RO79038B - Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei - Google Patents

Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei

Info

Publication number
RO79038B
RO79038B RO96069A RO9606978A RO79038B RO 79038 B RO79038 B RO 79038B RO 96069 A RO96069 A RO 96069A RO 9606978 A RO9606978 A RO 9606978A RO 79038 B RO79038 B RO 79038B
Authority
RO
Romania
Prior art keywords
sodium
phosphonomethylglycine
preparation
mol
phosphonomethylglicine
Prior art date
Application number
RO96069A
Other languages
English (en)
Other versions
RO79038A (ro
Original Assignee
Monsanto Company
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Company filed Critical Monsanto Company
Publication of RO79038A publication Critical patent/RO79038A/ro
Publication of RO79038B publication Critical patent/RO79038B/ro

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/38Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813N-Phosphonomethylglycine; Salts or complexes thereof

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Dentistry (AREA)
  • Engineering & Computer Science (AREA)
  • Plant Pathology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Agronomy & Crop Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

Conform prezentei inventii, procedeul pentru prepararea unei sari de sodiu a N-fosfonometilglicinei, în care raportul molar între cationul de sodiu si anion reprezinta între 1,5 si 1, este caracterizat prin aceea ca, în scopul obtinerii unui complex cristalizat continînd amestecul sarurilor mono si disodice, N-fosfonometilglicina se neutralizeaza cu o solutie apoasa alcalina cu continut de sodiu, aleasa dintre hidroxid, carbonat, bicarbonat, sulfit, bisulfit, sulfura, formiat, acetat, silicat, cantitatea de baza fiind astfel aleasa încît sa reprezinte între 1,25 si 1,75 mol sodiu/mol, N-fosfonometilglicina, eventual amestecul de reactie se încalzeste pentru îndepartarea produselor secundare nedorite si apoi se usuca sarea de sodiu obtinuta.
RO96069A 1978-01-03 1978-12-27 Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei RO79038B (ro)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/866,677 US4140513A (en) 1978-01-03 1978-01-03 Sodium sesquiglyphosate

Publications (2)

Publication Number Publication Date
RO79038A RO79038A (ro) 1984-10-31
RO79038B true RO79038B (ro) 1984-11-30

Family

ID=25348146

Family Applications (2)

Application Number Title Priority Date Filing Date
RO96069A RO79038B (ro) 1978-01-03 1978-12-27 Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei
RO78115568A RO89365A (ro) 1978-01-03 1978-12-27 Compozitie solida erbicida si de reglare a cresterii plantelor

Family Applications After (1)

Application Number Title Priority Date Filing Date
RO78115568A RO89365A (ro) 1978-01-03 1978-12-27 Compozitie solida erbicida si de reglare a cresterii plantelor

Country Status (41)

Country Link
US (1) US4140513A (ro)
JP (1) JPS54109921A (ro)
AR (1) AR221857A1 (ro)
AT (1) AT363274B (ro)
AU (1) AU522518B2 (ro)
BE (1) BE873199A (ro)
BG (2) BG29424A3 (ro)
BR (1) BR7900007A (ro)
CA (1) CA1120951A (ro)
CH (1) CH641187A5 (ro)
CS (1) CS207728B2 (ro)
DD (1) DD140968A5 (ro)
DE (1) DE2900025C2 (ro)
DK (1) DK158356C (ro)
EG (1) EG13903A (ro)
ES (1) ES476485A1 (ro)
FI (1) FI65437C (ro)
FR (1) FR2413398A1 (ro)
GB (1) GB2011906B (ro)
HK (1) HK684A (ro)
HU (1) HU184659B (ro)
IE (1) IE47773B1 (ro)
IL (1) IL56356A (ro)
IN (1) IN150741B (ro)
IT (1) IT1162701B (ro)
KE (1) KE3342A (ro)
MW (1) MW179A1 (ro)
MX (1) MX5697E (ro)
MY (1) MY8400322A (ro)
NL (1) NL7812635A (ro)
NO (1) NO150841C (ro)
PH (1) PH19009A (ro)
PL (2) PL119534B1 (ro)
PT (1) PT69016A (ro)
RO (2) RO79038B (ro)
SE (1) SE444685B (ro)
SG (1) SG54883G (ro)
SU (1) SU1050565A3 (ro)
YU (1) YU310178A (ro)
ZA (1) ZA787349B (ro)
ZM (1) ZM279A1 (ro)

