NO129126B - - Google Patents
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- Publication number
- NO129126B NO129126B NO04857/68A NO485768A NO129126B NO 129126 B NO129126 B NO 129126B NO 04857/68 A NO04857/68 A NO 04857/68A NO 485768 A NO485768 A NO 485768A NO 129126 B NO129126 B NO 129126B
- Authority
- NO
- Norway
- Prior art keywords
- reaction mixture
- ammonia
- reaction
- zone
- section
- Prior art date
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 193
- 229910021529 ammonia Inorganic materials 0.000 claims description 87
- 239000011541 reaction mixture Substances 0.000 claims description 83
- 238000002156 mixing Methods 0.000 claims description 55
- 238000006243 chemical reaction Methods 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 229910001868 water Inorganic materials 0.000 claims description 25
- 239000003795 chemical substances by application Substances 0.000 claims description 21
- 239000010802 sludge Substances 0.000 claims description 20
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 18
- 150000003863 ammonium salts Chemical class 0.000 claims description 17
- 239000007791 liquid phase Substances 0.000 claims description 17
- 239000003337 fertilizer Substances 0.000 claims description 15
- 238000001035 drying Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 239000001103 potassium chloride Substances 0.000 claims description 9
- 235000011164 potassium chloride Nutrition 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 8
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims description 7
- 150000007513 acids Chemical class 0.000 claims description 7
- 230000000694 effects Effects 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 230000002378 acidificating effect Effects 0.000 claims description 6
- 238000001704 evaporation Methods 0.000 claims description 6
- 230000008569 process Effects 0.000 claims description 6
- 230000004888 barrier function Effects 0.000 claims description 5
- 230000008020 evaporation Effects 0.000 claims description 5
- 238000006386 neutralization reaction Methods 0.000 claims description 3
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims description 2
- 229910052939 potassium sulfate Inorganic materials 0.000 claims description 2
- 235000011151 potassium sulphates Nutrition 0.000 claims description 2
- 238000000227 grinding Methods 0.000 claims 1
- 239000012258 stirred mixture Substances 0.000 claims 1
- 238000011144 upstream manufacturing Methods 0.000 claims 1
- 239000002253 acid Substances 0.000 description 25
- 239000000047 product Substances 0.000 description 20
- YYRMJZQKEFZXMX-UHFFFAOYSA-N calcium;phosphoric acid Chemical compound [Ca+2].OP(O)(O)=O.OP(O)(O)=O YYRMJZQKEFZXMX-UHFFFAOYSA-N 0.000 description 17
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 16
- 239000002426 superphosphate Substances 0.000 description 16
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 12
- 238000004898 kneading Methods 0.000 description 9
- 125000005341 metaphosphate group Chemical group 0.000 description 9
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 8
- 239000007788 liquid Substances 0.000 description 8
- 238000002360 preparation method Methods 0.000 description 8
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 7
- 239000011591 potassium Substances 0.000 description 7
- 229910052700 potassium Inorganic materials 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- 230000007480 spreading Effects 0.000 description 6
- 238000003892 spreading Methods 0.000 description 6
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 description 5
- 229910000389 calcium phosphate Inorganic materials 0.000 description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 description 5
- 239000011707 mineral Substances 0.000 description 5
- 235000010755 mineral Nutrition 0.000 description 5
- 235000019691 monocalcium phosphate Nutrition 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- 239000004254 Ammonium phosphate Substances 0.000 description 4
- 235000019289 ammonium phosphates Nutrition 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 230000007062 hydrolysis Effects 0.000 description 4
- 238000006460 hydrolysis reaction Methods 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 229920006395 saturated elastomer Polymers 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- ZRIUUUJAJJNDSS-UHFFFAOYSA-N ammonium phosphates Chemical class [NH4+].[NH4+].[NH4+].[O-]P([O-])([O-])=O ZRIUUUJAJJNDSS-UHFFFAOYSA-N 0.000 description 3
