CN105713754A - Transparent soap and preparation method thereof - Google Patents

Transparent soap and preparation method thereof Download PDF

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Publication number
CN105713754A
CN105713754A CN201610039624.3A CN201610039624A CN105713754A CN 105713754 A CN105713754 A CN 105713754A CN 201610039624 A CN201610039624 A CN 201610039624A CN 105713754 A CN105713754 A CN 105713754A
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CN
China
Prior art keywords
soap
parts
transparent
fatty acid
essence
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610039624.3A
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Chinese (zh)
Inventor
张玉华
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Guangxi University
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Guangxi University
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Filing date
Publication date
Application filed by Guangxi University filed Critical Guangxi University
Priority to CN201610039624.3A priority Critical patent/CN105713754A/en
Publication of CN105713754A publication Critical patent/CN105713754A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0095Solid transparent soaps or detergents
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a transparent soap. The transparent soap comprises, by mass, 28-33 parts of fatty acid, 4-9 parts of glycerol, 13-18 parts of surfactants, 20-25 parts of solvents, 15-20 parts of 30% sodium hydroxide solution, 1-6 parts of rock candy, 1-2 parts of essence, 1-6 parts of preservatives and 1-6 parts of antioxidants. The transparent soap has the advantages of high solubility, good plasticity, large foam output, skin care, beautifying, high resistance to oxygen, durability, exquisite foam, gentleness to the skin and capability of making the skin fresh and smooth, thereby having good skin care effect.

