CN102113488A - Cyflumetofen-containing insecticidal/acaricidal composition - Google Patents
Cyflumetofen-containing insecticidal/acaricidal composition Download PDFInfo
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- CN102113488A CN102113488A CN2010106140905A CN201010614090A CN102113488A CN 102113488 A CN102113488 A CN 102113488A CN 2010106140905 A CN2010106140905 A CN 2010106140905A CN 201010614090 A CN201010614090 A CN 201010614090A CN 102113488 A CN102113488 A CN 102113488A
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- pyridaben
- insecticidal
- mite ester
- cyflumetofen
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Abstract
The invention belongs to the field of pesticide insecticidal/acaricidal compositions, in particular to a cyflumetofen-containing insecticidal/acaricidal composition. Aiming at the practical problems that the using amount of a pesticide is large, cost is high, the resistance of pests is easy to generate due to reuse, and the like in the conventional singly used propargite and pyridaben for preventing and controlling harmful acarids, the invention provides the cyflumetofen-containing insecticidal/acaricidal composition. The technical scheme is that: the cyflumetofen-containing insecticidal/acaricidal composition comprises active ingredients A and B, wherein A is cyflumetofen, and B is one of the pyridaben and the propargite. The insecticidal/acaricidal composition has the advantages that: after the cyflumetofen is compounded with the propargite or the pyridaben, the insecticidal/acaricidal composition has obvious synergy and persistent prevention and control effects; the using amount of the pesticide is reduced, the residual amount of the pesticide on crops is reduced, and environmental pollution is abated; and the insecticidal/acaricidal composition is safe for human and animals and has high environmental compatibility, and the pesticide resistance of the harmful acarids is difficult to generate.
Description
Technical field
The invention belongs to agricultural insecticide miticide composition field, particularly a kind of fourth fluorine mite ester insecticide acaricide composition that contains.
Background technology
Fourth fluorine mite ester, English name Cyflumetofen, trade name Danisraba is by the novel acyl group acetonitrile class miticide of Japan big tomb chemical company exploitation, does not have cross resistance with existing insecticide.Get permission registration and sell in Japan first in 2007, and be used for the main mite class that crops such as fruit tree, vegetables, tea tree and flowers control parasitize plant.To the ovum of tetranychid with to become mite all effective, to if the activity of mite is higher.
Pyridaben, chemical name are that (4-tertiary butyl benzylthio-4-chloro-3 (H)-pyridazin-3-one is a kind of heterocyclic miticide to 2-tertiary butyl-5-.It is widely used in cotton, peach, apple, pears, oranges and tangerines, tea etc. productions and goes up the various multiple tetranychids of control.Tagging property of pyridaben is strong, and quick-acting is good, and ovum, children are all had outstanding preventive effect as if mite and one-tenth mite.
Alkynes mite spy, chemical name is 2-(4-tert-butyl benzene oxy)-cyclohexyl Propargyl sulfite, for low toxicity broad spectrum activity organic base miticide, has and tags and stomach poison function, does not inhale and permeability in not having.To becoming mite, effective as if mite, the lasting period can reach 30～50 days, can be used for preventing and treating various crop and evil mites such as apple, oranges and tangerines, cotton, vegetables, tea, flowers, can also effectively prevent and treat the mite class to organic phosphor and organo-chlorine pesticide generation resistance.
Along with improving constantly of name of the country rapid economy development and living standards of the people, more and more higher requirement has been proposed for quantity, quality and the safety thereof of peasant's product.But, over past ten years, because high-quality, high yield and the variation of fruit tree crops such as oranges and tangerines, apple, and climate warming and the invasion of external pest, the generation harm of fruit tree pest insect totally is ascendant trend significantly.