- ROPDWRCJTIRLTR-UHFFFAOYSA-L calcium metaphosphate Chemical compound [Ca+2].[O-]P(=O)=O.[O-]P(=O)=O ROPDWRCJTIRLTR-UHFFFAOYSA-L 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 239000011343 solid material Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000013459 approach Methods 0.000 description 2
- 230000001174 ascending effect Effects 0.000 description 2
- 159000000007 calcium salts Chemical class 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- MOMKYJPSVWEWPM-UHFFFAOYSA-N 4-(chloromethyl)-2-(4-methylphenyl)-1,3-thiazole Chemical compound C1=CC(C)=CC=C1C1=NC(CCl)=CS1 MOMKYJPSVWEWPM-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 235000019739 Dicalciumphosphate Nutrition 0.000 description 1
- 240000001973 Ficus microcarpa Species 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 108010074506 Transfer Factor Proteins 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 229910000148 ammonium phosphate Inorganic materials 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 239000001166 ammonium sulphate Substances 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 1
- NEFBYIFKOOEVPA-UHFFFAOYSA-K dicalcium phosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])([O-])=O NEFBYIFKOOEVPA-UHFFFAOYSA-K 0.000 description 1
- 229910000390 dicalcium phosphate Inorganic materials 0.000 description 1
- 229940038472 dicalcium phosphate Drugs 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 239000010440 gypsum Substances 0.000 description 1
- 229910052602 gypsum Inorganic materials 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- OQZCJRJRGMMSGK-UHFFFAOYSA-M potassium metaphosphate Chemical compound [K+].[O-]P(=O)=O OQZCJRJRGMMSGK-UHFFFAOYSA-M 0.000 description 1
- 229940099402 potassium metaphosphate Drugs 0.000 description 1
- 239000001120 potassium sulphate Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 235000019983 sodium metaphosphate Nutrition 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B5/00—Measuring for diagnostic purposes; Identification of persons
- A61B5/15—Devices for taking samples of blood
- A61B5/150007—Details
- A61B5/150015—Source of blood
- A61B5/15003—Source of blood for venous or arterial blood
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B5/00—Measuring for diagnostic purposes; Identification of persons
- A61B5/15—Devices for taking samples of blood
- A61B5/150007—Details
- A61B5/150351—Caps, stoppers or lids for sealing or closing a blood collection vessel or container, e.g. a test-tube or syringe barrel
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B5/00—Measuring for diagnostic purposes; Identification of persons
- A61B5/15—Devices for taking samples of blood
- A61B5/150007—Details
- A61B5/150374—Details of piercing elements or protective means for preventing accidental injuries by such piercing elements
- A61B5/150381—Design of piercing elements
- A61B5/150389—Hollow piercing elements, e.g. canulas, needles, for piercing the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B5/00—Measuring for diagnostic purposes; Identification of persons
- A61B5/15—Devices for taking samples of blood
- A61B5/150007—Details
- A61B5/150374—Details of piercing elements or protective means for preventing accidental injuries by such piercing elements
- A61B5/150381—Design of piercing elements
- A61B5/150473—Double-ended needles, e.g. used with pre-evacuated sampling tubes
- A61B5/150496—Details of construction of hub, i.e. element used to attach the double-ended needle to a piercing device or sampling device
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B5/00—Measuring for diagnostic purposes; Identification of persons
- A61B5/15—Devices for taking samples of blood
- A61B5/150007—Details
- A61B5/150732—Needle holders, for instance for holding the needle by the hub, used for example with double-ended needle and pre-evacuated tube
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B5/00—Measuring for diagnostic purposes; Identification of persons
- A61B5/15—Devices for taking samples of blood
- A61B5/153—Devices specially adapted for taking samples of venous or arterial blood, e.g. with syringes
- A61B5/154—Devices using pre-evacuated means
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US68819067A | 1967-12-05 | 1967-12-05 | |
| US68808567A | 1967-12-05 | 1967-12-05 | |
| US68813267A | 1967-12-05 | 1967-12-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO129126B true NO129126B (de) | 1974-03-04 |
Family
ID=27418502
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO04857/68A NO129126B (de) | 1967-12-05 | 1968-12-04 |
Country Status (15)
| Country | Link |
|---|---|
