CN104629951B - Transparent toilet soap - Google Patents
Transparent toilet soap Download PDFInfo
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- CN104629951B CN104629951B CN201510094974.5A CN201510094974A CN104629951B CN 104629951 B CN104629951 B CN 104629951B CN 201510094974 A CN201510094974 A CN 201510094974A CN 104629951 B CN104629951 B CN 104629951B
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Abstract
The present invention discloses a kind of transparent toilet soap, is prepared according to a conventional method by following mass parts raw materials：80 90 parts of neat soap；15 parts of aliphatic acid；15 parts of glycerine；15 parts of sorbierite；28 parts of sucrose；13 parts of polyethylene glycol 400；0 0.12 parts of chelating agent；0 0.10 parts of antioxidant；01 parts of essential oil；03 parts of essence.The present invention uses general goods neat soap, and the raw material scope of application is wider；Used additive is medical grade or food grade, safe and environment-friendly；Product effective active thing content is high, and product durability is strong；Production technology uses conventional toilet soaps production technology, not high to technological requirement, equipment requirement.
Description
Technical field
The present invention relates to a kind of perfumed soap, more particularly to a kind of transparent toilet soap.
Background technology
Perfumed soap is essential washing and nursing article in daily life, based on sodium soap and other surfaces activating agent
Raw material is wanted, adds quality improver and appearance modifying agents, the manufactured product after machine-shaping.
Conventional transparent soap, such as butter, coconut oil, palm oil, also has castor oil using the very shallow grease of concise, color and luster
Deng raw material, the ethanol for making clarifier, glycerine, sucrose etc. are in addition also added.Transparent soap has two kinds of preparation methods：Solvent method and mechanism
Method.Solvent method boils saponification by grease in ethanol water, and soap frame is injected after addition agent, and solid soap is air-dried at room temperature-old
It is made after change.Mechanism method is that soap base is down to 20 DEG C of chillings by 100 DEG C in 2s and obtains neat soap, is added after clarifier through repeatedly milling
Transparent soap is made under control proper temperature.The sodium soap soap content of transparent soap is relatively low, and general 9%~38%.Above method system
The transparent soap obtained is high to technological requirement, and product content of fatty acid is low, and product is not durable.
The content of the invention
The purpose of the present invention is in view of the foregoing defects the prior art has, the technical problem to be solved is that provide one kind
Transparent toilet soap.
A kind of transparent toilet soap provided by the invention, is made of by mass percentage following components：
A kind of transparent toilet soap, is prepared according to a conventional method by following mass parts raw materials：
Preferably, the transparent toilet soap, is prepared according to a conventional method by following mass parts raw materials：
The neat soap, No. CAS：143-19-1,408-35-5, are to use natural animal grease such as tallow oil and natural plants
Oily such as coconut oil, palm oil obtain aliphatic acid by highly pressured hydrolysis after being mixed in a certain ratio and neutralize the sodium soap formed
Salt.
The aliphatic acid, is preferably C12-18 aliphatic acid, such as：Laurate, myristic acid, palmitic acid or sour stearic acid.
The glycerine, No. CAS：56-81-5.It is preferred that pharmaceutical grade glycerine, uses as clarifier and moisturizer in formula.
The sorbierite, No. CAS：56353-15-2.
The sucrose, No. CAS：57-50-1.
The polyethylene glycol 400, No. CAS：25322-68-3.
The essential oil, outer literary fame：Essential oil, essential oil are in the flower from plant, leaf, stem, root or fruit, are led to
Cross the volatile flavor that steam distillation, extrusion, cold-maceration or solvent extraction method refine extraction.
The essence, essence is often used using the industry.In formula, can as needed can be corresponding with unrestricted choice
Essence.
The chelating agent, metallic atom or ion with containing two or even two or more coordination atom ligand effect give birth to
Into the complex compound with cyclic structure.Including phosphoric acid salt, such as sodium tripolyphosphate, sodium pyrophosphate, calgon；Hydramine
Class, such as monoethanolamine, diethanol amine, triethanolamine；Aminocarboxylate, such as sodium ammonium triacetate (NTA), edetate
(EDETATE SODIUM or four sodium), diethylenetriamine pentacarboxylic acid salt (DTPA) etc.；Hydroxycarboxylate, such as tartaric acid, heptose hydrochlorate, grape
Sodium saccharate, sodium alginate etc.；Organic phosphonate, as ethylenediamine tetraacetic methene sodium phosphate, diethylene triamine pentamethylene phosphonic salt, it is double-
1,6- hexamethylene triamine pentamethylene phosphonic acids and hexamethylene diamine tetramethylene phosphonic acid etc..
