PH12019050018A1 - A composite soap and preparation method - Google Patents
A composite soap and preparation method Download PDFInfo
- Publication number
- PH12019050018A1 PH12019050018A1 PH12019050018A PH12019050018A PH12019050018A1 PH 12019050018 A1 PH12019050018 A1 PH 12019050018A1 PH 12019050018 A PH12019050018 A PH 12019050018A PH 12019050018 A PH12019050018 A PH 12019050018A PH 12019050018 A1 PH12019050018 A1 PH 12019050018A1
- Authority
- PH
- Philippines
- Prior art keywords
- parts
- soap
- composite
- weight
- composite soap
- Prior art date
Links
- 239000000344 soap Substances 0.000 title claims abstract description 86
- 239000002131 composite material Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title abstract description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 28
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 16
- 239000000194 fatty acid Substances 0.000 claims abstract description 16
- 229930195729 fatty acid Natural products 0.000 claims abstract description 16
- 239000011734 sodium Substances 0.000 claims abstract description 16
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 16
- 235000011187 glycerol Nutrition 0.000 claims abstract description 14
- -1 sodium fatty acid Chemical class 0.000 claims abstract description 14
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 13
- 239000003240 coconut oil Substances 0.000 claims abstract description 13
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 12
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 12
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000008117 stearic acid Substances 0.000 claims abstract description 12
- 239000002738 chelating agent Substances 0.000 claims abstract description 9
- 239000000945 filler Substances 0.000 claims abstract description 8
- 238000004898 kneading Methods 0.000 claims description 19
- 238000002156 mixing Methods 0.000 claims description 17
- 238000003756 stirring Methods 0.000 claims description 17
- 239000000284 extract Substances 0.000 claims description 14
- 240000007651 Rubus glaucus Species 0.000 claims description 12
- 235000011034 Rubus glaucus Nutrition 0.000 claims description 12
- 235000009122 Rubus idaeus Nutrition 0.000 claims description 12
- 229920001353 Dextrin Polymers 0.000 claims description 10
- 239000004375 Dextrin Substances 0.000 claims description 10
- 235000019425 dextrin Nutrition 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- 238000000227 grinding Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 4
- 238000005360 mashing Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- DDAQLPYLBPPPRV-UHFFFAOYSA-N [4-(hydroxymethyl)-2-oxo-1,3,2lambda5-dioxaphosphetan-2-yl] dihydrogen phosphate Chemical group OCC1OP(=O)(OP(O)(O)=O)O1 DDAQLPYLBPPPRV-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- 235000010216 calcium carbonate Nutrition 0.000 claims description 2
- 239000000378 calcium silicate Substances 0.000 claims description 2
- 229910052918 calcium silicate Inorganic materials 0.000 claims description 2
- 235000012241 calcium silicate Nutrition 0.000 claims description 2
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 claims description 2
- 229920001451 polypropylene glycol Polymers 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims 1
- 238000005187 foaming Methods 0.000 abstract description 6
- 239000008233 hard water Substances 0.000 abstract description 6
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 230000001954 sterilising effect Effects 0.000 abstract description 3
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 3
- 244000052616 bacterial pathogen Species 0.000 abstract description 2
- 239000013078 crystal Substances 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000006260 foam Substances 0.000 description 11
- 239000003814 drug Substances 0.000 description 9
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 description 9
- 239000007788 liquid Substances 0.000 description 7
- 239000011324 bead Substances 0.000 description 6
- 241000894006 Bacteria Species 0.000 description 4
- 244000025254 Cannabis sativa Species 0.000 description 4
- 229940079593 drug Drugs 0.000 description 4
- 238000010030 laminating Methods 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 241000282326 Felis catus Species 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 108010087806 Carnosine Proteins 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 239000004166 Lanolin Substances 0.000 description 2
- 241001562712 Muhlenbergia rigens Species 0.000 description 2
- CQOVPNPJLQNMDC-UHFFFAOYSA-N N-beta-alanyl-L-histidine Natural products NCCC(=O)NC(C(O)=O)CC1=CN=CN1 CQOVPNPJLQNMDC-UHFFFAOYSA-N 0.000 description 2
