RO79038B - Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei - Google Patents

Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei

Info

Publication number
RO79038B
RO79038B RO96069A RO9606978A RO79038B RO 79038 B RO79038 B RO 79038B RO 96069 A RO96069 A RO 96069A RO 9606978 A RO9606978 A RO 9606978A RO 79038 B RO79038 B RO 79038B
Authority
RO
Romania
Prior art keywords
sodium
phosphonomethylglycine
preparation
mol
phosphonomethylglicine
Prior art date
Application number
RO96069A
Other languages
English (en)
Other versions
RO79038A (ro
Original Assignee
Monsanto Company
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Company filed Critical Monsanto Company
Publication of RO79038A publication Critical patent/RO79038A/ro
Publication of RO79038B publication Critical patent/RO79038B/ro

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/38Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813N-Phosphonomethylglycine; Salts or complexes thereof

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Dentistry (AREA)
  • Engineering & Computer Science (AREA)
  • Plant Pathology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Agronomy & Crop Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

Conform prezentei inventii, procedeul pentru prepararea unei sari de sodiu a N-fosfonometilglicinei, în care raportul molar între cationul de sodiu si anion reprezinta între 1,5 si 1, este caracterizat prin aceea ca, în scopul obtinerii unui complex cristalizat continînd amestecul sarurilor mono si disodice, N-fosfonometilglicina se neutralizeaza cu o solutie apoasa alcalina cu continut de sodiu, aleasa dintre hidroxid, carbonat, bicarbonat, sulfit, bisulfit, sulfura, formiat, acetat, silicat, cantitatea de baza fiind astfel aleasa încît sa reprezinte între 1,25 si 1,75 mol sodiu/mol, N-fosfonometilglicina, eventual amestecul de reactie se încalzeste pentru îndepartarea produselor secundare nedorite si apoi se usuca sarea de sodiu obtinuta.
RO96069A 1978-01-03 1978-12-27 Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei RO79038B (ro)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/866,677 US4140513A (en) 1978-01-03 1978-01-03 Sodium sesquiglyphosate

Publications (2)

Publication Number Publication Date
RO79038A RO79038A (ro) 1984-10-31
RO79038B true RO79038B (ro) 1984-11-30

Family

ID=25348146

Family Applications (2)

Application Number Title Priority Date Filing Date
RO78115568A RO89365A (ro) 1978-01-03 1978-12-27 Compozitie solida erbicida si de reglare a cresterii plantelor
RO96069A RO79038B (ro) 1978-01-03 1978-12-27 Procedeu pentru prepararea unei sari de sodiu a n-fosfonometilglicinei

Family Applications Before (1)

Application Number Title Priority Date Filing Date
RO78115568A RO89365A (ro) 1978-01-03 1978-12-27 Compozitie solida erbicida si de reglare a cresterii plantelor

Country Status (41)

Country Link
US (1) US4140513A (ro)
JP (1) JPS54109921A (ro)
AR (1) AR221857A1 (ro)
AT (1) AT363274B (ro)
AU (1) AU522518B2 (ro)
BE (1) BE873199A (ro)
BG (2) BG40656A3 (ro)
BR (1) BR7900007A (ro)
CA (1) CA1120951A (ro)
CH (1) CH641187A5 (ro)
CS (1) CS207728B2 (ro)
DD (1) DD140968A5 (ro)
DE (1) DE2900025C2 (ro)
DK (1) DK158356C (ro)
EG (1) EG13903A (ro)
ES (1) ES476485A1 (ro)
FI (1) FI65437C (ro)
FR (1) FR2413398A1 (ro)
GB (1) GB2011906B (ro)
HK (1) HK684A (ro)
HU (1) HU184659B (ro)
IE (1) IE47773B1 (ro)
IL (1) IL56356A (ro)
IN (1) IN150741B (ro)
IT (1) IT1162701B (ro)
KE (1) KE3342A (ro)
MW (1) MW179A1 (ro)
MX (1) MX5697E (ro)
MY (1) MY8400322A (ro)
NL (1) NL7812635A (ro)
NO (1) NO150841C (ro)
PH (1) PH19009A (ro)
PL (2) PL114405B1 (ro)
PT (1) PT69016A (ro)
RO (2) RO89365A (ro)
SE (1) SE444685B (ro)
SG (1) SG54883G (ro)
SU (1) SU1050565A3 (ro)
YU (1) YU310178A (ro)
ZA (1) ZA787349B (ro)
ZM (1) ZM279A1 (ro)

