличающийся тем, что необожженная заготовка формуется при помощи одноосного и/или холодного изостатического прессования.
6. Способ по п. 1, отличающийся тем, что последующее уплотнение осуществляется при помощи горячего изостатического прессования (HIP).
7. Способ по п. 1, отличающийся тем, что спеченное изделие шлифуется и полируется до оптического качества.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102011086100.9 | 2011-11-10 | ||
DE102011086100 | 2011-11-10 | ||
PCT/EP2012/072344 WO2013068576A1 (de) | 2011-11-10 | 2012-11-12 | Verfahren zur herstellung transparenter keramikgegenstände mittels wirbelschichtgranulation |
Publications (1)
Publication Number | Publication Date |
---|---|
RU2014123398A true RU2014123398A (ru) | 2015-12-20 |
Family
ID=47143935
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
RU2014123398/03A RU2014123398A (ru) | 2011-11-10 | 2012-11-12 | Способ изготовления прозрачного керамического предмета при помощи гранулирования в псевдоожиженном слое |
Country Status (11)
Country | Link |
---|---|
US (1) | US20140374931A1 (ru) |
EP (1) | EP2776378A1 (ru) |
JP (1) | JP2015501775A (ru) |
KR (1) | KR20140103938A (ru) |
CN (1) | CN104220397A (ru) |
BR (1) | BR112014011382A8 (ru) |
DE (1) | DE102012220518A1 (ru) |
IL (1) | IL232543A0 (ru) |
IN (1) | IN2014CN04217A (ru) |
RU (1) | RU2014123398A (ru) |
WO (1) | WO2013068576A1 (ru) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2016021346A1 (ja) * | 2014-08-08 | 2016-02-11 | 信越化学工業株式会社 | 透明セラミックスの製造方法 |
CN105732011A (zh) * | 2014-12-10 | 2016-07-06 | 辽宁利永盛新材料有限公司 | 一种新型多功能硅藻土陶粒的制备方法 |
WO2018174814A1 (en) * | 2017-03-23 | 2018-09-27 | Dso National Laboratories | A protective material |
CN109836089A (zh) * | 2017-11-27 | 2019-06-04 | 辽宁法库陶瓷工程技术研究中心 | 一种多功能免烧型呼吸砖的制备方法 |
CN112299828A (zh) * | 2020-11-09 | 2021-02-02 | 新沂市锡沂高新材料产业技术研究院有限公司 | 一种应用于5g太阳能手机的透明陶瓷背板的制备方法 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4761390A (en) * | 1987-02-02 | 1988-08-02 | Raytheon Company | Optically transparent yttrium oxide |
JP2620287B2 (ja) * | 1988-03-09 | 1997-06-11 | 住友電気工業株式会社 | 透光性スピネル焼結体の製造方法 |
DD274980A1 (de) * | 1988-08-29 | 1990-01-10 | Leuna Werke Veb | Verfahren zur herstellung sphaerischer formlinge |
DE4304809A1 (de) * | 1993-02-17 | 1994-08-18 | Glatt Ingtech Gmbh | Verfahren zur Herstellung von feinkeramischem Preßgranulat mittels Wirbelschichtgranulationstrocknung |
DE19602525A1 (de) * | 1996-01-25 | 1997-08-07 | Starck H C Gmbh Co Kg | Sphärische Keramikformkörper, Verfahren zu ihrer Herstellung sowie deren Verwendung |
US6878456B2 (en) | 2001-12-28 | 2005-04-12 | 3M Innovative Properties Co. | Polycrystalline translucent alumina-based ceramic material, uses, and methods |
DE102004004259B3 (de) | 2004-01-23 | 2005-11-24 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Transparente polykristalline Sinterkeramik kubischer Kristallstruktur |
DE102007059091A1 (de) | 2007-12-07 | 2009-06-10 | ETEC Gesellschaft für technische Keramik mbH | Verfahren zur Herstellung einer polykristallinen transparenten Keramik |
DE102009035501B4 (de) * | 2009-07-30 | 2016-06-02 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | α-Al2O3-Sintermaterial und Verfahren zur Herstellung eines hochdichten und feinstkristallinen Formkörpers aus diesem Material sowie dessen Verwendung |
FR2954766B1 (fr) * | 2009-12-24 | 2015-04-24 | Saint Gobain Ct Recherches | Poudre de granules de ceramique |
US20140360345A1 (en) * | 2011-11-07 | 2014-12-11 | Ceramtec-Etec Gmbh | Transparent ceramic material |
