CN106106551A - A kind of acaricide and preparation method thereof - Google Patents

A kind of acaricide and preparation method thereof Download PDF

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Publication number
CN106106551A
CN106106551A CN201610437692.5A CN201610437692A CN106106551A CN 106106551 A CN106106551 A CN 106106551A CN 201610437692 A CN201610437692 A CN 201610437692A CN 106106551 A CN106106551 A CN 106106551A
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parts
acaricide
mixture
surfactant
fenoxycarb
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吴宏博
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HENAN ZHONG TIAN XIN BIOCHEMICAL TECHNOLOGY Co Ltd
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HENAN ZHONG TIAN XIN BIOCHEMICAL TECHNOLOGY Co Ltd
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
    • A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
    • A01N41/04—Sulfonic acids; Derivatives thereof
    • A01N41/08—Sulfonic acid halides; alpha-Hydroxy-sulfonic acids; Amino-sulfonic acids; Thiosulfonic acids; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
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  • Agronomy & Crop Science (AREA)
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  • Natural Medicines & Medicinal Plants (AREA)
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Abstract

The invention discloses a kind of acaricide and preparation method thereof, acaricide includes fatty alcohol-polyoxyethylene ether 4 10 parts by weight, Biphenthrin 5 12 parts, rotenone 14 parts, Pericarpium Citri junoris 38 parts, Fericarpium Citri Limoniae 27 parts, 15 25 parts of surfactant, Acetamiprid 14 parts, acequinocyl 10 15 parts, S-Ethyl ethylthio sulfonate 38 parts, swainson pea 10 15 parts, thyme oil 38 parts, fenpyroximate 10 15 parts and fenoxycarb 4 10 parts, processing technology of the present invention is simple, manufacturing process is environment friendly and pollution-free, the acaricide prepared can effectively kill various harmful acarids on crops, and crops will not be produced injury, additionally, life-time service, surrounding and soil will not be produced and pollute, environment protecting is good.