Description

A kind of transparent toilet soap and preparation method thereof
Technical field
The present invention relates to the technical field of washing product, in particular to a kind of transparent toilet soap and preparation method thereof.
Background technology
Fancy soap is requisite washing and nursing article in daily life, with sodium soap and other surfactants for the most former Material, adds quality improver and appearance modifying agents, the product made after machine-shaping.
Currently, in daily life, transparent soap presents the trend replacing fancy soap.Trace it to its cause, relative to commonly Fancy soap, transparent soap has that dissolubility is high, plasticity is good, foam volume is big and the many advantages such as skin-protecting face nursing, additionally, transparent soap Also there is the outward appearance of color gloss, therefore suffer from the favor of more and more people.Society grows with each passing day for transparent soap demand Meanwhile, do not require nothing more than producer and improve the yield of transparent soap, and transparent soap quality is had higher requirement.
At present, transparent soap market sold is broadly divided into two big classes: one is " addition " formula transparent soap, and fatty acid soaps contains Measuring low, clean result is poor, easily corrupt, good-looking is not durable;Another kind of transparent soap is " grinding pressure " formula transparent soap, the most semi-transparent Bright soap, content of fatty acid is high, harder, durable, and low price is typically used as senior laundry soap.
The preparation method of both the above transparent soap is primarily present the problem that transparency is the highest and fatty acid soaps content is low.
Summary of the invention
For above-mentioned problems of the prior art, it is an object of the invention to provide a kind of transparent toilet soap and preparation method thereof.
The present invention provides following technical scheme:
A kind of transparent toilet soap, the mass fraction ratio of each component of raw material is: fatty acid 28-33 part, glycerol 4-9 part, surfactant 13-18 part, solvent 20-25 part, 30% sodium hydroxide solution 15-20 part, crystal sugar 1-6 part, essence 1-2 part, preservative 1-6 Part, antioxidant 1-6 part.
Further illustrating, the preparation method of described a kind of transparent toilet soap is as follows:
First fatty acid, solvent are mixed in reaction pot, heating, be subsequently adding sodium hydroxide solution, temperature at 65 DEG C-78 DEG C, the time For 2-3 hour, Guan Huo, stand 0.5-1 hour;Add glycerol, surfactant, crystal sugar, after being stirred, add perfume (or spice) Essence, preservative, antioxidant, stir, and has both obtained Transparent soap soap base;Soap base injects mould, and freeze forming is soap blank; Being drawn off by soap blank, be dried, temperature is 23 DEG C-28 DEG C, and humidity is 38%-42%, and the time is 3-7 days.
It is suitable thus be readily produced and to possess general high-quality fragrant that the oils and fats formula of transparent toilet soap has the highest transparency, hardness The scourability that soap is had.Described essence, uses the industry to commonly use essence.In formula, can oneself as required By selecting corresponding essence.
Fatty acid replaces the oils and fats of traditional handicraft, thus avoids the loaded down with trivial details techniques such as refine, decolouring, deodorize process, thus simple Change flow process, improve the production efficiency of transparent toilet soap.Described fatty acid, preferably C12-18 fatty acid, such as: lauric acid, meat Myristic acid, Palmic acid or acid stearic acid.
Beneficial effects of the present invention:
A kind of transparent toilet soap that the present invention provides and preparation method thereof, solves transparent toilet soap transparency the highest low with fatty acid soaps content Problem.Described transparent toilet soap has that dissolubility is high, plasticity is good, foam volume is big and the many advantages such as skin-protecting face nursing, and Have good antioxidant, durable, foam is fine and smooth, gentle to skin, uses rear skin the most smooth, has skin and protect very well Reason effect.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, aobvious So, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based on the enforcement in the present invention Example, the every other embodiment that field those of ordinary skill is obtained under not making creative work premise, broadly fall into this The scope of bright protection.
Embodiment 1
A kind of transparent toilet soap, the mass fraction ratio of each component of raw material is: fatty acid 28 parts, glycerol 4 parts, 13 parts of surfactant, Solvent 20 parts, 30% sodium hydroxide solution 15 parts, 1 part of crystal sugar, 1 part of essence, preservative 1 part, 1 part of antioxidant.
The preparation method of a kind of transparent toilet soap is as follows:
First fatty acid, solvent being mixed in reaction pot, heating, be subsequently adding sodium hydroxide solution, temperature is at 65 DEG C, and the time is 2 Hour, Guan Huo, stand 0.5 hour;Add glycerol, surfactant, crystal sugar, after being stirred, add essence, prevent Rotten agent, antioxidant, stir, and has both obtained Transparent soap soap base;Soap base injects mould, and freeze forming is soap blank;By soap Block draws off, and is dried, and temperature is 23 DEG C, and humidity is 38%, and the time is 3 days.
Embodiment 2
A kind of transparent toilet soap, the mass fraction ratio of each component of raw material is: fatty acid 33 parts, glycerol 9 parts, 18 parts of surfactant, Solvent 25 parts, 30% sodium hydroxide solution 20 parts, 6 parts of crystal sugar, 2 parts of essence, preservative 6 parts, 6 parts of antioxidant.
The preparation method of a kind of transparent toilet soap is as follows:
First fatty acid, solvent being mixed in reaction pot, heating, be subsequently adding sodium hydroxide solution, temperature is at 78 DEG C, and the time is 3 Hour, Guan Huo, stand 1 hour;Add glycerol, surfactant, crystal sugar, after being stirred, add essence, anticorrosion Agent, antioxidant, stir, and has both obtained Transparent soap soap base;Soap base injects mould, and freeze forming is soap blank;By soap blank Drawing off, be dried, temperature is 28 DEG C, and humidity is 42%, and the time is 7 days.
Embodiment 3
A kind of transparent toilet soap, the mass fraction ratio of each component of raw material is: fatty acid 30 parts, glycerol 6 parts, 15 parts of surfactant, Solvent 22 parts, 30% sodium hydroxide solution 17 parts, 3 parts of crystal sugar, 1 part of essence, preservative 4 parts, 4 parts of antioxidant.
The preparation method of a kind of transparent toilet soap is as follows:
First fatty acid, solvent being mixed in reaction pot, heating, be subsequently adding sodium hydroxide solution, temperature is at 68 DEG C, and the time is 2.5 Hour, Guan Huo, stand 1 hour;Add glycerol, surfactant, crystal sugar, after being stirred, add essence, anticorrosion Agent, antioxidant, stir, and has both obtained Transparent soap soap base;Soap base injects mould, and freeze forming is soap blank;By soap blank Drawing off, be dried, temperature is 25 DEG C, and humidity is 40%, and the time is 5 days.
Embodiment 4
A kind of transparent toilet soap, the mass fraction ratio of each component of raw material is: fatty acid 30 parts, glycerol 6 parts, 15 parts of surfactant, Solvent 22 parts, 30% sodium hydroxide solution 17 parts, 3 parts of crystal sugar, 1 part of essence, preservative 4 parts, 4 parts of antioxidant.
The preparation method of a kind of transparent toilet soap is as follows:
First fatty acid, solvent being mixed in reaction pot, heating, be subsequently adding sodium hydroxide solution, temperature is at 68 DEG C, and the time is 2.5 Hour, Guan Huo, stand 1 hour;Add glycerol, surfactant, crystal sugar, after being stirred, add essence, anticorrosion Agent, antioxidant, stir, and has both obtained Transparent soap soap base;Soap base injects mould, and freeze forming is soap blank;By soap blank Drawing off, be dried, temperature is 25 DEG C, and humidity is 40%, and the time is 5 days.
Embodiment 5
A kind of transparent toilet soap, the mass fraction ratio of each component of raw material is: fatty acid 31 parts, glycerol 7 parts, 16 parts of surfactant, Solvent 23 parts, 30% sodium hydroxide solution 18 parts, 4 parts of crystal sugar, 1 part of essence, preservative 5 parts, 3 parts of antioxidant.
The preparation method of a kind of transparent toilet soap is as follows:
First fatty acid, solvent being mixed in reaction pot, heating, be subsequently adding sodium hydroxide solution, temperature is at 70 DEG C, and the time is 2.5 Hour, Guan Huo, stand 0.8 hour;Add glycerol, surfactant, crystal sugar, after being stirred, add essence, prevent Rotten agent, antioxidant, stir, and has both obtained Transparent soap soap base;Soap base injects mould, and freeze forming is soap blank;By soap Block draws off, and is dried, and temperature is 27 DEG C, and humidity is 41%, and the time is 5 days.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention being not restricted to the described embodiments, The change made under other any spirit without departing from the present invention and principle, modify, substitute, combine, simplify, all should For equivalence substitute mode, within being included in protection scope of the present invention.