Families Citing this family (50)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4481026A (en) * 1982-11-16 1984-11-06 Stauffer Chemical Company Aluminum N-phosphonomethylglycine and its use as a herbicide
US4472189A (en) * 1982-12-27 1984-09-18 Stauffer Chemical Co. Stannic N-phosphonomethyglycine and its use as a herbicide
FI86501C (fi) * 1985-05-29 1992-09-10 Stauffer Chemical Co Fast, i huvudsak icke-hygroskopisk fytoaktiv blandning och dess framstaellningsfoerfarande.
US5580841A (en) * 1985-05-29 1996-12-03 Zeneca Limited Solid, phytoactive compositions and method for their preparation
US5468718A (en) * 1985-10-21 1995-11-21 Ici Americas Inc. Liquid, phytoactive compositions and method for their preparation
BR8600460A (pt) * 1986-02-04 1987-09-01 Monsanto Brasil Processo para preparacao de um sal de metal alcalino particulado de n-fosfonometilglicina
US5047079A (en) * 1986-08-18 1991-09-10 Ici Americas Inc. Method of preparation and use of solid, phytoactive compositions
NZ231897A (en) 1988-12-30 1992-09-25 Monsanto Co Dry water-soluble granular composition comprising glyphosate and a liquid surfactant
DK165156C (da) * 1989-12-20 1993-03-01 Cheminova Agro As Herbicid formulering indeholdende glyphosatsyre
DE4029304A1 (de) * 1990-09-15 1992-03-19 Hoechst Ag Synergistische herbizide mittel
US6930075B1 (en) 1990-11-02 2005-08-16 Monsanto Technology, Llc Fatty acid-based herbicidal composition
IL101539A (en) 1991-04-16 1998-09-24 Monsanto Europe Sa Non-hygroscopic mono-ammonium salts of n-phosphonomethyl glycine derivatives their preparation and pesticidal compositons containing them
MY111437A (en) * 1992-07-31 2000-05-31 Monsanto Co Improved glyphosate herbicide formulation.
DE19533523A1 (de) * 1995-09-11 1997-03-13 Bayer Ag Verwendung von N-Phosphonomethyl-glycinestern in wäßriger Lösung als Herbizide
EA200000150A1 (ru) * 1997-07-22 2000-10-30 Монсанто Компани Составы, содержащие аммонний-глифосат в высокой концентрации
AU746589B2 (en) * 1997-07-30 2002-05-02 Monsanto Company Process and compositions promoting biological effectiveness of exogenous chemical substances in plants
ITTO980048A1 (it) * 1998-01-20 1999-07-20 Ipici Spa Composizioni erbicide, procedimenti per la loro preparazione ed impieghi
NZ506254A (en) * 1998-02-13 2002-10-25 Monsanto Co Liquid herbicide composition, applied to plant foliage, containing siloxane surfactant to enhance biological effectiveness of herbicide
GB9819693D0 (en) 1998-09-10 1998-11-04 Zeneca Ltd Glyphosate formulation
CA2351437C (en) 1998-11-23 2011-05-24 Monsanto Co. Compact storage and shipping system for glyphosate herbicide
KR20010104684A (ko) 1998-11-23 2001-11-26 죤 에이치. 뷰센 고농축 수성 글리포세이트 조성물
CA2352099C (en) 1998-11-30 2008-01-15 Monsanto Technology Llc Promoting biological effectiveness of exogenous chemical substances in plants
US6369001B1 (en) 1999-08-11 2002-04-09 Monsanto Technology, Llc Microemulsion coformulation of a graminicide and a water-soluble herbicide
US6746976B1 (en) 1999-09-24 2004-06-08 The Procter & Gamble Company Thin until wet structures for acquiring aqueous fluids
JP5433120B2 (ja) 1999-09-30 2014-03-05 モンサント テクノロジー エルエルシー 向上した安定性を有するパッケージミックス農薬組成物
US6992045B2 (en) * 2000-05-19 2006-01-31 Monsanto Technology Llc Pesticide compositions containing oxalic acid
US7135437B2 (en) 2000-05-19 2006-11-14 Monsanto Technology Llc Stable liquid pesticide compositions