| BE (1) | BE725011A (de) |
| BR (1) | BR6804631D0 (de) |
| CA (1) | CA928600A (de) |
| CH (1) | CH480057A (de) |
| DE (3) | DE1818046C2 (de) |
| DK (1) | DK122430B (de) |
| ES (1) | ES361060A1 (de) |
| FI (1) | FI53362C (de) |
| FR (1) | FR1593474A (de) |
| IE (1) | IE32583B1 (de) |
| IL (1) | IL31211A (de) |
| NL (1) | NL6817366A (de) |
| NO (1) | NO129126B (de) |
| RO (1) | RO57807A (de) |
| SE (1) | SE350843B (de) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1009110A (en) * | 1971-04-30 | 1977-04-26 | Abbott Laboratories | Blood collecting assembly |
| FR2268707B1 (de) * | 1974-04-26 | 1976-12-17 | Becton Dickinson France | |
| US4106497A (en) * | 1977-02-04 | 1978-08-15 | Becton, Dickinson And Company | Multiple sample needle assembly with indicator means |
| DE2828088A1 (de) * | 1978-06-27 | 1980-01-10 | Riedel De Haen Ag | Vorrichtung zur kontaminationsfreien probenahme von fluessigkeiten |
| DE2948653C2 (de) * | 1979-12-04 | 1984-01-05 | Walter Sarstedt Kunststoff-Spritzgußwerk, 5223 Nümbrecht | Blutentnahmevorrichtung |
| DE3049503C2 (de) * | 1980-12-30 | 1983-04-28 | Walter Sarstedt Kunststoff-Spritzgußwerk, 5223 Nümbrecht | "Blutentnahmevorrichtung" |
| DE8504693U1 (de) * | 1985-02-20 | 1986-01-02 | KABE Labortechnik GmbH, 5223 Nümbrecht | Blutentnahmevorrichtung |
| DE4019197A1 (de) * | 1990-06-15 | 1992-01-02 | Charles Dr Med Bannerman | Kanuele zur blutentnahme und zur injektion |
| IT1246994B (it) * | 1991-01-10 | 1994-12-12 | Diesse Diagnostica | Tappo perforabile atto al prelievo del sangue con dispositivi a doppio ago in provette sotto vuoto |
| IL101680A (en) * | 1992-04-23 | 1995-08-31 | Travenol Lab Israel Ltd | Blood sampling device |
| DE19617000C1 (de) * | 1996-04-27 | 1998-01-22 | Sarstedt Walter Geraete | Blutentnahmevorrichtung mit einem eine Kanüle aufweisenden Halter |
| DE10028482B4 (de) | 2000-06-08 | 2004-09-16 | Kabe-Labortechnik Gmbh | Behältnis für die Entnahme von Proben und insbesondere Blutproben |
| DE20301575U1 (de) | 2003-01-31 | 2003-06-05 | Sarstedt Ag & Co | Blutentnahmevorrichtung mit einem eine Kanüle aufweisenden Halter |
| CN104470432B (zh) * | 2012-08-02 | 2016-10-12 | 张建铭 | 具有针尖保护的针筒式真空采血器 |
| CN104470433B (zh) * | 2012-08-02 | 2017-07-14 | 张建铭 | 具有留置导管的整体式真空采血装置 |
| CN104470436B (zh) * | 2012-08-02 | 2017-04-26 | 张建铭 | 整体式真空采血装置 |
| WO2014063344A1 (zh) * | 2012-10-26 | 2014-05-01 | Zhang Jianming | 具有针尖保护套的整体式真空采血装置 |
| WO2014063347A1 (zh) * | 2012-10-26 | 2014-05-01 | Zhang Jianming | 具有针尖保护套的自动撤针整体式真空采血装置 |
| ES2675824B1 (es) * | 2017-01-12 | 2019-04-29 | Biotechnology Inst I Mas D Sl | Dispositivo contenedor para la recoleccion, el almacenamiento y el procesado de sangre o de un compuesto sanguineo |
-
1968
- 1968-11-21 CA CA035816A patent/CA928600A/en not_active Expired
- 1968-11-27 FR FR1593474D patent/FR1593474A/fr not_active Expired
- 1968-12-03 IL IL31211A patent/IL31211A/xx unknown
- 1968-12-03 SE SE16507/68A patent/SE350843B/xx unknown
- 1968-12-04 NO NO04857/68A patent/NO129126B/no unknown
- 1968-12-04 DK DK591668AA patent/DK122430B/da not_active IP Right Cessation
- 1968-12-04 DE DE1818046A patent/DE1818046C2/de not_active Expired
- 1968-12-04 NL NL6817366A patent/NL6817366A/xx unknown
- 1968-12-04 ES ES361060A patent/ES361060A1/es not_active Expired
- 1968-12-04 DE DE6809915U patent/DE6809915U/de not_active Expired
- 1968-12-04 DE DE1812742A patent/DE1812742C3/de not_active Expired
- 1968-12-05 CH CH1829968A patent/CH480057A/de not_active IP Right Cessation
- 1968-12-05 BR BR204631/68A patent/BR6804631D0/pt unknown
- 1968-12-05 IE IE1482/68A patent/IE32583B1/xx unknown
- 1968-12-05 BE BE725011D patent/BE725011A/xx not_active Expired
- 1968-12-05 FI FI3500/68A patent/FI53362C/fi active
- 1968-12-05 RO RO58401A patent/RO57807A/ro unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IL31211A0 (en) | 1969-02-27 |
| IE32583L (en) | 1969-06-05 |
| DE1812742A1 (de) | 1969-07-03 |
| DE1812742C3 (de) | 1980-04-10 |
| ES361060A1 (es) | 1970-12-01 |
| SE350843B (de) | 1972-11-06 |
| RO57807A (de) | 1975-03-15 |
| DE1818046C2 (de) | 1980-10-23 |
| BR6804631D0 (pt) | 1973-04-26 |
| FR1593474A (de) | 1970-05-25 |
| FI53362B (de) | 1977-12-30 |
| BE725011A (de) | 1969-05-16 |
| DE1818046B1 (de) | 1980-03-13 |
| IE32583B1 (en) | 1973-09-19 |
| NL6817366A (de) | 1969-06-09 |
| DE6809915U (de) | 1980-07-31 |
| CA928600A (en) | 1973-06-19 |
| DK122430B (da) | 1972-03-06 |
| CH480057A (de) | 1969-10-31 |
| IL31211A (en) | 1973-01-30 |
| DE1812742B2 (de) | 1979-08-02 |
| FI53362C (fi) | 1978-04-10 |
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