NL8301590A - Synthetische, kristallijne en poreuze materialen die silicium- en boriumoxyden bevatten, werkwijzen voor hun bereiding en hun toepassingen. - Google Patents
Synthetische, kristallijne en poreuze materialen die silicium- en boriumoxyden bevatten, werkwijzen voor hun bereiding en hun toepassingen. Download PDFInfo
- Publication number
- NL8301590A NL8301590A NL8301590A NL8301590A NL8301590A NL 8301590 A NL8301590 A NL 8301590A NL 8301590 A NL8301590 A NL 8301590A NL 8301590 A NL8301590 A NL 8301590A NL 8301590 A NL8301590 A NL 8301590A
- Authority
- NL
- Netherlands
- Prior art keywords
- crystalline
- synthetic
- porous materials
- materials according
- cation
- Prior art date
Links
- 239000002178 crystalline material Substances 0.000 title claims description 12
- 239000011148 porous material Substances 0.000 title claims description 12
- 239000010703 silicon Substances 0.000 title claims description 9
- 238000000034 method Methods 0.000 title description 6
- 238000002360 preparation method Methods 0.000 title description 6
- 229910052710 silicon Inorganic materials 0.000 title description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 14
- 239000002585 base Substances 0.000 claims description 10
- 238000001228 spectrum Methods 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 9
- VDZOOKBUILJEDG-UHFFFAOYSA-M tetrabutylammonium hydroxide Chemical compound [OH-].CCCC[N+](CCCC)(CCCC)CCCC VDZOOKBUILJEDG-UHFFFAOYSA-M 0.000 claims description 9
- 238000002441 X-ray diffraction Methods 0.000 claims description 7
- 150000001768 cations Chemical class 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 7
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- WGTYBPLFGIVFAS-UHFFFAOYSA-M tetramethylammonium hydroxide Substances [OH-].C[N+](C)(C)C WGTYBPLFGIVFAS-UHFFFAOYSA-M 0.000 claims description 6
- 150000001639 boron compounds Chemical class 0.000 claims description 5
- 229910052810 boron oxide Inorganic materials 0.000 claims description 5
- MOWNZPNSYMGTMD-UHFFFAOYSA-N oxidoboron Chemical class O=[B] MOWNZPNSYMGTMD-UHFFFAOYSA-N 0.000 claims description 5
- 229910052814 silicon oxide Inorganic materials 0.000 claims description 5
- QEMXHQIAXOOASZ-UHFFFAOYSA-N tetramethylammonium Chemical compound C[N+](C)(C)C QEMXHQIAXOOASZ-UHFFFAOYSA-N 0.000 claims description 5
- -1 NH4 cation Chemical class 0.000 claims description 4
- 229910021538 borax Inorganic materials 0.000 claims description 4
- 150000001642 boronic acid derivatives Chemical class 0.000 claims description 4
- 150000003377 silicon compounds Chemical class 0.000 claims description 4
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 4
- QVOFCQBZXGLNAA-UHFFFAOYSA-M tributyl(methyl)azanium;hydroxide Chemical group [OH-].CCCC[N+](C)(CCCC)CCCC QVOFCQBZXGLNAA-UHFFFAOYSA-M 0.000 claims description 4
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 3
- 239000004327 boric acid Substances 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 235000012239 silicon dioxide Nutrition 0.000 claims description 3
- 229910002012 Aerosil® Inorganic materials 0.000 claims description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 2
- 239000004115 Sodium Silicate Substances 0.000 claims description 2
- JLMKXBLSZPRYPU-UHFFFAOYSA-N [OH-].C(CCC)[NH2+]C Chemical compound [OH-].C(CCC)[NH2+]C JLMKXBLSZPRYPU-UHFFFAOYSA-N 0.000 claims description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 2
- 239000000908 ammonium hydroxide Substances 0.000 claims description 2
- 235000010338 boric acid Nutrition 0.000 claims description 2