Families Citing this family (50)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4481026A (en) * 1982-11-16 1984-11-06 Stauffer Chemical Company Aluminum N-phosphonomethylglycine and its use as a herbicide
US4472189A (en) * 1982-12-27 1984-09-18 Stauffer Chemical Co. Stannic N-phosphonomethyglycine and its use as a herbicide
KR860008713A (ko) * 1985-05-29 1986-12-18 죤 알. 페넬 고체식물 훨성조성물 및 그 제조방법
US5580841A (en) * 1985-05-29 1996-12-03 Zeneca Limited Solid, phytoactive compositions and method for their preparation
US5468718A (en) * 1985-10-21 1995-11-21 Ici Americas Inc. Liquid, phytoactive compositions and method for their preparation
BR8600460A (pt) * 1986-02-04 1987-09-01 Monsanto Brasil Processo para preparacao de um sal de metal alcalino particulado de n-fosfonometilglicina
US5047079A (en) * 1986-08-18 1991-09-10 Ici Americas Inc. Method of preparation and use of solid, phytoactive compositions
NZ231897A (en) 1988-12-30 1992-09-25 Monsanto Co Dry water-soluble granular composition comprising glyphosate and a liquid surfactant
DK165156C (da) * 1989-12-20 1993-03-01 Cheminova Agro As Herbicid formulering indeholdende glyphosatsyre
DE4029304A1 (de) * 1990-09-15 1992-03-19 Hoechst Ag Synergistische herbizide mittel
US6930075B1 (en) 1990-11-02 2005-08-16 Monsanto Technology, Llc Fatty acid-based herbicidal composition
IL101539A (en) 1991-04-16 1998-09-24 Monsanto Europe Sa Non-hygroscopic mono-ammonium salts of n-phosphonomethyl glycine derivatives their preparation and pesticidal compositons containing them
MY111437A (en) * 1992-07-31 2000-05-31 Monsanto Co Improved glyphosate herbicide formulation.
DE19533523A1 (de) * 1995-09-11 1997-03-13 Bayer Ag Verwendung von N-Phosphonomethyl-glycinestern in wäßriger Lösung als Herbizide
WO1999004635A1 (en) * 1997-07-22 1999-02-04 Monsanto Company High-loaded ammonium glyphosate formulations
NZ502499A (en) * 1997-07-30 2001-11-30 Monsanto Co Herbicide consisting of glyphosate composition and polyamine derivatives
ITTO980048A1 (it) * 1998-01-20 1999-07-20 Ipici Spa Composizioni erbicide, procedimenti per la loro preparazione ed impieghi
WO1999040785A1 (en) * 1998-02-13 1999-08-19 Monsanto Company Storage-stable composition containing exogenous chemical substance and siloxane surfactant
GB9819693D0 (en) 1998-09-10 1998-11-04 Zeneca Ltd Glyphosate formulation
CZ304306B6 (cs) 1998-11-23 2014-02-26 Monsanto Technology Llc Vysoce koncentrované vodné glyfosátové kompozice
ES2552540T3 (es) 1998-11-23 2015-11-30 Monsanto Technology Llc Sistema de almacenamiento y transporte compacto para herbicida glifosato
EP1135024B1 (en) 1998-11-30 2004-12-29 Flamel Technologies Promoting biological effectiveness of exogenous chemical substances in plants
US6369001B1 (en) 1999-08-11 2002-04-09 Monsanto Technology, Llc Microemulsion coformulation of a graminicide and a water-soluble herbicide
US6746976B1 (en) 1999-09-24 2004-06-08 The Procter & Gamble Company Thin until wet structures for acquiring aqueous fluids
JP5433120B2 (ja) 1999-09-30 2014-03-05 モンサント テクノロジー エルエルシー 向上した安定性を有するパッケージミックス農薬組成物
US7135437B2 (en) 2000-05-19 2006-11-14 Monsanto Technology Llc Stable liquid pesticide compositions
MY158895A (en) * 2000-05-19 2016-11-30 Monsanto Technology Llc Potassium glyphosate formulations
US6992045B2 (en) 2000-05-19 2006-01-31 Monsanto Technology Llc Pesticide compositions containing oxalic acid