MY158895A (en) 2000-05-19 2016-11-30 Monsanto Technology Llc Potassium glyphosate formulations
US6300323B1 (en) 2000-08-08 2001-10-09 Ishihara Sangyo Kaisha, Ltd. (Poly)ethereal ammonium salts of herbicides bearing acidic moieties and their use as herbicides
DE10052489A1 (de) 2000-10-23 2002-05-02 Hermania Dr Schirm Gmbh Feste Glyphosat-Formulierung und Verfahren zur Herstellung
EP1494534A4 (en) * 2002-04-01 2005-08-17 Valent Biosciences Corp IMPROVED HERBICIDE COMPOSITION
WO2004019684A2 (en) * 2002-08-31 2004-03-11 Monsanto Technology Llc Process for the preparation of a dry pesticidal composition containing a dicarbodylate component
US20050037924A1 (en) * 2002-08-31 2005-02-17 Monsanto Technology Llc Sodium glyphosate compositions and process for their preparation
US8470741B2 (en) * 2003-05-07 2013-06-25 Croda Americas Llc Homogeneous liquid saccharide and oil systems
AU2005287122B2 (en) * 2004-09-17 2012-09-27 Monsanto Technology Llc Glyphosate formulations with early burndown symptoms
US7223718B2 (en) * 2005-03-07 2007-05-29 Falcon Lab Llc Enhanced glyphosate herbicidal concentrates
US20070049498A1 (en) * 2005-09-01 2007-03-01 Brigance Mickey R Agricultural compositions which enhance performance of herbicides
AU2009260813B2 (en) * 2008-06-18 2013-10-10 Stepan Company Ultra-high loading glyphosate concentrate
DK2337452T3 (en) 2008-07-03 2014-12-15 Monsanto Technology Llc COMBINATION OF derivatized SACCHARIDSURFAKTANTER AND ETHERAMINOXIDSURFAKTANTER AS HERBICIDADJUVANTER
CN102215695B (zh) * 2008-09-29 2014-10-08 孟山都技术公司 包含酰胺基烷基胺表面活性剂的草甘膦制剂
US9233993B2 (en) 2009-06-30 2016-01-12 Monsanto Technology Llc N-phosphonomethylglycine guanidine derivative salts
US20110071027A1 (en) * 2009-09-18 2011-03-24 Volker Heide High strength aqueous glyphosate salt concentrates and methods
BR112012011625B1 (pt) 2009-11-16 2018-10-02 Imtrade Australia Pty Ltd formulações de glifosato de carga elevada e processo de preparação das mesmas
AU2011323770B2 (en) 2010-10-25 2015-07-16 Stepan Company Glyphosate formulations based on compositions derived from natural oil metathesis
EP3164004B1 (en) 2014-07-02 2019-09-18 Stepan Company Agricultural compositions with reduced aquatic toxicity
WO2017196951A1 (en) 2016-05-11 2017-11-16 Monsanto Technology Llc Glyphosate formulations containing amidoalkylamine surfactants
WO2018031610A1 (en) 2016-08-09 2018-02-15 Monsanto Technology Llc Solid herbicidal concentrate compositions
EP3628738A1 (en) 2018-09-25 2020-04-01 KWS SAAT SE & Co. KGaA Method for controlling weed beets and other weeds
EP3628160A1 (en) 2018-09-25 2020-04-01 KWS SAAT SE & Co. KGaA Use of glyphosate herbicide for controlling unwanted vegetation in beta vulgaris growing areas
CN116574129B (zh) * 2023-04-14 2025-04-25 湖北泰盛化工有限公司 一种消除细晶的草甘膦结晶方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL38138A (en) * 1970-11-19 1974-07-31 Ciba Geigy Ag Process and compositions containing thiourea derivatives for the promotion of fruit abscission
PH16509A (en) * 1971-03-10 1983-11-08 Monsanto Co N-phosphonomethylglycine phytotoxicant composition
US3799758A (en) * 1971-08-09 1974-03-26 Monsanto Co N-phosphonomethyl-glycine phytotoxicant compositions
US3853530A (en) * 1971-03-10 1974-12-10 Monsanto Co Regulating plants with n-phosphonomethylglycine and derivatives thereof