- 235000009308 Rhexia virginica Nutrition 0.000 description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 229940039717 lanolin Drugs 0.000 description 2
- 235000019388 lanolin Nutrition 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 2
- 229920001817 Agar Polymers 0.000 description 1
- 240000002791 Brassica napus Species 0.000 description 1
- 235000004977 Brassica sinapistrum Nutrition 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- QRYRORQUOLYVBU-VBKZILBWSA-N Carnosic acid Natural products CC([C@@H]1CC2)(C)CCC[C@]1(C(O)=O)C1=C2C=C(C(C)C)C(O)=C1O QRYRORQUOLYVBU-VBKZILBWSA-N 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 241001092459 Rubus Species 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- CQOVPNPJLQNMDC-ZETCQYMHSA-N carnosine Chemical compound [NH3+]CCC(=O)N[C@H](C([O-])=O)CC1=CNC=N1 CQOVPNPJLQNMDC-ZETCQYMHSA-N 0.000 description 1
- 229940044199 carnosine Drugs 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003974 emollient agent Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 229940079776 sodium cocoyl isethionate Drugs 0.000 description 1
- 239000008234 soft water Substances 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/18—Water-insoluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/267—Organic compounds, e.g. vitamins containing oxygen containing free fatty acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/34—Organic compounds, e.g. vitamins containing phosphorus
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Abstract
The invention discloses a composite soap which is composed of the following parts by weight:30-50 parts of sodium fatty acid, 10-20 parts of stearic acid, 3-8 parts of coconut oil, 1-3 parts of glycerin, and a chelating agent 0.1-0.5 parts, 10-30 parts of filler. The composite soap of the invention has a good foaming performance, good sterilization effect, can kill a variety of pathogenic bacteria, has strong resistance to hard water, and is not easy to produce soap scale, and the addition of chelating agent contributes to the formation of a beneficial crystal form of the soap, so that the soap is used. It is slippery and does not easily adhere to the wall of the container. The preparation method of the invention is simple and easy, and has a wide source of raw materials, and is suitable for large-scale industrial application.
Description
(3) The milled soap piece is placed into a vacuum plodder for vacuum beading, the outlet temperature of the bead is controlled at 42 © C, and the temperature of the laminating machine is controlled at 8 © C; (4) The long soap body pressed out by the plodder directly enters the printer to print, and the formed soap body is obtained. When printing, the temperature of the mold is -15 °C.
Experimental Example 1:
Refer to GB/T 7462-94 for foam performance determination. The surface layer of the sample was scraped 2 mm, the inner layer soap was taken, and the samples of Examples 1-4 were weighed, and the solution of mass fraction of 0.08 was prepared by using 3 mmol/LCa2+ hard water, and placed in a water bath at 52 ° C to maintain a constant temperature at 50 © C. The foam height of the samples was measured at 30 s and 10 min. Each group of samples was measured three times, and the results of three measurements were the final results. The foam height at 30 s was taken as the foaming index of the sample, and the foam height at 10 min was taken as the foam stability index of the sample. Then, the pH value of the sample at the mass concentration at room temperature was measured.
The measurement results are shown in Table 1:
Table 1 Foam and pH of soap bars test group 30sFoam heightmm | 10minFoam pH value heightmmmm * Significant (P<0.05)
It can be seen from Table 1 that the 30s foam height of Example 2 and the foam height of 10 minutes are significantly higher than that of Example 1, and other conditions are the same as in Example 1, except that the gray raspberry extract is added to Example 2, It was proved that the gray raspberry extract had a promoting effect on the foaming performance of the composite soap; in Example 3, compared with Example 1, the p H value was significantly reduced, the 30 s foam height, and the 10 min foam height were not significantly different, compared with Example 1. The other conditions are the same. Only the extract of
Xing'an Raspberry has been added in Example 3. It proves that Xing'an Rapeseed extract has no promoting effect on the foaming performance of the composite soap, and can significantly reduce the p H value, which is not conducive to skin care and emollient.
Experimental Example 2:
The composite soaps prepared in Examples 1-4 were prepared, and 10 g of each group was ground and ground to prepare a solution having a mass fraction of 0.4, which was a test drug.
