NO20064430L - Fjerning av permanganatreduserende forbindelser fra en metanolkarbonyleringsprosesstrom - Google Patents

Fjerning av permanganatreduserende forbindelser fra en metanolkarbonyleringsprosesstrom

Info

Publication number
NO20064430L
NO20064430L NO20064430A NO20064430A NO20064430L NO 20064430 L NO20064430 L NO 20064430L NO 20064430 A NO20064430 A NO 20064430A NO 20064430 A NO20064430 A NO 20064430A NO 20064430 L NO20064430 L NO 20064430L
Authority
NO
Norway
Prior art keywords
methanol carbonylation
removal
carbonylation process
process stream
reducing compounds
Prior art date
Application number
NO20064430A
Other languages
English (en)
Inventor
David A Trueba
Mark O Scates
Raymond J Zinobile
Original Assignee
Celanese Int Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=34911125&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=NO20064430(L) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Celanese Int Corp filed Critical Celanese Int Corp
Publication of NO20064430L publication Critical patent/NO20064430L/no

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/143Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/32Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/324Tray constructions
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08Acetic acid

Abstract

Det beskrives en forbedring av metanolkarbonyleringsprosessen for fremstilling av eddiksyre. Nærmere bestemt beskrives en fremgangsmåte for å redusere dannelsen av alkyljodider og Cs-gkarboksylsyrer ved å fjerne permanganafreduserende forbindelser ("PRC-forbindelser) fra den lette fase av den kondenserte lettforbindelse-toppsfrøm, innbefattende (a) destillering av den lette fase for å danne en PRC-anriket toppsfrøm, og (b) eksfrahering av den fredje toppsfrøm med vann i minst to på hverandre følgende trinn og utskillelse fra denne av én eller flere vandige sfrømmer inneholdende PRC-forbindelser.
NO20064430A 2004-03-02 2006-09-29 Fjerning av permanganatreduserende forbindelser fra en metanolkarbonyleringsprosesstrom NO20064430L (no)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/708,420 US7223886B2 (en) 2004-03-02 2004-03-02 Removal of permanganate reducing compounds from methanol carbonylation process stream
PCT/US2005/006092 WO2005085166A1 (en) 2004-03-02 2005-02-24 Removal of permanganate reducing compounds from methanol carbonylation process stream

Publications (1)

Publication Number Publication Date
NO20064430L true NO20064430L (no) 2006-09-29

Family

ID=34911125

Family Applications (1)

Application Number Title Priority Date Filing Date
NO20064430A NO20064430L (no) 2004-03-02 2006-09-29 Fjerning av permanganatreduserende forbindelser fra en metanolkarbonyleringsprosesstrom

Country Status (20)

Country Link
US (2) US7223886B2 (no)
EP (2) EP1720821B1 (no)
JP (4) JP2007526310A (no)
KR (2) KR20060129428A (no)
CN (1) CN100522916C (no)
AR (1) AR048247A1 (no)
AU (1) AU2005219834B2 (no)
BR (1) BRPI0508438B1 (no)
CA (1) CA2556998C (no)
ES (2) ES2859449T3 (no)
MY (2) MY139400A (no)
NO (1) NO20064430L (no)
NZ (1) NZ549260A (no)
PL (1) PL209551B1 (no)
RS (1) RS20060494A (no)
RU (1) RU2372321C2 (no)
TW (2) TWI433834B (no)
UA (1) UA84906C2 (no)
WO (1) WO2005085166A1 (no)
ZA (1) ZA200607203B (no)