US6300323B1 (en) 2000-08-08 2001-10-09 Ishihara Sangyo Kaisha, Ltd. (Poly)ethereal ammonium salts of herbicides bearing acidic moieties and their use as herbicides
DE10052489A1 (de) 2000-10-23 2002-05-02 Hermania Dr Schirm Gmbh Feste Glyphosat-Formulierung und Verfahren zur Herstellung
RU2318384C2 (ru) * 2002-04-01 2008-03-10 Вэйлент Байосайенсиз Копэрейшн Гербицидная композиция и способ контроля роста растений
US20050037924A1 (en) * 2002-08-31 2005-02-17 Monsanto Technology Llc Sodium glyphosate compositions and process for their preparation
BR0314096A (pt) * 2002-08-31 2005-07-12 Monsanto Technology Llc Processo para a preparação de uma composição pesticida seca contendo um sal solúvel em água de ácido glifosato e um componente dicarboxilato
US8470741B2 (en) * 2003-05-07 2013-06-25 Croda Americas Llc Homogeneous liquid saccharide and oil systems
BRPI0515552A (pt) * 2004-09-17 2008-07-29 Monsanto Technology Llc formulações de glifosato com sintomas de queimação precoce
US7223718B2 (en) * 2005-03-07 2007-05-29 Falcon Lab Llc Enhanced glyphosate herbicidal concentrates
US20070049498A1 (en) * 2005-09-01 2007-03-01 Brigance Mickey R Agricultural compositions which enhance performance of herbicides
BRPI0914226B1 (pt) * 2008-06-18 2021-01-19 Stepan Company concentrado contendo sal de glifosato de carga ultra alta, método para fabricação do mesmo e método para controlar vegetação indesejada
BRPI0915368B1 (pt) 2008-07-03 2019-01-15 Monsanto Technology Llc composição compreendendo glifosato ou um sal ou um ester de glifosato e método de controlar crescimento de planta
HUE035603T2 (en) 2008-09-29 2018-05-28 Monsanto Technology Llc Glyphosate preparations containing amidoalkylamine surfactants
AR080540A1 (es) 2009-06-30 2012-04-18 Monsanto Technology Llc Sales de n- fosfonometil glicina y derivados de guanidina y una composicion herbicida
US20110071027A1 (en) * 2009-09-18 2011-03-24 Volker Heide High strength aqueous glyphosate salt concentrates and methods
CA2779734C (en) 2009-11-16 2016-12-20 Imtrade Australia Pty Ltd High load glyphosate formulations
CA2815668C (en) 2010-10-25 2018-02-27 Stepan Company Glyphosate formulations based on compositions derived from natural oil metathesis
EP3164004B1 (en) 2014-07-02 2019-09-18 Stepan Company Agricultural compositions with reduced aquatic toxicity
CA3022682C (en) 2016-05-11 2025-11-18 Monsanto Technology Llc GLYPHOSATE FORMULATIONS CONTAINING AMIDOALKYLAMINE SURFACTANTS
AR109317A1 (es) 2016-08-09 2018-11-21 Monsanto Technology Llc Composiciones de concentrados herbicidas sólidos
EP3628738A1 (en) 2018-09-25 2020-04-01 KWS SAAT SE & Co. KGaA Method for controlling weed beets and other weeds
EP3628160A1 (en) 2018-09-25 2020-04-01 KWS SAAT SE & Co. KGaA Use of glyphosate herbicide for controlling unwanted vegetation in beta vulgaris growing areas
CN116574129B (zh) * 2023-04-14 2025-04-25 湖北泰盛化工有限公司 一种消除细晶的草甘膦结晶方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL38138A (en) * 1970-11-19 1974-07-31 Ciba Geigy Ag Process and compositions containing thiourea derivatives for the promotion of fruit abscission
US3853530A (en) * 1971-03-10 1974-12-10 Monsanto Co Regulating plants with n-phosphonomethylglycine and derivatives thereof
US3799758A (en) * 1971-08-09 1974-03-26 Monsanto Co N-phosphonomethyl-glycine phytotoxicant compositions
PH16509A (en) * 1971-03-10 1983-11-08 Monsanto Co N-phosphonomethylglycine phytotoxicant composition