Select Staphylococcus aureus (ATCC25923) and Escherichia coli (441490), inoculate them in nutrient broth medium, incubate at 37 °C for 18 h, take 11 sterile tubes, and add 1 ml of nutrient broth liquid medium to the first tube. 1ml of each tube, take 0.4ml of the test drug diluent into the first tube, mix and take 1ml to the second tube, dilute in order, take 10ml out of the 10th tube, discard the 11th tube without adding liquid Control. 0.1 ml of the diluted bacterial solution was added to each tube, and cultured at 37 ° C for 24 hours. Remove and observe the growth of the bacteria. If the liquid medicine tube is turbid, it means that the bacteria grows, and the test drug has no bacteriostatic effect; if the liquid medicine tube is clear, it means that the growth of the bacteria is inhibited, and the liquid of the maximum dilution which can inhibit the growth of the bacteria is the minimum of the drug. Inhibitory concentration (MIC). The tubes of the clear liquid broth were transferred to the broth agar plate and cultured for 24 hours. The
A composite soap and preparation method—# & 5 EB RH HS 77%
Claim of Priority
This application claims priority from China provisional Patent Application
Serial No. CN CN201810551820.8, filed May 31, 2018, currently pending.
The invention belongs to the technical field of solid soap preparation, and in particular relates to a multifunctional composite soap and a preparation method.
The solid soap is classified into a complex soap in which a solid soap and a soap having a sodium fatty acid sodium as a main active ingredient are blended with a surfactant other than sodium fatty acid. After long-term use and development, solid soap has excellent decontamination and washing performance in soft water, rich in foam, good wettability, mild performance, easy to degrade, and less impact on the environment. At the same time, it also found many shortcomings, such as poor low-temperature solubility, which in turn affects its low-temperature detergency; poor resistance to hard water, and in the hard water, it will synthesize insoluble and non-washing calcium with Ca2+ and Mg2+.
Magnesium metal soap, which removes some of the soap from washing power, and the resulting metal soap mixes with the dirt to form an objectionable soap scum, which is adsorbed on the washed fabric and the container, making the fabric difficult to rinse, causing the fabric to be yellowish and hard. Brittle fracture, reduced density.
Patent 201310704666.0 discloses a traditional Chinese medicine liquid soap consisting of 40-60 parts of sodium lauryl sulfate, 6-10 parts of lanolin, 2-4 parts of Luxian grass and 2-4 parts of cat grass. The preparation steps are as follows: taking deer grass and cat grass, and boiling water twice, the first time adding water is 8-12 times the weight of the medicine, boiling for 1-2 hours, and the second adding water is 6-10 of the weight of the medicine. Double the amount, boil for 1-2h, combine the decoction, concentrate to 10 times the total weight of deer grass and cat grass, add sodium lauryl sulfate, lanolin, melt at 70- 80 °C, that is. Patent 201410674325.8 discloses a neutral moisturizing cleansing soap comprising the following parts by weight: 40-60 parts of sodium cocoyl isethionate; fatty acid 3-10 Parts; 5-20 parts of fatty alcohol; 0.2-2 parts of glycerin; 0.1-0.5 parts of chelating agent; 20-40 parts of filler; 5-15 parts of water.
The pH value is between 4.5 and 6.5, which is close to the weak acid environment of human skin. It can avoid the skin irritation during the washing process, and there is no sand grain feeling. The soap body is not easy to be smashed in water.
However, the above soap has poor foaming performance, poor sterilization effect, poor resistance to hard water, and easy to produce soap scale.
The object of the present invention is to provide a multifunctional composite soap and a preparation method thereof.
A composite soap consisting of the following parts by weight: 30-50 parts of sodium fatty acid, 10-20 parts of stearic acid, 3-8 parts of coconut oil, 1-3 parts of glycerin, 0.1-0.5 parts of chelating agent, Filler 10-30 parts.
The chelating agent is one or more of hydroxyethylidene diphosphate, 1- decene-8-0l acetate, polyoxypropylene glycol, and tetrasodium ethylenediaminetetraacetate.
The filler is one or more of starch, dextrin, calcium carbonate, and calcium silicate.
The complex soap further comprises 1-3 parts of the gray raspberry extract.
