CN103479545B - Folium Perillae gargarism - Google Patents
Folium Perillae gargarism Download PDFInfo
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- CN103479545B CN103479545B CN201310412854.6A CN201310412854A CN103479545B CN 103479545 B CN103479545 B CN 103479545B CN 201310412854 A CN201310412854 A CN 201310412854A CN 103479545 B CN103479545 B CN 103479545B
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- China
- Prior art keywords
- gargarism
- folium perillae
- present
- xylitol
- ethanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 235000004347 Perilla Nutrition 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 5
- 239000004141 Sodium laurylsulphate Substances 0.000 claims abstract description 5
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 5
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 5
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims abstract description 5
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims abstract description 5
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims abstract description 5
- 239000000811 xylitol Substances 0.000 claims abstract description 5
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 5
- 229960002675 xylitol Drugs 0.000 claims abstract description 5
- 235000010447 xylitol Nutrition 0.000 claims abstract description 5
- 244000124853 Perilla frutescens Species 0.000 claims abstract description 4
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 claims description 6
- DFPMSGMNTNDNHN-ZPHOTFPESA-N naringin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1O[C@H]1[C@H](OC=2C=C3O[C@@H](CC(=O)C3=C(O)C=2)C=2C=CC(O)=CC=2)O[C@H](CO)[C@@H](O)[C@@H]1O DFPMSGMNTNDNHN-ZPHOTFPESA-N 0.000 claims description 6
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims description 6
- 239000001606 7-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2S,3R,4R,5R,6S)-3,4,5-trihydroxy-6-methyloxan-2-yl]oxyoxan-2-yl]oxy-5-hydroxy-2-(4-hydroxyphenyl)chroman-4-one Substances 0.000 claims description 5
- 239000004378 Glycyrrhizin Substances 0.000 claims description 5
- 230000003115 biocidal effect Effects 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- LPLVUJXQOOQHMX-UHFFFAOYSA-N glycyrrhetinic acid glycoside Natural products C1CC(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2=O)C(O)=O)C)(C)CC2)(C)C2C(C)(C)C1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O LPLVUJXQOOQHMX-UHFFFAOYSA-N 0.000 claims description 5
- 229960004949 glycyrrhizic acid Drugs 0.000 claims description 5
- UYRUBYNTXSDKQT-UHFFFAOYSA-N glycyrrhizic acid Natural products CC1(C)C(CCC2(C)C1CCC3(C)C2C(=O)C=C4C5CC(C)(CCC5(C)CCC34C)C(=O)O)OC6OC(C(O)C(O)C6OC7OC(O)C(O)C(O)C7C(=O)O)C(=O)O UYRUBYNTXSDKQT-UHFFFAOYSA-N 0.000 claims description 5
- 235000019410 glycyrrhizin Nutrition 0.000 claims description 5
- 229940052490 naringin Drugs 0.000 claims description 5
- 229930019673 naringin Natural products 0.000 claims description 5
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 claims description 5
- 235000012141 vanillin Nutrition 0.000 claims description 5
- 210000004195 gingiva Anatomy 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 description 5
- 241000229722 Perilla <angiosperm> Species 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 230000003385 bacteriostatic effect Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 208000006558 Dental Calculus Diseases 0.000 description 2
- 241000588724 Escherichia coli Species 0.000 description 2
- 235000004348 Perilla frutescens Nutrition 0.000 description 2
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000001408 fungistatic effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000207923 Lamiaceae Species 0.000 description 1
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 206010044029 Tooth deposit Diseases 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 235000004626 essential fatty acids Nutrition 0.000 description 1
- DNJIEGIFACGWOD-UHFFFAOYSA-N ethanethiol Chemical compound CCS DNJIEGIFACGWOD-UHFFFAOYSA-N 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- 210000002200 mouth mucosa Anatomy 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 229940117960 vanillin Drugs 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The present invention relates to a kind of Folium Perillae gargarism, be made up of following compositions in weight percentage: perilla oil 0.4-0.8%, xylitol 6-10%, tetrasodium pyrophosphate 0.12-0.18%, ethanol 8-12%, sodium lauryl sulphate 0.2-0.4%, surplus are water.The strong tooth of Folium Perillae gargarism of the present invention, care gingiva, fresh breath.
