NO762283L - - Google Patents
Info
- Publication number
- NO762283L NO762283L NO762283A NO762283A NO762283L NO 762283 L NO762283 L NO 762283L NO 762283 A NO762283 A NO 762283A NO 762283 A NO762283 A NO 762283A NO 762283 L NO762283 L NO 762283L
- Authority
- NO
- Norway
- Prior art keywords
- water
- vinyl chloride
- polymerization
- dispersion
- monomer
- Prior art date
Links
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 239000000178 monomer Substances 0.000 claims description 20
- 238000006116 polymerization reaction Methods 0.000 claims description 20
- 239000006185 dispersion Substances 0.000 claims description 17
- 239000003995 emulsifying agent Substances 0.000 claims description 14
- 239000003999 initiator Substances 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 13
- 229920000642 polymer Polymers 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 11
- 229920001944 Plastisol Polymers 0.000 claims description 10
- 239000004999 plastisol Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- 238000007720 emulsion polymerization reaction Methods 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 125000004432 carbon atom Chemical group C* 0.000 claims description 6
- 238000002844 melting Methods 0.000 claims description 5
- 230000008018 melting Effects 0.000 claims description 5
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 239000004816 latex Substances 0.000 description 15
- 229920000126 latex Polymers 0.000 description 15
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 14
- 239000011164 primary particle Substances 0.000 description 10
- 239000002245 particle Substances 0.000 description 9
- 229960000541 cetyl alcohol Drugs 0.000 description 7
- 239000000839 emulsion Substances 0.000 description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- WFUGQJXVXHBTEM-UHFFFAOYSA-N 2-hydroperoxy-2-(2-hydroperoxybutan-2-ylperoxy)butane Chemical compound CCC(C)(OO)OOC(C)(CC)OO WFUGQJXVXHBTEM-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 3
- 239000002585 base Substances 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 150000002432 hydroperoxides Chemical class 0.000 description 3
- 230000000977 initiatory effect Effects 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 3
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 229940056585 ammonium laurate Drugs 0.000 description 2
- 229940088990 ammonium stearate Drugs 0.000 description 2
- VJCJAQSLASCYAW-UHFFFAOYSA-N azane;dodecanoic acid Chemical compound [NH4+].CCCCCCCCCCCC([O-])=O VJCJAQSLASCYAW-UHFFFAOYSA-N 0.000 description 2
- JPNZKPRONVOMLL-UHFFFAOYSA-N azane;octadecanoic acid Chemical compound [NH4+].CCCCCCCCCCCCCCCCCC([O-])=O JPNZKPRONVOMLL-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 239000011874 heated mixture Substances 0.000 description 2
- 239000000693 micelle Substances 0.000 description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- HLZKNKRTKFSKGZ-UHFFFAOYSA-N tetradecan-1-ol Chemical compound CCCCCCCCCCCCCCO HLZKNKRTKFSKGZ-UHFFFAOYSA-N 0.000 description 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 2
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 1
- QTDIEDOANJISNP-UHFFFAOYSA-N 2-dodecoxyethyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOCCOS(O)(=O)=O QTDIEDOANJISNP-UHFFFAOYSA-N 0.000 description 1
- BIISIZOQPWZPPS-UHFFFAOYSA-N 2-tert-butylperoxypropan-2-ylbenzene Chemical compound CC(C)(C)OOC(C)(C)C1=CC=CC=C1 BIISIZOQPWZPPS-UHFFFAOYSA-N 0.000 description 1
- FRIBMENBGGCKPD-UHFFFAOYSA-N 3-(2,3-dimethoxyphenyl)prop-2-enal Chemical compound COC1=CC=CC(C=CC=O)=C1OC FRIBMENBGGCKPD-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 description 1
- 239000004159 Potassium persulphate Substances 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 230000003679 aging effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 150000008055 alkyl aryl sulfonates Chemical class 0.000 description 1
- -1 alkyl ether sulfate Chemical class 0.000 description 1
- 150000008051 alkyl sulfates Chemical class 0.000 description 1
- 150000008052 alkyl sulfonates Chemical class 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 1
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000010556 emulsion polymerization method Methods 0.000 description 1
- 239000000194 fatty acid Chemical class 0.000 description 1
- 229930195729 fatty acid Chemical class 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 125000005395 methacrylic acid group Chemical class 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229940043348 myristyl alcohol Drugs 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 235000015927 pasta Nutrition 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 description 1
- 235000019394 potassium persulphate Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 150000003856 quaternary ammonium compounds Chemical class 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 229940012831 stearyl alcohol Drugs 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- CIHOLLKRGTVIJN-UHFFFAOYSA-N tert‐butyl hydroperoxide Chemical compound CC(C)(C)OO CIHOLLKRGTVIJN-UHFFFAOYSA-N 0.000 description 1