The method for extracting the gray raspberry extract is as follows: taking the gray raspberry leaves, mashing and slurring, adding 3-8 times by weight of water to reflux for 3 times, combining the filtrate, decolorizing the activated carbon, and evaporating and drying. .
The preparation method of the above composite soap is carried out according to the following steps: (1) According to parts by weight, take 30-50 parts of sodium fatty acid, 10-20 parts of stearic acid, 3-8 parts of coconut oil, 1-3 parts of glycerin, 0.1-0.5 parts of chelating agent, 10-30 parts of filler, adding to a kneading machine for conventional soap making, kneading and stirring and mixing uniformly, wherein the stirring time is 12-18 minutes, and the stirring temperature is 35-50 © C, (2) The kneading and mixing of the materials after mixing, adding to the mill, grinding the soap body, the thickness of the milled soap sheet is controlled to be 0.1-0.5 mm; (3) passing the milled soap sheet into a vacuum plodder for vacuum beading; (4) The long soap body pressed out by the plodder directly enters the printer to print, and the formed soap body is obtained.
Step (3) When the vacuum bead is pressed, the outlet temperature of the bead head is controlled at 38-55 ° C, and the temperature of the cooling water of the beading machine is controlled at 3-12 ° C.
When the step (4) is printed, the temperature of the mold is -10 to -20 °C.
The invention has the beneficial effects that the composite soap of the invention has good foaming performance, good sterilization effect, can kill various pathogenic bacteria, has strong resistance to hard water, and is not easy to produce soap scale, and the addition of a chelating agent contributes to the beneficial crystal form of the soap. The resulting soap makes the soap smooth and does not easily adhere to the container wall. The preparation method of the invention is simple and easy, and has a wide source of raw materials, and is suitable for large-scale industrial production.
The invention will be further described below in conjunction with specific embodiments.
Example 1
A composite soap consisting of the following parts by weight: 40 parts of sodium fatty acid, 15 parts of stearic acid, 6 parts of coconut oil, 2 parts of glycerin, 0.3 parts of tetrasodium edetate, and 20 parts of dextrin.
The preparation method of the above composite soap is carried out according to the following steps: (1) According to the parts by weight, take 40 parts of sodium fatty acid, 15 parts of stearic acid, 6 parts of coconut oil, 2 parts of glycerin, 0.3 parts of tetrasodium edetate, 20 parts of dextrin, and added to conventional soap. In the kneading machine, knead and stirred to mix evenly, wherein the stirring time is 15 minutes, and the stirring temperature is 40 ° C; (2) The kneading and mixing of the materials after mixing, adding to the mill, grinding the soap body, the thickness of the milled soap sheet is controlled to 0.3 mm; (3) The milled soap piece is placed into a vacuum plodder for vacuum beading, the outlet temperature of the bead is controlled at 42 ° C, and the temperature of the laminating machine is controlled at 8 © C; (4) The long soap body pressed out by the plodder directly enters the printer to print, and the formed soap body is obtained. When printing, the temperature of the mold is -15 °C.
Example 2
A composite soap consisting of the following parts by weight: 40 parts of sodium fatty acid, 15 parts of stearic acid, 6 parts of coconut oil, 2 parts of glycerin, 0.3 parts of tetrasodium edetate, 20 parts of dextrin, 2 pieces of gray raspberry extract.
The method for extracting the gray raspberry extract is as follows: taking the gray raspberry leaves, mashing and slurring, adding 6 times by weight of water to reflux for 3 times, combining the filtrate, decolorizing the activated carbon, and evaporating and drying.
The preparation method of the above composite soap is carried out according to the following steps: (1) According to parts by weight, take 40 parts of sodium fatty acid, 15 parts of stearic acid, 6 parts of coconut oil, 2 parts of glycerin, 0.3 parts of tetrasodium edetate, 20 parts of dextrin, and 2 extracts of gray raspberry a portion, added to a conventional kneading machine for kneading, kneading and stirring and mixing uniformly, wherein the stirring time is 15 minutes, the stirring temperature is 40 ° C; (2) The kneading and mixing of the materials after mixing, adding to the mill, grinding the soap body, the thickness of the milled soap sheet is controlled to 0.3 mm; (3) The milled soap piece is placed into a vacuum plodder for vacuum beading, the outlet temperature of the bead is controlled at 42 © C, and the temperature of the laminating machine is controlled at 8 © C; (4) The long soap body pressed out by the plodder directly enters the printer to print, and the formed soap body is obtained. When printing, the temperature of the mold is -15 °C.