- IJRVQAXSAHHCNH-UHFFFAOYSA-M butyl(trimethyl)azanium;hydroxide Chemical group [OH-].CCCC[N+](C)(C)C IJRVQAXSAHHCNH-UHFFFAOYSA-M 0.000 claims description 2
- 229910052605 nesosilicate Inorganic materials 0.000 claims description 2
- 150000004762 orthosilicates Chemical class 0.000 claims description 2
- 229910002027 silica gel Inorganic materials 0.000 claims description 2
- 239000000741 silica gel Substances 0.000 claims description 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 2
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 2
- 239000004328 sodium tetraborate Substances 0.000 claims description 2
- DZLFLBLQUQXARW-UHFFFAOYSA-N tetrabutylammonium Chemical compound CCCC[N+](CCCC)(CCCC)CCCC DZLFLBLQUQXARW-UHFFFAOYSA-N 0.000 claims description 2
- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 claims description 2
- QCOGKXLOEWLIDC-UHFFFAOYSA-O butyl(methyl)azanium Chemical group CCCC[NH2+]C QCOGKXLOEWLIDC-UHFFFAOYSA-O 0.000 claims 3
- 229910052681 coesite Inorganic materials 0.000 claims 2
- 239000000470 constituent Substances 0.000 claims 2
- 229910052906 cristobalite Inorganic materials 0.000 claims 2
- 229910052682 stishovite Inorganic materials 0.000 claims 2
- 229910052905 tridymite Inorganic materials 0.000 claims 2
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 239000008119 colloidal silica Substances 0.000 claims 1
- HVMLGVVFRKCJOV-UHFFFAOYSA-N dibutyl(dimethyl)azanium Chemical group CCCC[N+](C)(C)CCCC HVMLGVVFRKCJOV-UHFFFAOYSA-N 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 7
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 229920002994 synthetic fiber Polymers 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 2
- 239000005695 Ammonium acetate Substances 0.000 description 2
- 108091065810 E family Proteins 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 235000019257 ammonium acetate Nutrition 0.000 description 2
- 229940043376 ammonium acetate Drugs 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 229940075614 colloidal silicon dioxide Drugs 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- KFJNCGCKGILQMF-UHFFFAOYSA-M dibutyl(dimethyl)azanium;hydroxide Chemical compound [OH-].CCCC[N+](C)(C)CCCC KFJNCGCKGILQMF-UHFFFAOYSA-M 0.000 description 2
- 125000001453 quaternary ammonium group Chemical group 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 125000005207 tetraalkylammonium group Chemical group 0.000 description 2
- CBXCPBUEXACCNR-UHFFFAOYSA-N tetraethylammonium Chemical compound CC[N+](CC)(CC)CC CBXCPBUEXACCNR-UHFFFAOYSA-N 0.000 description 2
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229910001413 alkali metal ion Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000005297 pyrex Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 125000003698 tetramethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 1
- OSBSFAARYOCBHB-UHFFFAOYSA-N tetrapropylammonium Chemical compound CCC[N+](CCC)(CCC)CCC OSBSFAARYOCBHB-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
- C01B35/10—Compounds containing boron and oxygen
- C01B35/1009—Compounds containing boron and oxygen having molecular-sieve properties
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
- C01B33/10—Compounds containing silicon, fluorine, and other elements
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Catalysts (AREA)
- Silicon Compounds (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT21132/82A IT1157932B (it) | 1982-05-07 | 1982-05-07 | Materiali sintetici, cristallini, porosi costituiti da ossidi di silicio e boro, loro metodo di preparazione e loro usi |