Description

A kind of acaricide and preparation method thereof
Technical field
The present invention relates to acaricide preparing technical field, be specially a kind of acaricide and preparation method thereof.
Background technology
Demodicid mite class, belongs to Arthropoda Arachnoidea, and phytophagous mites, mainly by tetranychid, Panonychus citri, rust mite etc., is a kind of normal The insect seen, the crop such as danger to vegetables, fruit tree, Cotton Gossypii, often result in destructive disaster, the most important harmful demodicid mite is numerous due to it Cycle of growing is short, and breeding amount is big, and mobility is little, and selfing degree is high, is particularly easy to develop immunity to drugs, though the most existing acaricide So can kill acaricide worm to a certain extent, but while removing acarid, crops are caused injury, and its residual Environment is produced and pollutes by thing, and environmental-protecting performance is poor.
Summary of the invention
It is an object of the invention to provide a kind of acaricide and preparation method thereof, to solve proposition in above-mentioned background technology Problem.
For achieving the above object, the present invention provides following technical scheme: a kind of acaricide, acaricide includes by weight Fatty alcohol-polyoxyethylene ether 4-10 part, Biphenthrin 5-12 part, rotenone 1-4 part, Pericarpium Citri junoris 3-8 part, Fericarpium Citri Limoniae 2-7 part, surface Activating agent 15-25 part, Acetamiprid 1-4 part, acequinocyl 10-15 part, S-Ethyl ethylthio sulfonate 3-8 part, swainson pea 10-15 part, thyme oil 3-8 Part, fenpyroximate 10-15 part and fenoxycarb 4-10 part.
Preferably, preferred composition proportion is fatty alcohol-polyoxyethylene ether 7 parts, Biphenthrin 8 parts, rotenone 3 parts, Pericarpium Citri junoris 5 parts, Fericarpium Citri Limoniae 4 parts, 20 parts of surfactant, Acetamiprid 2 parts, acequinocyl 7 parts, S-Ethyl ethylthio sulfonate 6 parts, swainson pea 12 parts, Herba thymi vulgaris Oil 5 parts, fenpyroximate 12 parts and fenoxycarb 7 parts.
Preferably, acaricide is configured to microemulsion, suspending agent, aqueous emulsion or cream.
Preferably, its preparation method comprises the following steps:
A, pulverizing adding in pulverizer after Pericarpium Citri junoris, Fericarpium Citri Limoniae, swainson pea mixing, carry out filtering residue after pulverizing, the filtrate obtained is A Mixture；
B, in A mixture, add fatty alcohol-polyoxyethylene ether, Biphenthrin, rotenone and 1/3 surfactant, mix laggard Row mechanical agitation, stir speed (S.S.) is 500-800 rev/min, and mixing time is 3min-7min, stands afterwards and obtains B mixture；
C, in B mixture, it is sequentially added into Acetamiprid, acequinocyl, S-Ethyl ethylthio sulfonate and 1/3 surfactant, pours into afterwards in reactor Heating, is slowly added to thyme oil, fenpyroximate in heating process, constant temperature after being heated to 60 DEG C obtains C mixture；
D, adding fenoxycarb and 1/3 surfactant in C mixture, stirring afterwards is cooled to room temperature, i.e. obtains acaricide.
Compared with prior art, the invention has the beneficial effects as follows: processing technology of the present invention is simple, and manufacturing process environmental protection is without dirt Contaminating, the acaricide prepared can effectively kill various harmful acarids on crops, and crops will not be produced injury, it addition, Life-time service, will not produce surrounding and soil and pollute, and environment protecting is good；Additionally the present invention is configured to microemulsion, suspension Agent, aqueous emulsion or cream, it is possible to greatly reduce the harm to dispenser personnel.
Detailed description of the invention
Below the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment It is only a part of embodiment of the present invention rather than whole embodiments, based on the embodiment in the present invention, the common skill in this area The every other embodiment that art personnel are obtained under not making creative work premise, broadly falls into the model of present invention protection Enclose.
The present invention provides a kind of technical scheme: a kind of acaricide, acaricide includes aliphatic alcohol polyethenoxy by weight Ether 4-10 part, Biphenthrin 5-12 part, rotenone 1-4 part, Pericarpium Citri junoris 3-8 part, Fericarpium Citri Limoniae 2-7 part, surfactant 15-25 part, Acetamiprid 1-4 part, acequinocyl 10-15 part, S-Ethyl ethylthio sulfonate 3-8 part, swainson pea 10-15 part, thyme oil 3-8 part, fenpyroximate 10-15 Part and fenoxycarb 4-10 part.
Embodiment one:
The composition proportion used is: fatty alcohol-polyoxyethylene ether 4 parts, Biphenthrin 5 parts, rotenone 1 part, Pericarpium Citri junoris 3 parts, Fericarpium Citri Limoniae 2 parts, 15 parts of surfactant, Acetamiprid 1 part, acequinocyl 10 parts, S-Ethyl ethylthio sulfonate 3 parts, swainson pea 10 parts, thyme oil 3 parts, azoles demodicid mite Ester 10 parts and fenoxycarb 4-part.
In the present embodiment, acaricide is configured to microemulsion, suspending agent, aqueous emulsion or cream.
The preparation method of the present embodiment comprises the following steps:
A, pulverizing adding in pulverizer after Pericarpium Citri junoris, Fericarpium Citri Limoniae, swainson pea mixing, carry out filtering residue after pulverizing, the filtrate obtained is A Mixture；
B, in A mixture, add fatty alcohol-polyoxyethylene ether, Biphenthrin, rotenone and 1/3 surfactant, mix laggard Row mechanical agitation, stir speed (S.S.) is 500 revs/min, and mixing time is 3min, stands afterwards and obtains B mixture；
C, in B mixture, it is sequentially added into Acetamiprid, acequinocyl, S-Ethyl ethylthio sulfonate and 1/3 surfactant, pours into afterwards in reactor Heating, is slowly added to thyme oil, fenpyroximate in heating process, constant temperature after being heated to 60 DEG C obtains C mixture；
D, adding fenoxycarb and 1/3 surfactant in C mixture, stirring afterwards is cooled to room temperature, i.e. obtains acaricide.
Embodiment two:
The composition proportion used is: fatty alcohol-polyoxyethylene ether 5 parts, Biphenthrin 6 parts, rotenone 2 parts, Pericarpium Citri junoris 4 parts, Fericarpium Citri Limoniae 3 parts, 16 parts of surfactant, Acetamiprid 2 parts, acequinocyl 11 parts, S-Ethyl ethylthio sulfonate 4 parts, swainson pea 11 parts, thyme oil 4 parts, azoles demodicid mite Ester 11 parts and fenoxycarb 5 parts.
In the present embodiment, demodicid mite agent is configured to microemulsion, suspending agent, aqueous emulsion or cream.