Also Published As

Publication number Publication date
DK158356C (da) 1990-10-01
IE47773B1 (en) 1984-06-13
SG54883G (en) 1984-07-27
ES476485A1 (es) 1979-11-16
PL114405B1 (en) 1981-01-31
YU310178A (en) 1983-09-30
PH19009A (en) 1985-12-03
FI790006A7 (fi) 1979-07-04
DK158356B (da) 1990-05-07
NO790009L (no) 1979-07-04
SU1050565A3 (ru) 1983-10-23
KE3342A (en) 1983-11-25
DK979A (da) 1979-07-04
EG13903A (en) 1982-09-30
NL7812635A (nl) 1979-07-05
NO150841C (no) 1985-01-09
JPS54109921A (en) 1979-08-29
AT363274B (de) 1981-07-27
CH641187A5 (de) 1984-02-15
BE873199A (fr) 1979-06-29
MX5697E (es) 1983-12-15
FR2413398B1 (ro) 1984-06-15
CS207728B2 (en) 1981-08-31
DE2900025C2 (de) 1984-08-16
RO89365A (ro) 1986-05-30
PL212563A1 (pl) 1979-10-22
SE444685B (sv) 1986-04-28
PT69016A (en) 1979-02-01
JPS6238358B2 (ro) 1987-08-17
GB2011906B (en) 1982-06-30
HU184659B (en) 1984-09-28
MW179A1 (en) 1980-03-12
BR7900007A (pt) 1979-08-07
AR221857A1 (es) 1981-03-31
IT1162701B (it) 1987-04-01
NO150841B (no) 1984-09-17
HK684A (en) 1984-01-13
DE2900025A1 (de) 1979-07-12
IN150741B (ro) 1982-12-04
IE790010L (en) 1979-07-03
BG29424A3 (bg) 1980-11-14
RO79038A (ro) 1984-10-31
FI65437B (fi) 1984-01-31
SE7900016L (sv) 1979-09-06
AU4304779A (en) 1979-07-12
GB2011906A (en) 1979-07-18
FR2413398A1 (fr) 1979-07-27
US4140513A (en) 1979-02-20
IL56356A0 (en) 1979-03-12
ZA787349B (en) 1979-12-27
IL56356A (en) 1982-09-30
FI65437C (fi) 1984-05-10
CA1120951A (en) 1982-03-30
PL119534B1 (en) 1982-01-30
IT7919009A0 (it) 1979-01-02
DD140968A5 (de) 1980-04-09
ZM279A1 (en) 1980-10-21
ATA1179A (de) 1980-12-15
BG40656A3 (bg) 1987-01-15
MY8400322A (en) 1984-12-31
AU522518B2 (en) 1982-06-10

Similar Documents

Publication Publication Date Title
RO79038B (ro) Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei
GB1284136A (en) Exothermic compositions and heat collars containing said compositions
ZA755925B (en) Manufacture of concentrated aqueous solutions of formaldehyde
GB1295540A (ro)
MD225B1 (ro) Procedeu de obtinere a formei hidratate cristaline a sarii de sodiu a acidului 3-acetoximetil-7-[2(2-amino-4-tiazolil-2-metoxiiminoacetamido]-cef-3-em-4-carbonic a sin-izomerului
GB1527473A (en) Production of 3,3-dimethyl-2-hydroxy-butyric acid and its salts
ES539151A0 (es) Procedimiento de blanqueo de pastas papeleras quimicas por peroxido de hidrogeno
ES445893A1 (es) Procedimiento para la preparacion de hidrato de polihidrixi-fulfato de aluminio.
JPS5325646A (en) Method of preparing aqueous slurry of calcium carbonate for paper coating
GB1260198A (en) Alkali metal oxide and alkaline earth metal oxide source material
GB1282868A (en) Glass-making batches
BE831611A (fr) Procede pour l'extraction de carbonate de guanidine a partir de solutions aqueuses diluees
JPS52139695A (en) Production of calcium peroxide
SU138232A1 (ru) Способ получени бромистых солей
ES414870A1 (es) Procedimiento de preparacion de nuevos derivados de la 6- alfa-metilprednisolona.
ES441319A1 (es) Procedimiento para preparar granulos conteniendo carbonato calcico.
GB999487A (en) Set-retarded calcium sulphate hemihydrate
ES392494A3 (es) Procedimiento continuo para la fabricacion de sales alcali-nas del acido dicloroisocianurico.
ES391184A1 (es) Un procedimiento para la produccion de anhidridos arilen- sulfonicos.
JPS5622628A (en) Novel aluminum hydroxide gel, its manufacture and utilization
Wéber et al. Recent Results of Conductivity Investigations on Aluminate Liquors in Alumina Works
ES481140A1 (es) Procedimiento de obtencion de trimetilolpropano.
JPS5542249A (en) Production of calcium potassium silicate
RO81751B1 (ro) Procedeu de preparare a clorhidratului acidului iminodiacetic
BR7605996A (pt) Processo para obtencao de sulfato de sodio anidrico(na2so4)a partir de sal de glauber (na2so10h2o)