Mite pest, be commonly called as two spotted spider mite, it is one of primary pest of crops such as fruit tree, cotton, vegetables, not only have a strong impact on the growing way of fruit tree and crops, because the generation algebraically of mite class is many, breeding spreads fast again, and alternately growth of many generations, thereby the control quite difficulty of getting up, again because mite class and general farmland insect pest physiological mechanism different, general colleges and universities' insecticide does not almost have preventive and therapeutic effect to the mite class.In the past, it is less that China is used to prevent and treat the specialized acaricide of mite class, generally is to use mixture of dicofol, tetradiphon, isocarbophos, azacyclotin and they and diesel oil etc. etc., and control efficiency is undesirable.All need to use a large amount of agricultural chemicals and carry out pest control every year, retrieves crop yield loss as far as possible.But the agricultural chemicals abuse makes insect produce more and more serious resistance to agricultural chemicals, causes the pest control effect to reduce year by year.The miserable environment of many chemical pesticides pollutes environment, therefore, is badly in need of more novel form, more efficient, safer, the Pesticidal products of environmental protection more.
The different cultivars composition carries out composite, is the modal method of control resistant insect.Heterogeneity is carried out composite, can improve imitation, reduces the consumption of active ingredient, saves drug cost, delays the generation of pest resistance to insecticide, reduces environmental pollution, is the important means of integrated control insect.By retrieval, do not find fourth fluorine mite ester and the document that is selected from any Recompounded pesticide among pyridaben or the alkynes mite spy.
The inventor has filtered out fourth fluorine mite ester and any complex composition that is selected among pyridaben or the alkynes mite spy by a large amount of desk research and field experiment, and mandarin tree, apple tree, common Panonychus citri, Tetranychus urticae, the Tetranychus cinnabarinus of cotton are had greater activity; Reduce the dosage of agricultural chemicals, reduced the residual quantity of agricultural chemicals on crop, reduced environmental pollution; Person poultry safety, good, the harmful mite of Environmental compatibility are difficult for developing immunity to drugs, thereby have finished the present invention.
Summary of the invention
Be easy to generate practical problems such as resistance at the dosage of use alkynes mite spy, the existence of pyridaben pest control mite is big separately at present, cost is higher, reuse insect, the present invention proposes a kind of fourth fluorine mite ester insecticide acaricide composition that contains, it can fully improve the performance of drug effect, improve insecticidal effect, reduce dosage, reduce cost, delay the drug-fast generation of evil mite.
Technical scheme of the present invention is: a kind of fourth fluorine mite ester insecticide acaricide composition that contains, contain A and B in its active ingredient, and wherein A is a fourth fluorine mite ester, B is selected from a kind of among pyridaben or the alkynes mite spy.
Above-mentioned active ingredient fourth fluorine mite ester, pyridaben and alkynes mite spy all are insecticidal/acaricidal agents well-known in the art, can buy by various commercial channel.
When described active ingredient B selected pyridaben for use, the weight ratio of fourth fluorine mite ester and pyridaben was 1: 3～3: 1.
When described active ingredient B selected for use the alkynes mite special, fourth fluorine mite ester and alkynes mite spy's weight ratio was 1: 4～4: 1.
Described effective constituents A and the B weight percentage in described composition is 1%～80%.
Also comprise auxiliary agent, solvent and filler in the described composition.
The formulation of described composition is pulvis, granule, missible oil, wetting powder, microemulsion, aqueous emulsion, aqueous suspension agent or water dispersible granules.
Beneficial effect of the present invention is: after fourth fluorine mite ester and alkynes mite spy or pyridaben are composite, have notable synergistic and hold the effect control efficiency; Mandarin tree, apple tree, common Panonychus citri, Tetranychus urticae, the Tetranychus cinnabarinus of cotton there is greater activity; Reduce the dosage of agricultural chemicals, reduced the residual quantity of agricultural chemicals on crop, reduced environmental pollution; Person poultry safety, good, the harmful mite of Environmental compatibility are difficult for developing immunity to drugs.
Embodiment
Specify the present invention below in conjunction with embodiment.Percentage all is weight percentage among the embodiment, and the treatment dosage of field efficacy is effective ingredient consumption.
Embodiment 1:40% fourth fluorine mite ester pyridaben aqueous suspension agent
Preparation method: press formula rate, fourth fluorine mite ester, pyridaben, dispersant sodium lignin sulfonate, wetting agent OP-10, thickener CMC, defoamer organic silicone, antifreeze glycol are placed reactor successively, adding water mixes, mixture being introduced again and being ground to the material fineness in the sand mill is 1-5um, promptly makes 40% fourth fluorine mite ester pyridaben aqueous suspension agent.