- 229920001567 vinyl ester resin Polymers 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F14/02—Monomers containing chlorine
- C08F14/04—Monomers containing two carbon atoms
- C08F14/06—Vinyl chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polymerisation Methods In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE7507570A SE405255C (sv) | 1975-07-01 | 1975-07-01 | Forfarande for framstellning av vinylkloridpolymerer genom emulsionspolymerisation i nervaro av alifatisk alkohol innehallande 14-24 kolatomer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO762283L true NO762283L (fi) | 1977-01-04 |
| NO147756B NO147756B (no) | 1983-02-28 |
Family
ID=20325035
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO762283A NO147756B (no) | 1975-07-01 | 1976-06-30 | Fremgangsmaate for fremstilling av vinylkloridpolymerisat |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4310649A (fi) |
| JP (1) | JPS526786A (fi) |
| BE (1) | BE843639A (fi) |
| CA (1) | CA1056997A (fi) |
| DE (1) | DE2629655C3 (fi) |
| FI (1) | FI61317C (fi) |
| FR (1) | FR2316252A1 (fi) |
| GB (1) | GB1546600A (fi) |
| NO (1) | NO147756B (fi) |
| SE (1) | SE405255C (fi) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1065540A (en) * | 1975-07-01 | 1979-10-30 | Bela K. Mikofalvy | Process for producing dispersion resins by homo or copolymerization of vinyl or vinylidene halides |
| NO145164C (no) * | 1978-11-06 | 1982-01-27 | Sintef | Fremgangsmaate for fremstilling av polymerlateks. |
| DE3120708A1 (de) * | 1981-05-25 | 1982-12-09 | Basf Ag, 6700 Ludwigshafen | Verfahren zur diskontinuierlichen polymerisation von vinylchlorid |
| DE3210891A1 (de) * | 1982-03-25 | 1983-09-29 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von verpastbaren polymeren des vinylchlorids |
| DE3242088A1 (de) * | 1982-11-13 | 1984-05-17 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von verpastbaren polymeren des vinylchlorids |
| GB8309275D0 (en) * | 1983-04-06 | 1983-05-11 | Allied Colloids Ltd | Dissolution of water soluble polymers in water |
| DE3478448D1 (en) * | 1983-12-03 | 1989-07-06 | Huels Chemische Werke Ag | Process for producing vinyl chloride polymers |
| DE3421354A1 (de) * | 1984-06-08 | 1985-12-12 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung hochmolekularer thermoplastharze |
| JPS61100253A (ja) * | 1984-10-23 | 1986-05-19 | 株式会社 フジ医療器 | 指圧装置 |
| JPH01150959U (fi) * | 1988-04-04 | 1989-10-18 | ||
| JPH068329B2 (ja) * | 1988-12-27 | 1994-02-02 | 信越化学工業株式会社 | 塩化ビニル系重合体の製造方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2531196A (en) * | 1942-10-20 | 1950-11-21 | Du Pont | Vinyl polymers and process for producing the same |
| US2643995A (en) * | 1949-03-25 | 1953-06-30 | Monsanto Chemicals | Emulsion polymerization process |
| GB978875A (fi) * | 1963-03-29 | Ici Ltd | ||
| US3383346A (en) * | 1965-04-07 | 1968-05-14 | Goodyear Tire & Rubber | Particle size control in seed technique emulsion polymerization using hydroxyl group-containing modifier |
| GB1102980A (en) * | 1966-01-31 | 1968-02-14 | Kanegafuchi Chemical Ind | Improvements in and relating to the preparation of vinyl chloride polymers |
| DE1770817A1 (de) * | 1968-07-06 | 1972-01-13 | Huels Chemische Werke Ag | Verfahren zur Herstellung von Polyvinylchlorid |
| US3755225A (en) * | 1971-08-17 | 1973-08-28 | Diamond Shamrock Corp | Process for preparing homo- and copolymers of vinyl chloride in aqueous emulsion with post addition of a water-soluble ethylene oxide-ethylene glycol adduct |
| JPS5339477B2 (fi) * | 1971-12-07 | 1978-10-21 | ||
| JPS5339478B2 (fi) * | 1971-12-13 | 1978-10-21 | ||
| US4071675A (en) * | 1977-03-03 | 1978-01-31 | Stauffer Chemical Company | Emulsion polymerization of vinyl chloride using mixed emulsifier system in a single step in the absence of seed formation |
-
1975
- 1975-07-01 SE SE7507570A patent/SE405255C/xx not_active IP Right Cessation
-
1976
- 1976-06-21 GB GB25690/76A patent/GB1546600A/en not_active Expired
- 1976-06-22 FI FI761817A patent/FI61317C/fi not_active IP Right Cessation
- 1976-06-25 CA CA255,692A patent/CA1056997A/en not_active Expired
- 1976-06-30 FR FR7619871A patent/FR2316252A1/fr active Granted
- 1976-06-30 NO NO762283A patent/NO147756B/no unknown
- 1976-06-30 BE BE168514A patent/BE843639A/xx not_active IP Right Cessation
- 1976-07-01 DE DE2629655A patent/DE2629655C3/de not_active Expired
- 1976-07-01 JP JP51077114A patent/JPS526786A/ja active Granted
-
1978
- 1978-01-23 US US05/871,896 patent/US4310649A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| US4310649A (en) | 1982-01-12 |
| GB1546600A (en) | 1979-05-23 |
| SE405255B (sv) | 1978-11-27 |
| JPS5338188B2 (fi) | 1978-10-13 |
| FR2316252B1 (fi) | 1980-08-01 |
| SE7507570L (sv) | 1977-01-02 |
| SE405255C (sv) | 1985-09-09 |
| DE2629655C3 (de) | 1981-08-27 |
| JPS526786A (en) | 1977-01-19 |
| FI61317C (fi) | 1982-07-12 |
| DE2629655A1 (de) | 1977-01-13 |
| CA1056997A (en) | 1979-06-19 |
| FR2316252A1 (fr) | 1977-01-28 |
| FI761817A (fi) | 1977-01-02 |
| NO147756B (no) | 1983-02-28 |
| FI61317B (fi) | 1982-03-31 |
| BE843639A (fr) | 1976-12-30 |
| DE2629655B2 (de) | 1980-09-25 |
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