The preparation method of the present embodiment comprises the following steps:
A, pulverizing adding in pulverizer after Pericarpium Citri junoris, Fericarpium Citri Limoniae, swainson pea mixing, carry out filtering residue after pulverizing, the filtrate obtained is A Mixture；
B, in A mixture, add fatty alcohol-polyoxyethylene ether, Biphenthrin, rotenone and 1/3 surfactant, mix laggard Row mechanical agitation, stir speed (S.S.) is 600 revs/min, and mixing time is 4min, stands afterwards and obtains B mixture；
C, in B mixture, it is sequentially added into Acetamiprid, acequinocyl, S-Ethyl ethylthio sulfonate and 1/3 surfactant, pours into afterwards in reactor Heating, is slowly added to thyme oil, fenpyroximate in heating process, constant temperature after being heated to 60 DEG C obtains C mixture；
D, adding fenoxycarb and 1/3 surfactant in C mixture, stirring afterwards is cooled to room temperature, i.e. obtains acaricide.
Embodiment three:
The composition proportion used is: fatty alcohol-polyoxyethylene ether 10 parts, Biphenthrin 12 parts, rotenone 4 parts, Pericarpium Citri junoris 8 parts, Fructus Citri Limoniae Skin 7 parts, 25 parts of surfactant, Acetamiprid 4 parts, acequinocyl 15 parts, S-Ethyl ethylthio sulfonate 8 parts, swainson pea 15 parts, thyme oil 8 parts, azoles Demodicid mite ester 15 parts and fenoxycarb 10 parts.
In the present embodiment, acaricide is configured to microemulsion, suspending agent, aqueous emulsion or cream.
The present embodiment preparation method comprises the following steps:
A, pulverizing adding in pulverizer after Pericarpium Citri junoris, Fericarpium Citri Limoniae, swainson pea mixing, carry out filtering residue after pulverizing, the filtrate obtained is A Mixture；
B, in A mixture, add fatty alcohol-polyoxyethylene ether, Biphenthrin, rotenone and 1/3 surfactant, mix laggard Row mechanical agitation, stir speed (S.S.) is 800 revs/min, and mixing time is 7min, stands afterwards and obtains B mixture；
C, in B mixture, it is sequentially added into Acetamiprid, acequinocyl, S-Ethyl ethylthio sulfonate and 1/3 surfactant, pours into afterwards in reactor Heating, is slowly added to thyme oil, fenpyroximate in heating process, constant temperature after being heated to 60 DEG C obtains C mixture；
D, adding fenoxycarb and 1/3 surfactant in C mixture, stirring afterwards is cooled to room temperature, i.e. obtains acaricide.
Embodiment four:
The composition proportion used is: fatty alcohol-polyoxyethylene ether 9 parts, Biphenthrin 11 parts, rotenone 4 parts, Pericarpium Citri junoris 7 parts, Fructus Citri Limoniae Skin 6 parts, 22 parts of surfactant, Acetamiprid 4 parts, acequinocyl 14 parts, S-Ethyl ethylthio sulfonate 7 parts, swainson pea 14 parts, thyme oil 7 parts, azoles Demodicid mite ester 14 parts and fenoxycarb 9 parts.
In the present embodiment, acaricide is configured to microemulsion, suspending agent, aqueous emulsion or cream.
The preparation method of the present embodiment comprises the following steps:
A, pulverizing adding in pulverizer after Pericarpium Citri junoris, Fericarpium Citri Limoniae, swainson pea mixing, carry out filtering residue after pulverizing, the filtrate obtained is A Mixture；
B, in A mixture, add fatty alcohol-polyoxyethylene ether, Biphenthrin, rotenone and 1/3 surfactant, mix laggard Row mechanical agitation, stir speed (S.S.) is 750 revs/min, and mixing time is 6min, stands afterwards and obtains B mixture；
C, in B mixture, it is sequentially added into Acetamiprid, acequinocyl, S-Ethyl ethylthio sulfonate and 1/3 surfactant, pours into afterwards in reactor Heating, is slowly added to thyme oil, fenpyroximate in heating process, constant temperature after being heated to 60 DEG C obtains C mixture；
D, adding fenoxycarb and 1/3 surfactant in C mixture, stirring afterwards is cooled to room temperature, i.e. obtains acaricide.
Embodiment five:
The composition proportion used is: fatty alcohol-polyoxyethylene ether 7 parts, Biphenthrin 8 parts, rotenone 3 parts, Pericarpium Citri junoris 5 parts, Fructus Citri Limoniae Skin 4 parts, 20 parts of surfactant, Acetamiprid 2 parts, acequinocyl 7 parts, S-Ethyl ethylthio sulfonate 6 parts, swainson pea 12 parts, thyme oil 5 parts, azoles Demodicid mite ester 12 parts and fenoxycarb 7 parts.
In the present embodiment, acaricide is configured to microemulsion, suspending agent, aqueous emulsion or cream.
The preparation method of the present embodiment comprises the following steps:
A, pulverizing adding in pulverizer after Pericarpium Citri junoris, Fericarpium Citri Limoniae, swainson pea mixing, carry out filtering residue after pulverizing, the filtrate obtained is A Mixture；
B, in A mixture, add fatty alcohol-polyoxyethylene ether, Biphenthrin, rotenone and 1/3 surfactant, mix laggard Row mechanical agitation, stir speed (S.S.) is 650 revs/min, and mixing time is 5min, stands afterwards and obtains B mixture；
C, in B mixture, it is sequentially added into Acetamiprid, acequinocyl, S-Ethyl ethylthio sulfonate and 1/3 surfactant, pours into afterwards in reactor Heating, is slowly added to thyme oil, fenpyroximate in heating process, constant temperature after being heated to 60 DEG C obtains C mixture；
D, adding fenoxycarb and 1/3 surfactant in C mixture, stirring afterwards is cooled to room temperature, i.e. obtains acaricide.
Experimental example:
In multiple experiment wares, it is separately added into various acarid, is respectively adopted common acaricide agent and each real-time example of the present invention prepares and kills Demodicid mite agent is sprayed, and sprays 2 days continuously, measures acaricidal rate respectively, experimental data such as following table behind 5 days and 10 days:
From above table data, embodiment five prepares acaricide can obtain optimum efficiency.
Processing technology of the present invention is simple, and manufacturing process is environment friendly and pollution-free, and the acaricide prepared can effectively kill crops Upper various harmful acarids, and crops will not be produced injury, it addition, life-time service, surrounding and soil will not be produced Polluting, environment protecting is good；Additionally the present invention is configured to microemulsion, suspending agent, aqueous emulsion or cream, it is possible to it is right to greatly reduce The harm of dispenser personnel.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, permissible Understand and these embodiments can be carried out multiple change without departing from the principles and spirit of the present invention, revise, replace And modification, the scope of the present invention be defined by the appended.

