MXPA05001848A - Metodo de produccion para cuerpo formado de zeolita y metodo de produccion para composicion estratificada de zeolita. - Google Patents
Metodo de produccion para cuerpo formado de zeolita y metodo de produccion para composicion estratificada de zeolita.Info
- Publication number
- MXPA05001848A MXPA05001848A MXPA05001848A MXPA05001848A MXPA05001848A MX PA05001848 A MXPA05001848 A MX PA05001848A MX PA05001848 A MXPA05001848 A MX PA05001848A MX PA05001848 A MXPA05001848 A MX PA05001848A MX PA05001848 A MXPA05001848 A MX PA05001848A
- Authority
- MX
- Mexico
- Prior art keywords
- zeolite
- production method
- tpabr
- tetrapropylammonium
- tpaoh
- Prior art date
Links
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title claims abstract description 128
- 229910021536 Zeolite Inorganic materials 0.000 title claims abstract description 126
- 239000010457 zeolite Substances 0.000 title claims abstract description 126
- 238000000034 method Methods 0.000 title abstract description 21
- 238000000465 moulding Methods 0.000 title abstract 4
- 239000002131 composite material Substances 0.000 title 1
- 238000010438 heat treatment Methods 0.000 claims abstract description 47
- LPSKDVINWQNWFE-UHFFFAOYSA-M tetrapropylazanium;hydroxide Chemical compound [OH-].CCC[N+](CCC)(CCC)CCC LPSKDVINWQNWFE-UHFFFAOYSA-M 0.000 claims abstract description 38
- 238000001035 drying Methods 0.000 claims abstract description 26
- BGQMOFGZRJUORO-UHFFFAOYSA-M tetrapropylammonium bromide Chemical compound [Br-].CCC[N+](CCC)(CCC)CCC BGQMOFGZRJUORO-UHFFFAOYSA-M 0.000 claims abstract description 23
- 238000002425 crystallisation Methods 0.000 claims abstract description 16
- 230000008025 crystallization Effects 0.000 claims abstract description 16
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000001556 precipitation Methods 0.000 claims abstract description 7
- 239000012528 membrane Substances 0.000 claims description 71
- 238000004519 manufacturing process Methods 0.000 claims description 34
- 239000000203 mixture Substances 0.000 claims description 21
- 238000004898 kneading Methods 0.000 claims description 13
- -1 tetrapropylammonium ions Chemical class 0.000 claims description 13
- 239000011248 coating agent Substances 0.000 claims description 3
- 238000000576 coating method Methods 0.000 claims description 3
- 230000003068 static effect Effects 0.000 claims description 2
- 238000001694 spray drying Methods 0.000 claims 1
- 239000002808 molecular sieve Substances 0.000 abstract description 12
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 abstract description 12
- 238000000926 separation method Methods 0.000 abstract description 10
- 239000007788 liquid Substances 0.000 abstract description 5
- 230000007423 decrease Effects 0.000 abstract description 2
- 238000005373 pervaporation Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract 4
- 238000005336 cracking Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 62
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 27
- 239000000758 substrate Substances 0.000 description 25
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 24
- OSBSFAARYOCBHB-UHFFFAOYSA-N tetrapropylammonium Chemical compound CCC[N+](CCC)(CCC)CCC OSBSFAARYOCBHB-UHFFFAOYSA-N 0.000 description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 20
- 239000002245 particle Substances 0.000 description 11
- 239000000377 silicon dioxide Substances 0.000 description 11
- 238000003756 stirring Methods 0.000 description 9
- 239000000126 substance Substances 0.000 description 9
- 238000002156 mixing Methods 0.000 description 8
- 238000012423 maintenance Methods 0.000 description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 6
- 229910052681 coesite Inorganic materials 0.000 description 6
- 229910052906 cristobalite Inorganic materials 0.000 description 6
- 235000012239 silicon dioxide Nutrition 0.000 description 6