WO2014096142A1 (de) * | 2012-12-19 | 2014-06-26 | Ceramtec-Etec Gmbh | Keramikwerkstoff |
-
2012
- 2012-11-12 US US14/357,472 patent/US20140374931A1/en not_active Abandoned
- 2012-11-12 CN CN201280066625.7A patent/CN104220397A/zh active Pending
- 2012-11-12 JP JP2014540497A patent/JP2015501775A/ja active Pending
- 2012-11-12 KR KR1020147015766A patent/KR20140103938A/ko not_active Application Discontinuation
- 2012-11-12 WO PCT/EP2012/072344 patent/WO2013068576A1/de active Application Filing
- 2012-11-12 EP EP12783242.6A patent/EP2776378A1/de not_active Withdrawn
- 2012-11-12 RU RU2014123398/03A patent/RU2014123398A/ru not_active Application Discontinuation
- 2012-11-12 DE DE102012220518A patent/DE102012220518A1/de not_active Withdrawn
- 2012-11-12 BR BR112014011382A patent/BR112014011382A8/pt not_active Application Discontinuation
-
2014
- 2014-05-11 IL IL232543A patent/IL232543A0/en unknown
- 2014-06-05 IN IN4217CHN2014 patent/IN2014CN04217A/en unknown
Also Published As
Publication number | Publication date |
---|---|
BR112014011382A2 (pt) | 2017-06-13 |
EP2776378A1 (de) | 2014-09-17 |
KR20140103938A (ko) | 2014-08-27 |
US20140374931A1 (en) | 2014-12-25 |
IL232543A0 (en) | 2014-06-30 |
BR112014011382A8 (pt) | 2017-06-20 |
DE102012220518A1 (de) | 2013-05-16 |
JP2015501775A (ja) | 2015-01-19 |
IN2014CN04217A (ru) | 2015-07-17 |
CN104220397A (zh) | 2014-12-17 |
WO2013068576A1 (de) | 2013-05-16 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
RU2014123398A (ru) | Способ изготовления прозрачного керамического предмета при помощи гранулирования в псевдоожиженном слое | |
Ghanizadeh et al. | Improved transparency and hardness in α-alumina ceramics fabricated by high-pressure SPS of nanopowders | |
Lallemant et al. | Transparent polycrystalline alumina obtained by SPS: Green bodies processing effect | |
WO2013181018A3 (en) | Method of fabricating high light transmission zirconia blanks for milling into natural appearance dental appliances | |
CN104341129B (zh) | 具有透水性的混凝土路面砖及其制备方法 | |
KR102123925B1 (ko) | 기공 함유 불투명 석영 유리의 제조 방법 | |
JP2010047460A (ja) | 透明セラミック及びその製造方法ならびにその透明セラミックスを用いた光学素子 | |
US10023795B2 (en) | Ceramic composite systems and method | |
JP2014088309A (ja) | 透明セスキオキサイド焼結体の製造方法及びその製造方法により製造された透明セスキオキサイド焼結体 | |
Alhaji et al. | Development of synthesis and granulation process of MgAl2O4 powder for the fabrication of transparent ceramic | |
Sun et al. | Gelcasting and reactive sintering of sheet-like YAG transparent ceramics | |
JP2014088286A (ja) | 不透明石英ガラスおよびその製造方法 | |
JP7022817B2 (ja) | セラミック構造体 | |
ES2584849T3 (es) | Procedimiento para la producción de un material cerámico transparente policristalino mediante un prensado cíclico | |
TWI743081B (zh) | 陶瓷成型品及透明燒結體之製造方法 | |
JP6341284B2 (ja) | 透明セラミックスの製造方法 | |
TWI530475B (zh) | 陶瓷體及其製備方法及應用該陶瓷體的電子裝置 | |
JP5477715B2 (ja) | 高度に透明なアルミナセラミック及びその製造方法 | |
CN104108933B (zh) | 一种高致密度钒酸铋陶瓷的制备方法 | |
JP5493419B2 (ja) | ZnS焼結体、ZnS焼結体群および光学部材、ならびにその製造方法 | |
Moghim et al. | Hot-pressing of bimodally distributed magnesium fluoride powder | |
Promdej et al. | Effect of hot isostatically pressed sintering on microstructure of translucent alumina compact | |
KR101357286B1 (ko) | 알루미나 성형체의 제조 방법 | |
CN106096492A (zh) | 一种指纹识别装置 | |
Kaiser et al. | Optimized shaping process for transparent spinel ceramic |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
FA92 | Acknowledgement of application withdrawn (lack of supplementary materials submitted) |
Effective date: 20170327 |