Families Citing this family (84)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7223886B2 (en) * 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7208624B2 (en) * 2004-03-02 2007-04-24 Celanese International Corporation Process for producing acetic acid
JP4526381B2 (ja) * 2004-12-27 2010-08-18 ダイセル化学工業株式会社 酢酸の製造方法
US7855306B2 (en) 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
US7619113B2 (en) * 2007-09-27 2009-11-17 Celanese International Corporation Method and apparatus for making acetic acid with improved purification
US7884237B2 (en) * 2008-11-07 2011-02-08 Celanese International Corp. Methanol carbonylation with improved aldehyde removal
US8575403B2 (en) 2010-05-07 2013-11-05 Celanese International Corporation Hydrolysis of ethyl acetate in ethanol separation process
US8680342B2 (en) 2010-05-07 2014-03-25 Celanese International Corporation Process for recovering alcohol produced by hydrogenating an acetic acid feed stream comprising water
JP5837576B2 (ja) 2010-05-18 2015-12-24 セラニーズ・インターナショナル・コーポレーション 過マンガン酸塩還元性化合物を除去することによって酢酸流を精製する方法
US9272970B2 (en) 2010-07-09 2016-03-01 Celanese International Corporation Hydrogenolysis of ethyl acetate in alcohol separation processes
US8710279B2 (en) 2010-07-09 2014-04-29 Celanese International Corporation Hydrogenolysis of ethyl acetate in alcohol separation processes
US8664454B2 (en) 2010-07-09 2014-03-04 Celanese International Corporation Process for production of ethanol using a mixed feed using copper containing catalyst
WO2012148509A1 (en) 2011-04-26 2012-11-01 Celanese International Corporation Process for producing ethanol using a stacked bed reactor
US9024083B2 (en) 2010-07-09 2015-05-05 Celanese International Corporation Process for the production of ethanol from an acetic acid feed and a recycled ethyl acetate feed
US8846988B2 (en) 2010-07-09 2014-09-30 Celanese International Corporation Liquid esterification for the production of alcohols
US8378141B2 (en) 2010-08-16 2013-02-19 Celanese International Corporation Process and system for supplying vapor from drying column to light ends column
US8530696B2 (en) 2010-09-24 2013-09-10 Celanese International Corporation Pump around reactor for production of acetic acid
US8877963B2 (en) 2010-09-28 2014-11-04 Celanese International Corporation Production of acetic acid with high conversion rate
US8394988B2 (en) 2010-09-28 2013-03-12 Celanese International Corporation Production of acetic acid with high conversion rate
US8461379B2 (en) 2010-10-12 2013-06-11 Celanese International Corporation Production of acetic acid comprising feeding at least one reactant to a recycle stream
SG189328A1 (en) * 2010-10-13 2013-05-31 Celanese Int Corp Process for recovering halogen promoters and removing permanganate reducing compounds
US8637698B2 (en) 2010-11-19 2014-01-28 Celanese International Corporation Production of acetic acid with an increased production rate
US8563773B2 (en) 2010-12-16 2013-10-22 Celanese International Corporation Eductor-based reactor and pump around loops for production of acetic acid
JP6130300B2 (ja) 2010-12-30 2017-05-17 セラニーズ・インターナショナル・コーポレーション 酢酸生成物流の精製
US8933278B2 (en) 2011-04-26 2015-01-13 Celanese International Corporation Process for producing ethanol and reducing acetic acid concentration
US8686200B2 (en) 2011-04-26 2014-04-01 Celanese International Corporation Process to recover alcohol from an acidic residue stream
US8686199B2 (en) 2011-04-26 2014-04-01 Celanese International Corporation Process for reducing the concentration of acetic acid in a crude alcohol product
US8884081B2 (en) 2011-04-26 2014-11-11 Celanese International Corporation Integrated process for producing acetic acid and alcohol
US9073816B2 (en) 2011-04-26 2015-07-07 Celanese International Corporation Reducing ethyl acetate concentration in recycle streams for ethanol production processes
US8592635B2 (en) 2011-04-26 2013-11-26 Celanese International Corporation Integrated ethanol production by extracting halides from acetic acid
US9000232B2 (en) 2011-04-26 2015-04-07 Celanese International Corporation Extractive distillation of crude alcohol product
US9000233B2 (en) 2011-04-26 2015-04-07 Celanese International Corporation Process to recover alcohol with secondary reactors for hydrolysis of acetal
US8754268B2 (en) 2011-04-26 2014-06-17 Celanese International Corporation Process for removing water from alcohol mixtures
US8927787B2 (en) 2011-04-26 2015-01-06 Celanese International Corporation Process for controlling a reboiler during alcohol recovery and reduced ester formation
US9024085B2 (en) 2011-04-26 2015-05-05 Celanese International Corporation Process to reduce ethanol recycled to hydrogenation reactor
US8927784B2 (en) 2011-04-26 2015-01-06 Celanese International Corporation Process to recover alcohol from an ethyl acetate residue stream
US9024084B2 (en) 2011-04-26 2015-05-05 Celanese International Corporation Reduced energy alcohol separation process having controlled pressure
US8927788B2 (en) 2011-04-26 2015-01-06 Celanese International Corporation Process to recover alcohol with reduced water from overhead of acid column
US8907141B2 (en) 2011-04-26 2014-12-09 Celanese International Corporation Process to recover alcohol with secondary reactors for esterification of acid
US9024082B2 (en) 2011-04-26 2015-05-05 Celanese International Corporation Using a dilute acid stream as an extractive agent