Prescription: fourth fluorine mite ester, 15%; Pyridaben, 25%; The dispersant sodium lignin sulfonate, 10%; Wetting agent OP-10,2%; Thickener CMC, 1%; The defoamer organic silicone, 0.01%; Antifreeze glycol, 8%; Aqueous solvent, surplus.
Use embodiment 1 and Comparative Examples to carry out field control effectiveness test below, so that beneficial effect of the present invention to be described better, experimental result is as shown in table 1 below.
Field control effectiveness test: adopt the anti-therapy of spraying, incubate the peak period dispenser, convert water 50kg even spraying by every mu of dosage, every sub-district 30m at the Tetranychus cinnabarinus ovum
2Be a processing, separate with the little ridge between processing, and establish guard row.Investigate dead borer population in 1 day, 3 days, 10 days, 15 days, 20 days behind the medicine, calculate control efficiency.
In the table 1, embodiment 1:40% fourth fluorine mite ester pyridaben aqueous suspension agent; Comparative Examples 1:20% fourth fluorine mite ester (single agent) aqueous suspension agent; Comparative Examples 2:20% pyridaben (single agent) aqueous suspension agent.
The field efficacy demonstration test result of table 1 embodiment 1 and 1,2 pairs of Tetranychus cinnabarinus of Comparative Examples
According to table 1 as can be seen: 1 three of embodiment handled after the dispenser the 1st day and the 3rd day control efficiency all more than 90%, 20 days control efficiency show that still more than 80% 40% fourth fluorine mite ester Damanling suspension agent has good quick-acting and lasting effect after the dispenser.Among 1500 times of liquid control efficiency of Comparative Examples 1 and the embodiment 1 1500 times of liquid the 1st day and the 3rd day quite, but the 20th day control efficiency is lower than the 20th day effect of embodiment 1, shows that lasting effect is lower than embodiment 1; Comparative Examples 2 quick-acting and lasting effect all are lower than embodiment 1.
Field control effectiveness test is the result show: after fourth fluorine mite ester and pyridaben are composite, get single agent compared to fourth fluorine mite ester or pyridaben and have notable synergistic and hold the effect control efficiency.
The special aqueous emulsion of embodiment 2:30% fourth fluorine mite ester alkynes mite
Preparation method: press formula rate, fourth fluorine mite ester and alkynes mite spy are dissolved in the organic solvent, and add auxiliary agent therein, add water, make the special aqueous emulsion of 30% fourth fluorine mite ester alkynes mite according to the conventional method for preparing aqueous emulsion.
Prescription: fourth fluorine mite ester, 13%; Alkynes mite spy, 17%; Surfactant is selected the mixture of phenethyl phenol polyethenoxy ether phosphate and agricultural newborn 33# for use, total consumption 8%; Solvent is selected dimethylbenzene and cyclohexanone for use, and consumption is respectively 10% and 8%; Water, surplus.
Embodiment 3:80% fourth fluorine mite ester pyridaben water dispersible granules
The preparation method: press formula rate, fourth fluorine mite ester and pyridaben are added in the filler, and add the auxiliary agent mixing therein, through comminution by gas stream, with powder water spray, granulation, the drying of pulverizing in the fluidized granulating machine, screening afterwards makes product.Capital equipment has mixer, airslide disintegrating mill, kneader, Squeezinggranulator, drying room or fluid-bed drying, or fluidized granulating machine, screening machine.
Prescription: fourth fluorine mite ester, 20%; Pyridaben, 60%; Dispersant alkylnaphthalene sulfonate formaldehyde condensation products, 4%; The wetting agent lauryl sodium sulfate, 6%; Filler diatomite, surplus.
Embodiment 4:15% fourth fluorine mite ester propargite microemulsion
Preparation method: press formula rate, fourth fluorine mite ester and alkynes mite spy are dissolved in the organic solvent, and add auxiliary agent therein, add water, make 15% fourth fluorine mite ester propargite microemulsion according to the conventional method for preparing microemulsion.