| IT2113282 | 1982-05-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NL8301590A true NL8301590A (nl) | 1983-12-01 |
Family
ID=11177209
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NL8301590A NL8301590A (nl) | 1982-05-07 | 1983-05-04 | Synthetische, kristallijne en poreuze materialen die silicium- en boriumoxyden bevatten, werkwijzen voor hun bereiding en hun toepassingen. |
Country Status (23)
| Country | Link |
|---|---|
| JP (1) | JPS58208129A (en:Method) |
| KR (1) | KR840004534A (en:Method) |
| AU (1) | AU1383983A (en:Method) |
| BE (1) | BE896686A (en:Method) |
| BR (1) | BR8302358A (en:Method) |
| DD (1) | DD209795A5 (en:Method) |
| DE (1) | DE3316488A1 (en:Method) |
| DK (1) | DK195883A (en:Method) |
| ES (1) | ES522608A0 (en:Method) |
| FR (1) | FR2526414A1 (en:Method) |
| GB (1) | GB2120226B (en:Method) |
| GR (1) | GR78258B (en:Method) |
| IL (1) | IL68543A0 (en:Method) |
| IT (1) | IT1157932B (en:Method) |
| LU (1) | LU84790A1 (en:Method) |
| NL (1) | NL8301590A (en:Method) |
| NO (1) | NO831584L (en:Method) |
| PL (1) | PL241838A1 (en:Method) |
| PT (1) | PT76656B (en:Method) |
| SE (1) | SE8302576L (en:Method) |
| YU (1) | YU95483A (en:Method) |
| ZA (1) | ZA832934B (en:Method) |
| ZW (1) | ZW9183A1 (en:Method) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2582639B1 (fr) * | 1985-05-28 | 1987-08-28 | Centre Nat Rech Scient | Nouveau procede de synthese de zeolites du type borosilicate, produits ainsi obtenus et leur utilisation |
| IT1213504B (it) | 1986-10-22 | 1989-12-20 | Eniricerche Spa | Zeoliti legate e procedimenye per la loro prosuzione. |
| AU634962B2 (en) * | 1988-06-10 | 1993-03-11 | Kohmix Co., Ltd. | Water-Soluble, film-forming inorganic compounds |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IN146957B (en:Method) * | 1976-10-18 | 1979-10-20 | Standard Oil Co | |
| GR66589B (en:Method) * | 1978-06-22 | 1981-03-30 | Snam Progetti | |
| US4331641A (en) * | 1979-11-07 | 1982-05-25 | National Distillers & Chemical Corp. | Synthetic crystalline metal silicate compositions and preparation thereof |
-
1982
- 1982-05-07 IT IT21132/82A patent/IT1157932B/it active
-
1983
- 1983-04-11 GR GR71163A patent/GR78258B/el unknown
- 1983-04-21 AU AU13839/83A patent/AU1383983A/en not_active Abandoned
- 1983-04-22 ZW ZW91/83A patent/ZW9183A1/xx unknown
- 1983-04-26 ZA ZA832934A patent/ZA832934B/xx unknown
- 1983-04-26 GB GB08311310A patent/GB2120226B/en not_active Expired
- 1983-04-27 YU YU00954/83A patent/YU95483A/xx unknown
- 1983-05-01 IL IL68543A patent/IL68543A0/xx unknown
- 1983-05-03 BR BR8302358A patent/BR8302358A/pt unknown
- 1983-05-03 DK DK195883A patent/DK195883A/da not_active Application Discontinuation
- 1983-05-04 NL NL8301590A patent/NL8301590A/nl not_active Application Discontinuation
- 1983-05-05 NO NO831584A patent/NO831584L/no unknown
- 1983-05-05 FR FR8307488A patent/FR2526414A1/fr active Granted
- 1983-05-05 DE DE19833316488 patent/DE3316488A1/de not_active Ceased
- 1983-05-05 SE SE8302576A patent/SE8302576L/ not_active Application Discontinuation
- 1983-05-06 JP JP58078389A patent/JPS58208129A/ja active Pending
- 1983-05-06 PT PT76656A patent/PT76656B/pt unknown
- 1983-05-06 ES ES522608A patent/ES522608A0/es active Granted
- 1983-05-06 DD DD83250710A patent/DD209795A5/de unknown
- 1983-05-06 LU LU84790A patent/LU84790A1/fr unknown
- 1983-05-06 PL PL24183883A patent/PL241838A1/xx unknown
- 1983-05-06 BE BE0/210720A patent/BE896686A/fr not_active IP Right Cessation