Preferably, the chelating agent is double-four methylene of 1,6- hexamethylene triamine pentamethylene phosphonic acids and hexamethylene diamine
The mixture of base phosphonic acids, double -1,6- hexamethylene triamine pentamethylene phosphonic acids and hexamethylene diamine tetramethylene phosphonic acid mass ratio
For 3:1-1:3.
Double -1,6- hexamethylene triamine pentamethylene phosphonic acids, No. CAS：34690-00-1.Hexamethylene diamine tetramethylene phosphine
Acid, No. CAS：23605-74-5.
The antioxidant, using the common antioxidant of the industry, such as 2,6- di-tert-butyl-4-methy phenol
(BHT)。
The transparent toilet soap of the present invention can use the general soapmaking step of conventional toilet soaps to be prepared.Specifically, it can take
Following step：
1) spice is kneaded：Each raw material is added to kneading in kneading machine to be uniformly mixed；
2) mill：Progress soap body in grinding mill is added to mill；
3) vacuum press strip：Add progress vacuum press strip in vacuum plodder；
4) print：The printing shaping in printer.
The advantages of technical solution of the present invention, is mainly reflected in following several respects：Using general goods neat soap, raw material is applicable in model
Enclose wider；Used additive is medical grade or food grade, safe and environment-friendly；Product effective active thing content is high, and product is durable
Property is strong；Production technology uses conventional toilet soaps production technology, not high to technological requirement, equipment requirement.
Embodiment
The present invention is specifically described below by embodiment, it is necessary to which indicated herein is that following embodiments are only used
It is further described in the present invention, it is impossible to be interpreted as limiting the scope of the invention.The people that is skilled in technique in the field
Member can make the present invention some nonessential modifications and adaptations according to the content of the invention described above.
Embodiment 1-4
Embodiment 1-4 data, which are corresponded to, by table 1 weighs each raw material.
(a) each raw material is added in the kneading machine of conventional soapmaking, kneading is uniformly mixed, and is stirred 12 minutes, is stirred
Temperature is mixed as 55 DEG C；
(b) the thing section after being uniformly mixed will be mediated, added in grinding mill, carried out soap body and mill, the soap flakes after milling
Thickness control is at 0.4 millimeter；
(c) by the soap flakes after milling, into vacuum plodder, vacuum press strip, wherein press strip big gun head outlet temperature control are carried out
For system at 50 DEG C, plodder leads to cooling water temperature control at 3 DEG C；
(d) the strip soap body that plodder extrudes is directly entered printer printing, obtains molding soap body, wherein mould during printing
The temperature of tool is at -10 DEG C.
It can obtain the transparent toilet soap of the present invention.
Table 1：Transparent toilet soap composition of raw materials list position：Kilogram
| Component | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Neat soap | 85 | 85 | 85 | 85 |
| Laurate | 3 | 3 | 3 | 3 |
| Glycerine | 3 | 3 | 3 | 3 |
| Sorbierite | 3 | 3 | 3 | 3 |
| Sucrose | 5 | 5 | 5 | 5 |
| Polyethylene glycol 400 | 2 | 2 | 2 | 2 |
| Double -1,6- hexamethylene triamines pentamethylene phosphonic acids | - | 0.05 | 1 | - |
| Hexamethylene diamine tetramethylene phosphonic acid | - | 0.05 | - | 1 |
The grease formula of neat soap is：85wt% tallow oils and 15wt% coconut oil, content of fatty acid is 69% in neat soap.
Test case 1：Foam is tested
Transparent toilet soap is dissolved in the water, soap lye solubility 1wt% is configured, at 25 DEG C, by professional standard QB/T 2486-
5.5 measure foaming power in 2008 laundry soap.5min foams are higher, show that foam performance is better.
Table 2:Foam test data table
| Foaming power, (5min)/ml | |
| Embodiment 1 | 325 |
| Embodiment 2 | 380 |
| Embodiment 3 | 340 |
| Embodiment 4 | 350 |
Test case 2：Transparency is tested
With reference to transparency assay method in QB/T 2485-2008 perfumed soap professional standards.Survey soap flakes transparency (6.50 ±
0.15mm cuts into slices), the higher transparency of data is better.