Example 3
A composite soap consisting of the following parts by weight: 40 parts of sodium fatty acid, 15 parts of stearic acid, 6 parts of coconut oil, 2 parts of glycerin, 0.3 parts of tetrasodium edetate, 20 parts of dextrin, Xing'an Rubus extract 2 parts.
The extraction method of the Xing'an stalk extract is: taking Xing'an stalk leaf, mashing, slurrying, adding 6 times by weight of water to reflux for 3 times, combining the filtrate, decolorizing the activated carbon, and evaporating to make.
The preparation method of the above composite soap is carried out according to the following steps: (1) According to the parts by weight, take 40 parts of sodium fatty acid, 15 parts of stearic acid, 6 parts of coconut oil, 2 parts of glycerin, 0.3 parts of tetrasodium edetate, 20 parts of dextrin, Xing'an Raspberry Extract 2 a portion, added to a conventional kneading machine for kneading, kneading and stirring and mixing uniformly, wherein the stirring time is 15 minutes, the stirring temperature is 40 ° C, (2) The kneading and mixing of the materials after mixing, adding to the mill, grinding the soap body, the thickness of the milled soap sheet is controlled to 0.3 mm; (3) The milled soap piece is placed into a vacuum plodder for vacuum beading, the outlet temperature of the bead is controlled at 42 ° C, and the temperature of the laminating machine is controlled at 8 ° C; (4) The long soap body pressed out by the plodder directly enters the printer to print, and the formed soap body is obtained. When printing, the temperature of the mold is -15 °C.
Example 4
A composite soap consisting of the following parts by weight: 40 parts of sodium fatty acid, 15 parts of stearic acid, 6 parts of coconut oil, 2 parts of glycerin, 0.3 parts of tetrasodium edetate, 20 parts of dextrin, 1 part of L- carnosine.
The preparation method of the above composite soap is carried out according to the following steps: (1) According to parts by weight, take 40 parts of sodium fatty acid, 15 parts of stearic acid, 6 parts of coconut oil, 2 parts of glycerin, 0.3 parts of tetrasodium edetate, 20 parts of dextrin and 1 part of L-carnosine. Adding to a kneading machine for conventional soap making, kneading and stirring and mixing uniformly, wherein the stirring time is 15 minutes, and the stirring temperature is 40 ° C; (2) the kneading and mixing of the materials after mixing, adding to the mill, grinding the soap body, the thickness of the milled soap sheet is controlled to 0.3 mm;
Claims (5)
1. A composite soap comprising the following components by weight: 30- 50 parts of sodium fatty acid, 10-20 parts of stearic ; acid, 3-8 parts of coconut oil, 1-3 parts of glycerin, chelated fhe mixture is 0.1-0.5 parts, and the filler is 10-30 parts. (tet cer ty¥ :
2. The composite soap according to claim 1, wherein the chelating agent is hydroxyethylidene diphosphate, 1-decene-8-0l acetate, polyoxypropylene glycol, ethylenediaminetetraacetic acid On or more of tetrasodium.
3. The composite soap according to claim 1, wherein the filler is one or more of starch, dextrin, calcium carbonate, and calcium silicate.
4. The composite soap according to claim 1, wherein the composite soap further comprises 1-3 parts of gray raspberry extract. (Xing'an Raspberry) The composite soap according to claim 4, wherein the gray raspberry extract is extracted by taking gray raspberry leaves, mashing, slurring, adding 3-8 times by weight of water reflux. The mixture was extracted 3 times, and the filtrate was combined, decolorized by activated carbon, and evaporated to dryness.