- 1983-05-07 KR KR1019830001960A patent/KR840004534A/ko not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| PT76656B (en) | 1986-04-16 |
| YU95483A (en) | 1985-10-31 |
| PL241838A1 (en) | 1984-06-18 |
| FR2526414B1 (en:Method) | 1985-04-19 |
| SE8302576D0 (sv) | 1983-05-05 |
| SE8302576L (sv) | 1983-11-08 |
| ZW9183A1 (en) | 1983-07-20 |
| LU84790A1 (fr) | 1984-03-07 |
| IL68543A0 (en) | 1983-09-30 |
| DK195883A (da) | 1983-11-08 |
| KR840004534A (ko) | 1984-10-22 |
| ES8406380A1 (es) | 1984-08-01 |
| DD209795A5 (de) | 1984-05-23 |
| JPS58208129A (ja) | 1983-12-03 |
| AU1383983A (en) | 1983-11-10 |
| FR2526414A1 (fr) | 1983-11-10 |
| GR78258B (en:Method) | 1984-09-26 |
| PT76656A (en) | 1983-06-01 |
| GB2120226A (en) | 1983-11-30 |
| DE3316488A1 (de) | 1983-11-10 |
| BR8302358A (pt) | 1984-01-10 |
| IT8221132A0 (it) | 1982-05-07 |
| IT1157932B (it) | 1987-02-18 |
| DK195883D0 (da) | 1983-05-03 |
| ES522608A0 (es) | 1984-08-01 |
| NO831584L (no) | 1983-11-08 |
| GB8311310D0 (en) | 1983-06-02 |
| GB2120226B (en) | 1985-10-23 |
| ZA832934B (en) | 1984-04-25 |
| BE896686A (fr) | 1983-11-07 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4476327A (en) | Process for the synthesis of glycol monomethylethers | |
| EP0100119B1 (en) | Process for the epoxidation of olefinic compounds | |
| NL8006939A (nl) | Poreus kristallijn materiaal bestaande uit silicium- en titaniumoxyden alsmede werkwijze voor de bereiding en toepassing daarvan. | |
| BE1001038A7 (fr) | Procede pour la preparation de materiaux synthetiques cristallins poreux constitues d'oxydes de silicium et de titane. | |
| JP2613790B2 (ja) | ゼオライト系合成物質及びその製法 | |
| KR100322780B1 (ko) | 실리콘 함유 화합물로 개질시킨 제올라이트 촉매를 사용하여 트리에틸렌디아민 및 피페라진을 합성하는 방법 | |
| EP2236461B1 (en) | Method for synthesizing all-silica zeolite beta with small crystal size | |
| EP0266825B1 (en) | Synthetic, crystalline, porous material containing oxides of silicon, titanium and gallium | |
| ITMI972250A1 (it) | Processo per preparare zeoliti legate | |
| US5474754A (en) | Preparation of an aluminosilicotitanate isomorphous with zeolite beta | |
| SU1739843A3 (ru) | Способ получени окси-и метоксипроизводных дифенилметана | |
| JP2001278619A (ja) | 結晶質固体の製造方法 | |
| EP0264744B1 (en) | Process for the preparation of 4,4'-diaminodiphenylmethane and its derivatives | |
| JPH08253313A (ja) | 合成ゼオライト物質 | |
| US5064629A (en) | Titanium-boron-oxide, synthetic materials based thereon and method of preparing the same | |
| US6245310B1 (en) | Process for the manufacture of dispersible alumino-silicates | |
| KR20020080451A (ko) | 티탄 함유 제올라이트의 제조방법 | |
| EP0102097B1 (en) | Process for oxidising vinylbenzene compounds to beta-phenylaldehydes | |
| CA1315767C (en) | Process for the preparation of crystalline (metallo) silicates | |
| EP0224531B1 (fr) | Zeolites du type borosilicate contenant du fluor | |
| US7462744B1 (en) | Synthesis of amines using boron-containing molecular sieve CHA | |
| JPS63112540A (ja) | ４，４’−ジアミノジフェニルメタン又はその誘導体の製法 | |
| LU84790A1 (fr) | Matieres synthetiques cristallines et poreuses constituees par des oxydes de silicium et de bore,leur procede de preparation et leur utilisation | |
| JPS6372640A (ja) | ジフエニルエ−テル類の製造方法 | |
| AU658223B2 (en) | Zeolite catalyst and catalysed reactions |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| BA | A request for search or an international-type search has been filed | ||
| BB | A search report has been drawn up | ||
| A85 | Still pending on 85-01-01 | ||
| BV | The patent application has lapsed |