Claims (4)

1. an acaricide, it is characterised in that: acaricide includes fatty alcohol-polyoxyethylene ether 4-10 part, biphenyl chrysanthemum by weight Ester 5-12 part, rotenone 1-4 part, Pericarpium Citri junoris 3-8 part, Fericarpium Citri Limoniae 2-7 part, surfactant 15-25 part, Acetamiprid 1-4 part, demodicid mite of going out Quinone 10-15 part, S-Ethyl ethylthio sulfonate 3-8 part, swainson pea 10-15 part, thyme oil 3-8 part, fenpyroximate 10-15 part and fenoxycarb 4-10 Part.
A kind of acaricide the most according to claim 1, it is characterised in that: preferably composition proportion is aliphatic alcohol polyethenoxy 7 parts of ether, Biphenthrin 8 parts, rotenone 3 parts, Pericarpium Citri junoris 5 parts, Fericarpium Citri Limoniae 4 parts, 20 parts of surfactant, Acetamiprid 2 parts, acequinocyl 7 parts, S-Ethyl ethylthio sulfonate 6 parts, swainson pea 12 parts, thyme oil 5 parts, fenpyroximate 12 parts and fenoxycarb 7 parts.
A kind of acaricide the most according to claim 1, it is characterised in that: acaricide is configured to microemulsion, suspending agent, water and milk Agent or cream.
A kind of acaricide the most according to claim 1, it is characterised in that: its preparation method comprises the following steps:
A, pulverizing adding in pulverizer after Pericarpium Citri junoris, Fericarpium Citri Limoniae, swainson pea mixing, carry out filtering residue after pulverizing, the filtrate obtained is A Mixture；
B, in A mixture, add fatty alcohol-polyoxyethylene ether, Biphenthrin, rotenone and 1/3 surfactant, mix laggard Row mechanical agitation, stir speed (S.S.) is 500-800 rev/min, and mixing time is 3min-7min, stands afterwards and obtains B mixture；
C, in B mixture, it is sequentially added into Acetamiprid, acequinocyl, S-Ethyl ethylthio sulfonate and 1/3 surfactant, pours into afterwards in reactor Heating, is slowly added to thyme oil, fenpyroximate in heating process, constant temperature after being heated to 60 DEG C obtains C mixture；
D, adding fenoxycarb and 1/3 surfactant in C mixture, stirring afterwards is cooled to room temperature, i.e. obtains acaricide.
CN201610437692.5A 2016-06-20 2016-06-20 A kind of acaricide and preparation method thereof Pending CN106106551A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110393187A (en) * 2019-09-05 2019-11-01 湖南宇山玉月农业科技有限公司 A kind of red turpentine beetle insecticide
CN113398051A (en) * 2020-10-12 2021-09-17 中华全国供销合作总社南京野生植物综合利用研究所 Plant combined extract for removing mites and acnes as well as preparation method and application thereof
CN113398051B (en) * 2020-10-12 2022-08-23 中华全国供销合作总社南京野生植物综合利用研究所 Plant combined extract for removing mites and acnes as well as preparation method and application thereof

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Application publication date: 20161116