Claims (2)

1. a transparent toilet soap, it is characterised in that the mass fraction ratio of each component of raw material is: fatty acid 28-33 part, glycerol 4-9 Part, surfactant 13-18 part, solvent 20-25 part, 30% sodium hydroxide solution 15-20 part, crystal sugar 1-6 part, essence 1-2 Part, preservative 1-6 part, antioxidant 1-6 part.
The preparation method of a kind of transparent toilet soap the most according to claim 1, it is characterised in that comprise the steps:
First fatty acid, solvent are mixed in reaction pot, heating, be subsequently adding sodium hydroxide solution, temperature at 65 DEG C-78 DEG C, the time For 2-3 hour, Guan Huo, stand 0.5-1 hour;Add glycerol, surfactant, crystal sugar, after being stirred, add perfume (or spice) Essence, preservative, antioxidant, stir, and has both obtained Transparent soap soap base;Soap base injects mould, and freeze forming is soap blank; Being drawn off by soap blank, be dried, temperature is 23 DEG C-28 DEG C, and humidity is 38%-42%, and the time is 3-7 days.
CN201610039624.3A 2016-01-21 2016-01-21 Transparent soap and preparation method thereof Pending CN105713754A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610039624.3A CN105713754A (en) 2016-01-21 2016-01-21 Transparent soap and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610039624.3A CN105713754A (en) 2016-01-21 2016-01-21 Transparent soap and preparation method thereof

Publications (1)

Publication Number Publication Date
CN105713754A true CN105713754A (en) 2016-06-29

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ID=56153704

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610039624.3A Pending CN105713754A (en) 2016-01-21 2016-01-21 Transparent soap and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105713754A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1362505A (en) * 2000-12-25 2002-08-07 资生堂贺妮健工业株式会社 Transparent bar-type soap composition
CN101497849A (en) * 2009-01-20 2009-08-05 佛山市美心美容保健用品有限公司 Transparent perfumed soap and preparation thereof
CN102776085A (en) * 2012-06-30 2012-11-14 澳宝化妆品(惠州)有限公司 Novel transparent soap
CN104629951A (en) * 2015-03-03 2015-05-20 上海制皂有限公司 Transparent soap

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1362505A (en) * 2000-12-25 2002-08-07 资生堂贺妮健工业株式会社 Transparent bar-type soap composition
CN101497849A (en) * 2009-01-20 2009-08-05 佛山市美心美容保健用品有限公司 Transparent perfumed soap and preparation thereof
CN102776085A (en) * 2012-06-30 2012-11-14 澳宝化妆品(惠州)有限公司 Novel transparent soap
CN104629951A (en) * 2015-03-03 2015-05-20 上海制皂有限公司 Transparent soap

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Application publication date: 20160629

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