5. The method for preparing a composite soap according to claim 1, wherein the method comprises the following steps: (1) According to parts by weight, take 30-50 parts of sodium fatty acid, 10-20 parts of stearic acid, 3-8 parts of coconut oil, 1-3 parts of glycerin, 0.1-0.5 parts of chelating agent, 10-30 parts of filler, adding to a kneading machine for conventional soap making, kneading and stirring and mixing uniformly, wherein the stirring time is 12-18 minutes, and the stirring temperature is 35-50 ° C; (2) The kneading and mixing of the materials after mixing, adding to the mill, grinding the soap body, the thickness of the milled soap sheet is controlled to be 0.1-0.5 mm; (3) passing the milled soap sheet into a vacuum plodder for vacuum beading; (4) The long soap body pressed out by the plodder directly enters the printer to print, and the formed soap body is obtained.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810551820.8A CN108774611A (en) | 2018-05-31 | 2018-05-31 | A kind of compound soap and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PH12019050018A1 true PH12019050018A1 (en) | 2019-12-02 |
Family
ID=64028331
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PH12019050018A PH12019050018A1 (en) | 2018-05-31 | 2019-01-23 | A composite soap and preparation method |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN108774611A (en) |
| PH (1) | PH12019050018A1 (en) |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100557006C (en) * | 2007-07-31 | 2009-11-04 | 上海制皂有限公司 | The preparation method of synthetic soap |
| CN104629951B (en) * | 2015-03-03 | 2018-05-04 | 上海制皂有限公司 | Transparent toilet soap |
| CN105540809A (en) * | 2015-12-14 | 2016-05-04 | 潘豪杰 | Heavy metal chelating agent |
| CN107955754A (en) * | 2017-11-20 | 2018-04-24 | 江门市蓬江区新科美日用工艺品厂有限公司 | A kind of antibacterial mite-removing perfumed soap |
-
2018
- 2018-05-31 CN CN201810551820.8A patent/CN108774611A/en active Pending
-
2019
- 2019-01-23 PH PH12019050018A patent/PH12019050018A1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN108774611A (en) | 2018-11-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR20150014742A (en) | saponification of the solution composition and atopic improved method of manfacturing soap | |
| CN110029026A (en) | A kind of sterilizing and itch-relieving medicated soap and preparation method thereof | |
| CN110709059A (en) | Dandruff-removing and itching-relieving shampoo composition containing multi-element zinc | |
| CN107828544A (en) | A kind of production method of the environmental protection ferment of highly effective and safe detergent | |
| CN105420143B (en) | A kind of east acetobacter and its method for producing astragalus polyose | |
| CN103301049A (en) | Andrographis paniculata hand sanitizer and preparation method thereof | |
| CN107375059A (en) | A kind of folium artemisiae argyi anti-drop liquid shampoo and preparation method thereof | |
| PH12019050018A1 (en) | A composite soap and preparation method | |
| CN108179073B (en) | Mild bactericidal laundry detergent and preparation method thereof | |
| CN104984196A (en) | Antibacterial composition containing cortex dictamni and preparation method thereof | |
| KR101300632B1 (en) | Natural supplementary detergent composition and preparation method thereof | |
| TW201010741A (en) | Cosmetic composition for anti-aging of the skin comprising phaseolus radiatus extract of fermentation-enzyme treatment | |
| CN109135974B (en) | Bee venom beauty handmade soap and preparation method thereof | |
| CN110438173A (en) | A kind of preparation method of arachidonic acid emulsion | |
| CN107177643B (en) | Tremella residue fermentation product, skin-care washing product containing fermentation product and preparation method of skin-care washing product | |
| CN105748358A (en) | Aquilaria agallocha essence activating lotion and preparation method thereof | |
| CN110157553A (en) | A kind of high-strength hard water adaptive type washes the dishes salt and preparation method thereof | |
| CN113088413B (en) | Preparation method of handmade soap capable of removing bacterial biofilm | |
| KR20130078929A (en) | Washing agent composition | |
| CN111956558B (en) | Artemisia argyi extract and preparation method and application thereof | |
| CN111053893A (en) | Antibacterial effervescent tablet and preparation method thereof | |
| CN115737706B (en) | Benzalkonium chloride solution and preparation method thereof | |
| CN110051583A (en) | It is a kind of to treat acne mildy wash and preparation method thereof | |
| CN110157552A (en) | A kind of high-effective cleansing of natural green washes the dishes salt and preparation method thereof | |
| CN110724609A (en) | Jatropha curcas oil plant soap base and preparation method thereof |