Description
Technical field
The present invention relates to a kind of gargarism, be specifically related to a kind of Folium Perillae gargarism.
Background technology
Gargarism, also referred to as collutory, collutory etc.Gargarism is easy to use, saves time, and does not need special apparatus, is very effective oral hygiene appliance.
Can the antibacterial, tartar, dental calculus, food debris etc. of residual harmful on oral mucosa and tooth, can stench be produced through corrupt, fermentation.Therefore the use of gargarism is very usual and necessary.
Summary of the invention
A kind of Folium Perillae gargarism, is made up of following compositions in weight percentage: perilla oil 0.4-0.8%, xylitol 6-10%, tetrasodium pyrophosphate 0.12-0.18%, ethanol 8-12%, sodium lauryl sulphate 0.2-0.4%, surplus are water.
Preferably,
A kind of Folium Perillae gargarism, is made up of following compositions in weight percentage: perilla oil 0.4-0.8%, xylitol 6-10%, tetrasodium pyrophosphate 0.12-0.18%, ethanol 8-12%, sodium lauryl sulphate 0.2-0.4%, biological antibiosis agent 0.4-0.6%, surplus are water.
Described biological antibiosis agent is one in naringin, glycyrrhizin and vanillin or its mixture.Preferably described biological antibiosis agent, is made up of by weight following component: naringin 50-70 part, glycyrrhizin 10-30 part and vanillin 10-30 part.Wherein, naringin, CAS accession number: 10236-47-2.Glycyrrhizin, CAS accession number: 1405-86-3.Vanillin, CAS accession number: 121-33-5.
Folium Perillae gargarism of the present invention, via common process, carries out manufacture by mixed above-mentioned each raw material and forms.
Folium Perillae is Labiatae annual herb plant.Have another name called red, the red Perilla frutescens of Perilla frutescens, all have distribution in China various places.Folium Perillae blade face in green or purple, blade back then all in purple, have the cold expelling that induces sweat, circulation of qi promoting and in, relieving cough and asthma, the wide intestinal of sharp diaphragm, separate the effect of all poison.Modern nutriology finds perilla oil main component: alpha-linolenic acid, Palmic acid, linoleic acid, oleic acid, stearic acid, vitamin E, 18 seed amino acids and various trace elements.Wherein essential fatty acid is particularly abundant.
The strong tooth of Folium Perillae gargarism of the present invention, care gingiva, fresh breath.
Detailed description of the invention
Embodiment 1-4
Composition of raw materials list position: kilogram
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | |
| Perilla oil | 0.6 | 0.6 | 0.6 | 0.6 |
| Xylitol | 8 | 8 | 8 | 8 |
| Tetrasodium pyrophosphate | 0.15 | 0.15 | 0.15 | 0.15 |
| Ethanol | 10 | 10 | 10 | 10 |
| Sodium lauryl sulphate | 0.3 | 0.3 | 0.3 | 0.3 |
| Naringin | 0.5 | / | / | 0.3 |
| Glycyrrhizin | / | 0.5 | / | 0.1 |
| Vanillin | / | / | 0.5 | 0.1 |
| Water | To 100 | To 100 | To 100 | To 100 |
In each embodiment, raw material gross weight is 100 kilograms, and wherein the addition of water deducts other raw material weights by 100 kilograms and determines.
Folium Perillae gargarism of the present invention can adopt the conventional method of this area to prepare completely, as " detergent compositions workshop manual ", (Xu Baocai etc. write, Chemical Industry Press, chemistry and applied chemistry publishing centre, January in 2006 the 1st edition) gargarism production technology disclosed in 700-717 page is prepared.Namely via common process, carry out manufacture by mixed above-mentioned each raw material and form.Obviously, the preparation method of gargarism is prior art in the present invention, not special character, and main improvement of the present invention is just the difference of formula.