- 229910052682 stishovite Inorganic materials 0.000 description 6
- 229910052905 tridymite Inorganic materials 0.000 description 6
- 238000001354 calcination Methods 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 229910001220 stainless steel Inorganic materials 0.000 description 5
- 239000010935 stainless steel Substances 0.000 description 5
- 238000002441 X-ray diffraction Methods 0.000 description 4
- 238000013019 agitation Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 239000004570 mortar (masonry) Substances 0.000 description 3
- 230000002269 spontaneous effect Effects 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000005452 bending Methods 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000009694 cold isostatic pressing Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 230000008646 thermal stress Effects 0.000 description 2
- 238000003826 uniaxial pressing Methods 0.000 description 2
- BYHQTRFJOGIQAO-GOSISDBHSA-N 3-(4-bromophenyl)-8-[(2R)-2-hydroxypropyl]-1-[(3-methoxyphenyl)methyl]-1,3,8-triazaspiro[4.5]decan-2-one Chemical compound C[C@H](CN1CCC2(CC1)CN(C(=O)N2CC3=CC(=CC=C3)OC)C4=CC=C(C=C4)Br)O BYHQTRFJOGIQAO-GOSISDBHSA-N 0.000 description 1
- 235000019687 Lamb Nutrition 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- 239000005388 borosilicate glass Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012013 faujasite Substances 0.000 description 1
- 239000002241 glass-ceramic Substances 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000000644 propagated effect Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 229940073455 tetraethylammonium hydroxide Drugs 0.000 description 1
- LRGJRHZIDJQFCL-UHFFFAOYSA-M tetraethylazanium;hydroxide Chemical compound [OH-].CC[N+](CC)(CC)CC LRGJRHZIDJQFCL-UHFFFAOYSA-M 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/22—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
- B01D53/228—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion characterised by specific membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
- B01D61/362—Pervaporation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0039—Inorganic membrane manufacture
- B01D67/0048—Inorganic membrane manufacture by sol-gel transition
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0039—Inorganic membrane manufacture
- B01D67/0051—Inorganic membrane manufacture by controlled crystallisation, e,.g. hydrothermal growth
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0081—After-treatment of organic or inorganic membranes
- B01D67/0095—Drying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/10—Supported membranes; Membrane supports
- B01D69/107—Organic support material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
- B01D71/02—Inorganic material
- B01D71/028—Molecular sieves
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
- C01B37/02—Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2323/00—Details relating to membrane preparation
- B01D2323/08—Specific temperatures applied
- B01D2323/081—Heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2323/00—Details relating to membrane preparation
- B01D2323/24—Use of template or surface directing agents [SDA]
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Water Supply & Treatment (AREA)
- Manufacturing & Machinery (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dispersion Chemistry (AREA)
- Geology (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2002237692 | 2002-08-16 | ||
PCT/JP2003/010373 WO2004016552A1 (fr) | 2002-08-16 | 2003-08-15 | Procede de production d'un moulage en zeolite et procede de production de composite lamine en zeolite |
Publications (1)
Publication Number | Publication Date |
---|---|
MXPA05001848A true MXPA05001848A (es) | 2005-06-03 |
Family
ID=31884443