WO2012151377A1 (en) 2011-05-05 2012-11-08 Celanese International Corporation Removal of aromatics from carbonylation process
US8697908B2 (en) 2011-05-05 2014-04-15 Celanese International Corporation Removal of amine compounds from carbonylation process stream containing corrosion metal contaminants
US8895786B2 (en) 2011-08-03 2014-11-25 Celanese International Corporation Processes for increasing alcohol production
US9663437B2 (en) 2011-09-13 2017-05-30 Celanese International Corporation Production of acetic acid with high conversion rate
WO2013070212A1 (en) 2011-11-09 2013-05-16 Celanese International Corporation Producing ethanol using two different streams from acetic acid carbonylation process
US8614359B2 (en) 2011-11-09 2013-12-24 Celanese International Corporation Integrated acid and alcohol production process
WO2013070211A1 (en) 2011-11-09 2013-05-16 Celanese International Corporation Integrated process for producing ethanol from methanol
WO2013070216A1 (en) 2011-11-09 2013-05-16 Celanese International Corporation Integrated ethanol production from methanol via carbonylation and hydrogenation by extracting halides from acetic acid
US8686201B2 (en) * 2011-11-09 2014-04-01 Celanese International Corporation Integrated acid and alcohol production process having flashing to recover acid production catalyst
US8809598B2 (en) 2011-11-09 2014-08-19 Celanese International Corporation Producing ethanol using two different streams from acetic acid carbonylation process
US8704013B2 (en) * 2011-11-09 2014-04-22 Celanese International Corporation Integrated process for producing ethanol
US9079121B2 (en) 2011-12-02 2015-07-14 Celanese International Corporation Distillation column having enlarged downcomers and method of downcomer enlargement
CN103282334B (zh) 2011-12-30 2015-11-25 国际人造丝公司 用于从加氢方法进行乙醇生产和回收的压力驱动蒸馏
BR112013007324B1 (pt) 2012-02-08 2020-10-20 Celanese International Corporation produção de ácido acético com alta taxa de conversão
US8859810B2 (en) * 2012-08-21 2014-10-14 Celanese International Corporation Process for recovering permanganate reducing compounds from an acetic acid production process
SG11201507677VA (en) 2013-03-15 2015-10-29 Celanese Int Corp Process for separating product gas using carbonylation processes
EP3201165B1 (en) 2014-10-02 2019-08-21 Celanese International Corporation Process for producing acetic acid
US9233907B1 (en) 2014-11-14 2016-01-12 Celanese International Corporation Reducing hydrogen iodide content in carbonylation processes
US9458078B2 (en) 2014-11-14 2016-10-04 Celanese International Corporation Processes for producing acetic acid from a reaction medium having low ethyl iodide content
US9302975B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for flashing a reaction medium
US9260369B1 (en) 2014-11-14 2016-02-16 Celanese International Corporation Processes for producing acetic acid product having low butyl acetate content
KR102493738B1 (ko) 2015-01-30 2023-01-30 셀라니즈 인터내셔날 코포레이션 아세트산의 제조 방법
US9561994B2 (en) 2015-01-30 2017-02-07 Celanese International Corporation Processes for producing acetic acid
US9487464B2 (en) 2015-01-30 2016-11-08 Celanese International Corporation Processes for producing acetic acid
WO2016122728A1 (en) 2015-01-30 2016-08-04 Celanese International Corporation Processes for producing acetic acid
US10413840B2 (en) 2015-02-04 2019-09-17 Celanese International Coporation Process to control HI concentration in residuum stream
US9512056B2 (en) 2015-02-04 2016-12-06 Celanese International Corporation Process to control HI concentration in residuum stream
US9505696B2 (en) * 2015-02-04 2016-11-29 Celanese International Corporation Process to control HI concentration in residuum stream
US9382183B1 (en) 2015-07-01 2016-07-05 Celanese International Corporation Process for flashing a reaction medium
US9302974B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for producing acetic acid
US10428006B2 (en) 2015-09-30 2019-10-01 Daicel Corporation Method and apparatus for producing acetic acid
KR102438920B1 (ko) 2015-10-02 2022-08-31 셀라니즈 인터내셔날 코포레이션 물의 재순환과 함께 아세트산을 생산하는 방법
US9957216B2 (en) 2015-11-13 2018-05-01 Celanese International Corporation Processes for producing acetic acid
US9908835B2 (en) 2015-11-13 2018-03-06 Celanese International Corporation Processes for purifying acetic and hydrating anhydride
BR112019008340A2 (pt) 2016-10-28 2019-08-06 Daicel Corp método para produzir ácido acético
CN110049963B (zh) * 2017-01-18 2022-02-18 株式会社大赛璐 乙酸的制备方法
US10428004B2 (en) 2017-01-18 2019-10-01 Daicel Corporation Method for producing acetic acid
ES2792108T3 (es) * 2017-02-07 2020-11-10 Daicel Corp Método de producción de ácido acético
WO2019183549A1 (en) 2018-03-23 2019-09-26 Lyondellbasell Acetyls, Llc Removal of permanganate reducing compounds from intermediate gaa process streams
CN111918857A (zh) 2018-03-23 2020-11-10 利安德巴塞尔乙酰有限责任公司 冰乙酸(gaa)纯化的改进方法
CN110546127B (zh) * 2018-03-27 2022-12-20 株式会社大赛璐 乙酸的制备方法
CN109232223A (zh) * 2018-11-02 2019-01-18 江苏索普(集团)有限公司 一种合成醋酸的工艺
US10807935B2 (en) 2018-11-02 2020-10-20 Celanese International Corporation Process for continuous acetic acid production
WO2021202270A1 (en) 2020-04-01 2021-10-07 Celanese International Corporation Processes for removing and/or reducing permanganate reducing compounds and alkyl iodides