Test case
Folium Perillae gargarism respectively obtained by Example 1-4 directly carries out the evaluating and measuring of fungistatic effect without dilution, bacteriostatic test is carried out according to QB/T3738 " evaluation methodology of daily chemical products antibacterial bacteriostatic effect ", 1 minute action time, activity is 100% Folium Perillae gargarism, and test strain is: staphylococcus aureus and escherichia coli.
Fungistatic effect test chart
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | |
| Bacteriostasis rate (staphylococcus aureus), % | 91.7 | 92.4 | 91.2 | 93.8 |
| Bacteriostasis rate (escherichia coli), % | 91.5 | 91.2 | 90.6 | 92.7 |
From upper table data, the Folium Perillae gargarism obtained by embodiment 1-4 has good antibacterial bacteriostatic effect.
Claims (1)
1. a Folium Perillae gargarism, it is characterized in that, be made up of following compositions in weight percentage: perilla oil 0.4-0.8%, xylitol 6-10%, tetrasodium pyrophosphate 0.12-0.18%, ethanol 8-12%, sodium lauryl sulphate 0.2-0.4%, biological antibiosis agent 0.4-0.6%, surplus are water;
Described biological antibiosis agent, is made up of by weight following component: naringin 50-70 part, glycyrrhizin 10-30 part and vanillin 10-30 part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310412854.6A CN103479545B (en) | 2013-09-11 | 2013-09-11 | Folium Perillae gargarism |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310412854.6A CN103479545B (en) | 2013-09-11 | 2013-09-11 | Folium Perillae gargarism |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103479545A CN103479545A (en) | 2014-01-01 |
| CN103479545B true CN103479545B (en) | 2016-02-24 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310412854.6A Expired - Fee Related CN103479545B (en) | 2013-09-11 | 2013-09-11 | Folium Perillae gargarism |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103479545B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113456546A (en) * | 2021-06-24 | 2021-10-01 | 上海乐宝日化股份有限公司 | Oral care solution |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1280773A (en) * | 2000-08-09 | 2001-01-24 | 郭兴华 | Natural antibacterial composition and its application |
| CN1365995A (en) * | 2001-01-18 | 2002-08-28 | 戴锡麒 | Photo-and bio-degradable antibacterial film for clothes |
| CN1440976A (en) * | 2003-04-01 | 2003-09-10 | 广州环叶制药有限公司 | Shaddock glycoside extracting and refining process from shaddock |
| CN102125507A (en) * | 2010-01-18 | 2011-07-20 | 南京泽恒医药技术开发有限公司 | Oral cavity supply composition with liquoric root extract and bioadhesive function |
| CN103263375A (en) * | 2013-05-30 | 2013-08-28 | 云南七丹药业股份有限公司 | Mouthrinse containing extract and preparation method of mouthrinse |
-
2013
- 2013-09-11 CN CN201310412854.6A patent/CN103479545B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1280773A (en) * | 2000-08-09 | 2001-01-24 | 郭兴华 | Natural antibacterial composition and its application |
| CN1365995A (en) * | 2001-01-18 | 2002-08-28 | 戴锡麒 | Photo-and bio-degradable antibacterial film for clothes |
| CN1440976A (en) * | 2003-04-01 | 2003-09-10 | 广州环叶制药有限公司 | Shaddock glycoside extracting and refining process from shaddock |
| CN102125507A (en) * | 2010-01-18 | 2011-07-20 | 南京泽恒医药技术开发有限公司 | Oral cavity supply composition with liquoric root extract and bioadhesive function |
| CN103263375A (en) * | 2013-05-30 | 2013-08-28 | 云南七丹药业股份有限公司 | Mouthrinse containing extract and preparation method of mouthrinse |
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| CN103479545A (en) | 2014-01-01 |
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Effective date of registration: 20200727 Address after: 154000 north side of Industrial Park of Huanan Forestry Bureau, Huanan County, Jiamusi City, Heilongjiang Province Patentee after: Huanan nongshengyuan Food Co.,Ltd. Address before: 233010 Incubation Workshop, 414 Changle Road, Yuhui District, Bengbu City, Anhui Province Patentee before: Bengbu Xingshi Intellectual Property Operations Co.,Ltd. |
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