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MXPA05001848A MXPA05001848A (es) | 2002-08-16 | 2003-08-15 | Metodo de produccion para cuerpo formado de zeolita y metodo de produccion para composicion estratificada de zeolita. |
Country Status (11)
Country | Link |
---|---|
EP (1) | EP1544170B1 (fr) |
JP (1) | JP4313307B2 (fr) |
CN (1) | CN1307096C (fr) |
AU (1) | AU2003255046A1 (fr) |
BR (1) | BR0313531B1 (fr) |
CA (1) | CA2494990C (fr) |
DE (1) | DE60333571D1 (fr) |
MX (1) | MXPA05001848A (fr) |
NZ (1) | NZ538140A (fr) |
WO (1) | WO2004016552A1 (fr) |
ZA (1) | ZA200501262B (fr) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4589073B2 (ja) * | 2004-10-07 | 2010-12-01 | 日本碍子株式会社 | ゼオライト成形体の製造方法 |
CN100408476C (zh) * | 2005-09-07 | 2008-08-06 | 中国石油化工股份有限公司 | 无粘结剂zsm型分子筛的制备方法 |
JP6234297B2 (ja) * | 2014-03-27 | 2017-11-22 | 株式会社タカギ | ゼオライト成形体およびその製造方法 |
CN107303506B (zh) * | 2016-04-21 | 2019-10-15 | 中国石油化工股份有限公司 | 一种石蜡烃择型异构化催化剂的预处理方法 |
CN109422272A (zh) * | 2017-08-31 | 2019-03-05 | 中国科学院大连化学物理研究所 | 一种合成具有afi结构杂原子金属磷酸铝分子筛的方法 |
CN109422273A (zh) * | 2017-08-31 | 2019-03-05 | 中国科学院大连化学物理研究所 | 一种合成具有ato结构杂原子金属磷酸铝分子筛的方法 |
CN109422280A (zh) * | 2017-08-31 | 2019-03-05 | 中国科学院大连化学物理研究所 | 一种合成具有afi结构磷酸铝分子筛的方法 |
CN110898684B (zh) * | 2019-11-22 | 2023-01-24 | 上海绿强新材料有限公司 | 一种emt分子筛膜的制备方法 |
CN116371463B (zh) * | 2023-03-13 | 2024-09-17 | 中触媒新材料股份有限公司 | 一种低磨损率sapo-34分子筛催化剂及其制备方法和应用 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59213615A (ja) * | 1983-05-13 | 1984-12-03 | Toa Nenryo Kogyo Kk | 膜状合成ゼオライト及びその製造方法 |
US5164169A (en) * | 1991-06-14 | 1992-11-17 | Mobil Oil Corporation | Zeolite Beta |
FR2715648B1 (fr) * | 1994-01-31 | 1996-04-05 | Elf Aquitaine | Solides microporeux cristallisés consistant en aluminophosphates substitués par un métal et éventuellement par du silicium et appartenant au type structural Fau, leurs synthèses et applications. |
JP3763598B2 (ja) * | 1995-09-11 | 2006-04-05 | 旭電化工業株式会社 | トラネキサム酸の製造方法 |
US6667265B1 (en) * | 1998-10-20 | 2003-12-23 | Ngk Insulators, Ltd. | Zeolite composite film and process for producing the same |
EP1061046B1 (fr) * | 1999-06-18 | 2007-09-26 | Nippon Shokubai Co., Ltd. | Moulage de zéolithe sans liant, procédé pour sa fabrication et son utilisation. |
JP2001114511A (ja) * | 1999-10-18 | 2001-04-24 | Masahiko Matsukata | βゼオライトおよびその製造方法 |
AU770058B2 (en) * | 2000-03-02 | 2004-02-12 | Ngk Insulators, Ltd. | Zeolite formed product, zeolite laminate intermediate, zeolite laminate composite and method for their preparation |
-
2003
- 2003-08-15 MX MXPA05001848A patent/MXPA05001848A/es active IP Right Grant
- 2003-08-15 WO PCT/JP2003/010373 patent/WO2004016552A1/fr active Application Filing
- 2003-08-15 NZ NZ538140A patent/NZ538140A/en unknown
- 2003-08-15 DE DE60333571T patent/DE60333571D1/de not_active Expired - Lifetime
- 2003-08-15 AU AU2003255046A patent/AU2003255046A1/en not_active Abandoned
- 2003-08-15 CA CA002494990A patent/CA2494990C/fr not_active Expired - Fee Related
- 2003-08-15 EP EP03788122A patent/EP1544170B1/fr not_active Expired - Lifetime
- 2003-08-15 JP JP2004528887A patent/JP4313307B2/ja not_active Expired - Fee Related
- 2003-08-15 ZA ZA200501262A patent/ZA200501262B/en unknown
- 2003-08-15 CN CNB038240912A patent/CN1307096C/zh not_active Expired - Fee Related
- 2003-08-15 BR BRPI0313531-4A patent/BR0313531B1/pt not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CN1307096C (zh) | 2007-03-28 |
EP1544170A4 (fr) | 2006-10-11 |
JPWO2004016552A1 (ja) | 2005-12-02 |
AU2003255046A1 (en) | 2004-03-03 |
NZ538140A (en) | 2006-04-28 |
ZA200501262B (en) | 2006-10-25 |
CA2494990C (fr) | 2008-07-29 |
BR0313531B1 (pt) | 2013-01-22 |
EP1544170A1 (fr) | 2005-06-22 |
DE60333571D1 (de) | 2010-09-09 |
CA2494990A1 (fr) | 2004-02-26 |
CN1688510A (zh) | 2005-10-26 |
EP1544170B1 (fr) | 2010-07-28 |
WO2004016552A1 (fr) | 2004-02-26 |
BR0313531A (pt) | 2005-07-12 |
JP4313307B2 (ja) | 2009-08-12 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG | Grant or registration |