Prescription: fourth fluorine mite ester, 5%; Alkynes mite spy, 10%; Surfactant is selected the mixture of phenethyl phenol polyethenoxy ether and agricultural newborn 34# for use, total consumption 16%; Antifreezing agent is selected isopropyl alcohol for use, consumption 4%; Solvent is selected dimethylbenzene and N for use, and dinethylformamide, consumption are respectively 10% and 8%; Water, surplus.
Embodiment 5:75% fourth fluorine mite ester pyridaben wetting powder
Preparation method: press formula rate, fourth fluorine mite ester and pyridaben are added in the filler, and add the auxiliary agent mixing therein, the mixed again wetting powder that gets behind comminution by gas stream.Capital equipment has mixer, airslide disintegrating mill.
Prescription: fourth fluorine mite ester, 20%; Pyridaben, 55%; Dispersant alkylnaphthalene sulfonate formaldehyde condensation products, 4%; The wetting agent lauryl sodium sulfate, 6%; Filler diatomite, surplus.
Use embodiment 4 and embodiment 5 to carry out field control effectiveness test with Comparative Examples below, so that beneficial effect of the present invention to be described better, experimental result is as shown in table 2 below.
Field control effectiveness test: adopt the anti-therapy of spraying, convert water 50kg even spraying by every mu of dosage, every sub-district 30m
2Be a processing, separate with the little ridge between processing, and establish guard row.Investigate dead borer population in 1 day, 3 days, 7 days behind the medicine, calculate control efficiency.
In the table 2, embodiment 4:15% fourth fluorine mite ester propargite microemulsion; Embodiment 5:75% fourth fluorine mite ester pyridaben wetting powder; Comparative Examples 1:20% fourth fluorine mite ester (single agent) aqueous suspension agent; Comparative Examples 3:20% pyridaben (single agent) wetting powder; Comparative Examples 4:40% alkynes mite spy (single agent) microemulsion.
The field efficacy demonstration test result of table 2 embodiment 4,5 and 1,3,4 pairs of panonychus citris of Comparative Examples
According to table 2 as can be seen: the control efficiency of embodiment 4 and embodiment 5 is significantly higher than the control efficiency of Comparative Examples 1, Comparative Examples 3 and Comparative Examples 4.Duration of test is observed, and oranges and tangerines do not have symptom of chemical damage, and test medicine is to oranges and tangerines safety.
Field control effectiveness test is the result show: by the special composite tool of fourth fluorine mite ester and alkynes mite or fourth fluorine mite ester pyridaben is composite all has significant synergies.
Claims (6)
1. one kind contains fourth fluorine mite ester insecticide acaricide composition, it is characterized in that, contains A and B in its active ingredient, and wherein A is a fourth fluorine mite ester, and B is selected from a kind of among pyridaben or the alkynes mite spy.
2. the fourth fluorine mite ester insecticide acaricide composition that contains according to claim 1 is characterized in that described active ingredient B is a pyridaben, and the weight ratio of A and B is 1: 3～3: 1.
3. the fourth fluorine mite ester insecticide acaricide composition that contains according to claim 1 is characterized in that described active ingredient B is alkynes mite spy, and the weight ratio of A and B is 1: 4～4: 1.
4. the fourth fluorine mite ester insecticide acaricide composition that contains according to claim 1 is characterized in that described effective constituents A and the B weight percentage in described composition is 1%～80%.
5. the fourth fluorine mite ester insecticide acaricide composition that contains according to claim 1 is characterized in that, also comprises auxiliary agent, solvent or filler in the described composition.