Also Published As

Publication number Publication date
GB2011906B (en) 1982-06-30
PL119534B1 (en) 1982-01-30
GB2011906A (en) 1979-07-18
DK979A (da) 1979-07-04
FR2413398A1 (fr) 1979-07-27
MX5697E (es) 1983-12-15
US4140513A (en) 1979-02-20
BG40656A3 (bg) 1987-01-15
KE3342A (en) 1983-11-25
CS207728B2 (en) 1981-08-31
DE2900025C2 (de) 1984-08-16
NO790009L (no) 1979-07-04
AT363274B (de) 1981-07-27
IE47773B1 (en) 1984-06-13
AU522518B2 (en) 1982-06-10
EG13903A (en) 1982-09-30
BR7900007A (pt) 1979-08-07
CA1120951A (en) 1982-03-30
PL212563A1 (pl) 1979-10-22
ZM279A1 (en) 1980-10-21
ZA787349B (en) 1979-12-27
JPS54109921A (en) 1979-08-29
BG29424A3 (bg) 1980-11-14
YU310178A (en) 1983-09-30
JPS6238358B2 (ro) 1987-08-17
BE873199A (fr) 1979-06-29
FI790006A7 (fi) 1979-07-04
PH19009A (en) 1985-12-03
IT7919009A0 (it) 1979-01-02
HK684A (en) 1984-01-13
DE2900025A1 (de) 1979-07-12
FI65437C (fi) 1984-05-10
DK158356C (da) 1990-10-01
RO89365A (ro) 1986-05-30
PT69016A (en) 1979-02-01
SG54883G (en) 1984-07-27
ATA1179A (de) 1980-12-15
ES476485A1 (es) 1979-11-16
NO150841C (no) 1985-01-09
IL56356A (en) 1982-09-30
IE790010L (en) 1979-07-03
NO150841B (no) 1984-09-17
SE7900016L (sv) 1979-09-06
FR2413398B1 (ro) 1984-06-15
DK158356B (da) 1990-05-07
AR221857A1 (es) 1981-03-31
DD140968A5 (de) 1980-04-09
AU4304779A (en) 1979-07-12
PL114405B1 (en) 1981-01-31
MW179A1 (en) 1980-03-12
IN150741B (ro) 1982-12-04
FI65437B (fi) 1984-01-31
IL56356A0 (en) 1979-03-12
RO79038A (ro) 1984-10-31
MY8400322A (en) 1984-12-31
SU1050565A3 (ru) 1983-10-23
CH641187A5 (de) 1984-02-15
SE444685B (sv) 1986-04-28
NL7812635A (nl) 1979-07-05
HU184659B (en) 1984-09-28
IT1162701B (it) 1987-04-01

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