Table 3:Transparency test data table
| Transparency, % | |
| Embodiment 1 | 30 |
| Embodiment 2 | 35 |
| Embodiment 3 | 31 |
| Embodiment 4 | 32 |
Comparing embodiment 1 and embodiment 2-4, chelating agent pair -1,6- hexamethylene triamine pentamethylene phosphonic acids and/or six methylenes
The addition of base diamines tetramethylene phosphonic acid, can lift the foam performance and transparency of perfumed soap.
Comparing embodiment 2 and embodiment 3-4, it is sub- using chelating agent pair -1,6- hexamethylene triamine pentamethylene phosphonic acids and six
The foam performance and transparency of methanediamine tetramethylene phosphonic acid compounding are better than using the foam performance of single chelating agent and transparent
Degree.
Claims (2)
1. a kind of transparent toilet soap, is prepared according to a conventional method by following mass parts raw materials：
The chelating agent is the mixing of double -1,6- hexamethylene triamine pentamethylene phosphonic acids and hexamethylene diamine tetramethylene phosphonic acid
Thing, double -1, the 6- hexamethylene triamine pentamethylene phosphonic acids and hexamethylene diamine tetramethylene phosphonic acid mass ratio are 3:1-1:
3。
2. transparent toilet soap as claimed in claim 1, it is characterised in that the aliphatic acid is laurate, myristic acid, palmitic acid
Or stearic acid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510094974.5A CN104629951B (en) | 2015-03-03 | 2015-03-03 | Transparent toilet soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510094974.5A CN104629951B (en) | 2015-03-03 | 2015-03-03 | Transparent toilet soap |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104629951A CN104629951A (en) | 2015-05-20 |
| CN104629951B true CN104629951B (en) | 2018-05-04 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510094974.5A Active CN104629951B (en) | 2015-03-03 | 2015-03-03 | Transparent toilet soap |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105296234B (en) * | 2015-11-09 | 2018-08-31 | 重庆琥珀茶油有限公司 | Camellia seed underwear special-purpose soap |
| CN105713754A (en) * | 2016-01-21 | 2016-06-29 | 广西大学 | Transparent soap and preparation method thereof |
| CN107641571A (en) * | 2016-07-20 | 2018-01-30 | 深圳市海馨生物科技有限公司 | A kind of perfumed soap composition of gentle environmental protection |
| CN106967545A (en) * | 2017-03-27 | 2017-07-21 | 江苏斯尔邦石化有限公司 | A kind of soap and preparation method thereof |
| CN108774611A (en) * | 2018-05-31 | 2018-11-09 | 刘士卫 | A kind of compound soap and preparation method thereof |
| CN109055050A (en) * | 2018-08-13 | 2018-12-21 | 深圳市科迪生物科技有限公司 | A kind of efficient hair follicle cleaning essential oil soap composition |
| CN109825386B (en) * | 2019-01-29 | 2021-09-10 | 丰益油脂科技（东莞）有限公司 | Soap grain containing organic sodium gluconate and environment-friendly soap |
| CN109777676A (en) * | 2019-03-18 | 2019-05-21 | 惠州市旭东实业有限公司 | A kind of craft facial soap |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6559110B1 (en) * | 2000-08-24 | 2003-05-06 | John A. Lopes | Syndet bar soap having an acidifying agent |
| CN103013715A (en) * | 2012-12-20 | 2013-04-03 | 广东鹏锦实业有限公司 | Transparent soap |
-
2015
- 2015-03-03 CN CN201510094974.5A patent/CN104629951B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6559110B1 (en) * | 2000-08-24 | 2003-05-06 | John A. Lopes | Syndet bar soap having an acidifying agent |
| CN103013715A (en) * | 2012-12-20 | 2013-04-03 | 广东鹏锦实业有限公司 | Transparent soap |
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| CN104629951A (en) | 2015-05-20 |
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Effective date of registration: 20221130 Address after: 7th Floor, Building 143, No. 2310, Yangshupu Road, Yangpu District, Shanghai 200090 Patentee after: Shanghai Soap Factory Co.,Ltd. Address before: 200431 building 35, No. 1001, Changjiang West Road, Baoshan District, Shanghai Patentee before: Shanghai Soap Co.,Ltd. |
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