6. the fourth fluorine mite ester insecticide acaricide composition that contains according to claim 1 is characterized in that the formulation of described composition is pulvis, granule, missible oil, wetting powder, microemulsion, aqueous emulsion, aqueous suspension agent or water dispersible granules.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010106140905A CN102113488A (en) | 2010-12-30 | 2010-12-30 | Cyflumetofen-containing insecticidal/acaricidal composition |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010106140905A CN102113488A (en) | 2010-12-30 | 2010-12-30 | Cyflumetofen-containing insecticidal/acaricidal composition |
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| CN201310070243.8A Division CN103125487B (en) | 2010-12-30 | 2010-12-30 | Insecticidal and acaricidal composition containing cyflumetofen |
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| CN102113488A true CN102113488A (en) | 2011-07-06 |
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| CN2010106140905A Pending CN102113488A (en) | 2010-12-30 | 2010-12-30 | Cyflumetofen-containing insecticidal/acaricidal composition |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102630676A (en) * | 2012-03-29 | 2012-08-15 | 陕西韦尔奇作物保护有限公司 | Efficient insecticidal composition |
| CN102972415A (en) * | 2012-12-24 | 2013-03-20 | 海利尔药业集团股份有限公司 | Insecticidal and acaricidal composition containing buprofezin and cyflumetofen |
| CN102972404A (en) * | 2012-12-24 | 2013-03-20 | 海利尔药业集团股份有限公司 | Pesticidal composition containing fluacrypyrim and cyflumetofen |
| CN103283731A (en) * | 2012-02-23 | 2013-09-11 | 深圳诺普信农化股份有限公司 | Pesticide composition for preventing and treating drug-fast tetranychid mites |
| CN103548832A (en) * | 2013-11-11 | 2014-02-05 | 陕西农心作物科技有限公司 | Acaricidal composition containing pyriminostrobin and cyflumetofen |
| CN105746515A (en) * | 2012-03-31 | 2016-07-13 | 陕西韦尔奇作物保护有限公司 | Pesticide composition with cyflumetofen |
| CN105851008A (en) * | 2012-06-27 | 2016-08-17 | 陕西美邦农药有限公司 | Pesticide composition containing acequinocyl |
| CN108041042A (en) * | 2017-12-10 | 2018-05-18 | 广东中迅农科股份有限公司 | A kind of composition pesticide containing cyflumetofen and fluazinam |
| CN111264535A (en) * | 2020-03-11 | 2020-06-12 | 山东滨海瀚生生物科技有限公司 | Agricultural acaricidal composition and application thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103283731A (en) * | 2012-02-23 | 2013-09-11 | 深圳诺普信农化股份有限公司 | Pesticide composition for preventing and treating drug-fast tetranychid mites |
| CN103283731B (en) * | 2012-02-23 | 2014-11-26 | 深圳诺普信农化股份有限公司 | Pesticide composition for preventing and treating drug-fast tetranychid mites |
| CN102630676B (en) * | 2012-03-29 | 2016-11-23 | 陕西韦尔奇作物保护有限公司 | A kind of Efficient insecticidal composition |
| CN102630676A (en) * | 2012-03-29 | 2012-08-15 | 陕西韦尔奇作物保护有限公司 | Efficient insecticidal composition |
| CN105746515A (en) * | 2012-03-31 | 2016-07-13 | 陕西韦尔奇作物保护有限公司 | Pesticide composition with cyflumetofen |
| CN105746515B (en) * | 2012-03-31 | 2018-03-30 | 陕西韦尔奇作物保护有限公司 | A kind of composition pesticide containing cyflumetofen |
| CN105851008A (en) * | 2012-06-27 | 2016-08-17 | 陕西美邦农药有限公司 | Pesticide composition containing acequinocyl |
| CN102972404A (en) * | 2012-12-24 | 2013-03-20 | 海利尔药业集团股份有限公司 | Pesticidal composition containing fluacrypyrim and cyflumetofen |
| CN102972415A (en) * | 2012-12-24 | 2013-03-20 | 海利尔药业集团股份有限公司 | Insecticidal and acaricidal composition containing buprofezin and cyflumetofen |
| CN103548832A (en) * | 2013-11-11 | 2014-02-05 | 陕西农心作物科技有限公司 | Acaricidal composition containing pyriminostrobin and cyflumetofen |
| CN103548832B (en) * | 2013-11-11 | 2014-12-17 | 陕西农心作物科技有限公司 | Acaricidal composition containing pyriminostrobin and cyflumetofen |
| CN108041042A (en) * | 2017-12-10 | 2018-05-18 | 广东中迅农科股份有限公司 | A kind of composition pesticide containing cyflumetofen and fluazinam |
| CN111264535A (en) * | 2020-03-11 | 2020-06-12 | 山东滨海瀚生生物科技有限公司 | Agricultural acaricidal composition and application thereof |
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Application publication date: 20110706 |