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3769329A (en) 1970-03-12 1973-10-30 Monsanto Co Production of carboxylic acids and esters
US5026908A (en) 1984-05-03 1991-06-25 Hoechst Celanese Corporation Methanol carbonylation process
US5001259A (en) 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
CA1228867A (en) 1984-05-03 1987-11-03 G. Paull Torrence Methanol carbonylation process
US5144068A (en) 1984-05-03 1992-09-01 Hoechst Celanese Corporation Methanol carbonylation process
AU8790391A (en) 1990-11-19 1992-05-21 Hoechst Celanese Corporation Removal of carbonyl impurities from a carbonylation process stream
GB9211671D0 (en) 1992-06-02 1992-07-15 Bp Chem Int Ltd Process
JP3244350B2 (ja) * 1993-07-08 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
JP3244351B2 (ja) * 1993-07-08 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
TW283702B (no) 1993-07-08 1996-08-21 Daicel Chem
JP3244385B2 (ja) * 1994-06-15 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
US5625095A (en) * 1994-06-15 1997-04-29 Daicel Chemical Industries, Ltd. Process for producing high purity acetic acid
JP3058577B2 (ja) * 1994-12-29 2000-07-04 千代田化工建設株式会社 カルボニル化反応方法及び反応器
WO1996033965A1 (fr) * 1995-04-27 1996-10-31 Daicel Chemical Industries, Ltd. Procede de production d'acide acetique
JP3883221B2 (ja) 1995-08-03 2007-02-21 ダイセル化学工業株式会社 アセトアルデヒドの分離除去方法
US5783731A (en) 1995-09-11 1998-07-21 Hoechst Celanese Corporation Removal of carbonyl impurities from a carbonylation process stream
JP3833295B2 (ja) * 1996-02-29 2006-10-11 千代田化工建設株式会社 酢酸の製造方法
US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
IN192600B (no) * 1996-10-18 2004-05-08 Hoechst Celanese Corp
US5935155A (en) 1998-03-13 1999-08-10 John Hopkins University, School Of Medicine Visual prosthesis and method of using same
JP4242952B2 (ja) * 1998-08-31 2009-03-25 ダイセル化学工業株式会社 酢酸の製造方法
US7223886B2 (en) * 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7223883B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream

Also Published As

Publication number Publication date
PL209551B1 (pl) 2011-09-30
JP2016000748A (ja) 2016-01-07
US7223886B2 (en) 2007-05-29
US8076507B2 (en) 2011-12-13
UA84906C2 (ru) 2008-12-10
RU2372321C2 (ru) 2009-11-10
BRPI0508438B1 (pt) 2016-07-26
KR101233605B1 (ko) 2013-02-14
TW200602311A (en) 2006-01-16
EP3486228B1 (en) 2020-12-02
PL381109A1 (pl) 2007-04-30
TW201204699A (en) 2012-02-01
WO2005085166A1 (en) 2005-09-15
US20050197508A1 (en) 2005-09-08
ES2859449T3 (es) 2021-10-04
US20080103335A1 (en) 2008-05-01
JP6506657B2 (ja) 2019-04-24
CN1926087A (zh) 2007-03-07
CN100522916C (zh) 2009-08-05
MY148351A (en) 2013-03-29
AR048247A1 (es) 2006-04-12
AU2005219834B2 (en) 2011-09-15
EP1720821A1 (en) 2006-11-15
ZA200607203B (en) 2007-12-27
AU2005219834A1 (en) 2005-09-15
JP2007526310A (ja) 2007-09-13
RU2006134649A (ru) 2008-04-10
JP6465934B2 (ja) 2019-02-06
NZ549260A (en) 2009-04-30
TWI433834B (zh) 2014-04-11
JP2018009009A (ja) 2018-01-18
BRPI0508438A (pt) 2007-07-24
TWI549939B (zh) 2016-09-21
EP1720821B1 (en) 2018-12-26
KR20120050537A (ko) 2012-05-18
ES2714170T3 (es) 2019-05-27
EP3486228A1 (en) 2019-05-22
JP2013082715A (ja) 2013-05-09
CA2556998C (en) 2013-07-02
CA2556998A1 (en) 2005-09-15
MY139400A (en) 2009-09-30
RS20060494A (en) 2008-09-29
KR20060129428A (ko) 2006-12-15

Similar Documents

Publication Publication Date Title
NO20064430L (no) Fjerning av permanganatreduserende forbindelser fra en metanolkarbonyleringsprosesstrom
NO20064427L (no) Fjerning av permanganatreduserende forbindelser fra en metanolkarbonyleringsprosesstrom
CA2605494A1 (en) Process for the production of acetic acid
TW430647B (en) Removal of acetaldehyde from a carbonylation process stream
JP2007526310A5 (no)
CA2467001A1 (en) Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid
WO2008016502A3 (en) Preparation of acetic acid
MY142041A (en) Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid
AR048248A1 (es) Metodo de control para procedimiento de eliminacion de compuestos de reduccion de permanganato de la corriente del procedimiento de carbonilacion de metanol y un metodo para la produccion de acido acetico.
NZ597205A (en) Recovery of butanol from a mixture of butanol, water and an organic extractant
WO2010010298A3 (fr) Procede de fabrication d'acide propionique bio-ressource a partir de glycerol
JP2014500856A5 (no)
MX341499B (es) Método y aparato para la fabricación de ácido acético con purificación mejorada.
NO20085357L (no) Fremgangsmate for fremstilling av renset hydrokinon og dannelse av det samme
WO2009120257A1 (en) Purification of acetic acid from wood acetylation process
CA2460795A1 (en) Propylene oxide purification
ATE532763T1 (de) Verfahren zur herstellung von hochreinem monopentaerythritol
RU2011143873A (ru) Удаление примесей углеводородов из полупродуктов производства уксусной кислоты
NO20085360L (no) Fremgangsmate for separering og rensing av hydrokinon fra rablandinger
TH74700B (th) การกำจัดสารประกอบเพื่อการรีดิวส์เพอร์แมงกาเนทจากกระแสของกรรมวิธีคาร์บอนิเลชันของเมธานอล
SE9800957D0 (sv) Förfarande vid upparbetning av en synteslösning innefattande en 1,3-dioxankarboxylsyra
JP2006232746A (ja) レゾルシンの精製方法
JP2005298381A (ja) 4,4,4−トリフルオロブタン−1−オールの精製方法

Legal Events

Date Code Title Description
FC2A Withdrawal, rejection or dismissal of laid open patent application